IP Library › Granted Patent US 10,471,388
Granted Patent B2
US 10,471,388 · App. 16/091,097 · Granted Nov 12, 2019

Sulfur dioxide removal from waste gas

Inventor: Alain Strickroth (Belvaux, LU)
Assignee: CPPE CARBON PROCESS & PLANT ENGINEERING S.A.
B01D53/8609B01D53/8665B01D53/8687B01J21/18B01J35/0026B01J35/023B01J35/1028C01B17/78B01D2255/702B01D2257/302B01D2258/025
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Quick Facts
Patent No.
US 10,471,388
App. No.
16/091,097
Granted
Nov 12, 2019
Kind
B2
Abstract

A process where a gas, containing SO 2 and O 2 is brought in contact with a mixture of from 95% vol. to 50% vol. of activated carbon catalyst and from 5% vol. to 50% vol. of an inert filler material, where the SO 2 is converted to H 2 SO 4 on the activated carbon catalyst and is then washed from the activated carbon catalyst to obtain a H 2 SO 4 solution.

Claims (20)

1. A process, comprising:

bringing a gas, containing SO 2 and O 2 , in contact with a mixture of from 95% vol. to 50% vol. of activated carbon catalyst and from 5% vol. to 50% vol. of an inert filler material;

wherein the mixture is a mixture of separate, distinct particles of filler and separate, distinct particles of activated carbon catalyst; and

wherein the SO 2 is converted to H 2 SO 4 on the activated carbon catalyst and is then washed from the activated carbon catalyst to obtain a H 2 SO 4 solution.

2. The process as claimed in claim 1 , wherein the filler material is between 10% vol. and 30% vol. of the mixture of activated carbon catalyst and a filler material.

3. The process as claimed in claim 1 , wherein the mixture contains no other solid ingredients than the activated carbon catalyst and the filler material.

4. The process as claimed in claim 1 , wherein the activated carbon catalyst is chosen from impregnated or activated carbon catalysts.

5. The process as claimed in claim 1 , wherein the filler is chosen from fillers made of ceramic material, made of metal, fillers made of plastic mineral or mixtures thereof.

6. The process as claimed in claim 1 , wherein the filler material is a shape comprising saddle shaped, ring shaped, ball shaped, torus shaped, prism shaped or irregular shaped.

7. The process as claimed in claim 1 , wherein the mixture is in a fixed bed.

8. The process as claimed in claim 1 , wherein the mixture is washed with water or an aqueous solution in an amount between 5 l/hour/m 3 of catalyst and 100 l/hour/m 3 of mixture.

9. The process as claimed in claim 1 , wherein the mixture is washed by intermittent spraying with water or an aqueous solution in counterflow to the gas.

10. The process as claimed in claim 1 , wherein the process is operated at a pressure from 0.9 to 1.1 atm.

11. The process as claimed in claim 1 , wherein the water saturated gas containing SO 2 and O 2 is a waste gas generated by chemical and metallurgical processes.

12. The process as claimed in claim 1 wherein the SO 2 content of the gas is between 300 ppm and 200,000 ppm.

13. The process as claimed in claim 1 , the gas being brought into contact with the mixture has a temperature of between 10 and 150° C.

14. The process as claimed in claim 1 , wherein the O 2 content of the gas is between 2 and 21% vol.

15. The process as claimed in claim 1 , wherein the H 2 SO 4 content of the H 2 SO 4 solution is between 5 and 50% vol.

16. The process as claimed in claim 1 , wherein heavy metals are removed from the gas.

17. The process as claimed in claim 1 , wherein organic contaminants are removed from the gas.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2018
From: STRICKROTH, ALAIN
To: CPPE CARBON PROCESS & PLANT ENGINEERING S.A.
Reel/Frame 047073/0851 →
Priority Claims (1)
LU 93012 · Apr 4, 2016 · national
Continuity (1)
Related Publication 20190126200A1 · May 2, 2019
Cited By (1)
US 12,654,132