IP Library Granted Patent US 10,487,388
Granted Patent B2
US 10,487,388 · App. 14/425,098 · Granted Nov 26, 2019

Tool with TiAlCrSiN PVD coating

Inventor: Veit Schier (Leinfelden-Echterdingen, DE)
Assignee: Walter AG
C23C14/0641B23B27/148C23C14/325C23C28/042C23C28/044C23C28/42C23C30/005Y10T428/24355Y10T428/24975
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Quick Facts
Patent No.
US 10,487,388
App. No.
14/425,098
Granted
Nov 26, 2019
Kind
B2
Abstract

Tool with main body made of carbide, cermet, ceramic, steel or high-speed steel and multi-layer wear-protection coating applied on the main body using a PVD process. The wear-protection coating comprises at least one layer (A) of Ti a Al (1−a) N where 0.33≤a≤1 with layer thickness of 20 nm to 3 μm and at least one layer (B) comprising a sequence of at least 4 sub-layers arranged alternately in a stack, of Ti b Si (1−b) N and Al c Cr (1−c) N where 0.70≤b≤0.98 and 0.3≤c≤0.75 with sub-layer thickness of 0.5 nm to 15 nm, and optionally further comprises a layer (C) of Ti d Si (1−d) N where 0.70≤d≤0.98 with layer thickness of 50 nm to 1 μm. The wear-protection coating can have further carbide layers and layers (A), (B) and (C) can contain up to 10 at. % of other metals, B, C and/or O per layer, depending on the process.

Claims (36)

1. A tool, comprising:

a main body made of hard metal, cermet, ceramic, steel or high-speed steel, and

a multi-layer wear protection coating which is applied on the main body by a PVD process,

wherein the wear protection coating comprises

at least one layer (A) of Ti a Al (1−a) N with 0.33≤a≤1 and with a layer thickness of from 20 nm to 3 μm, and

at least one layer (B) of a sequence of at least 4 alternating superposed sublayers of Ti b Si (1−b) N and Al c Cr (1−c) N with 0.70≤b≤0.98 and 0.3≤c≤0.75, each of the sublayers having a layer thickness that is the same and is from 3.0 nm to 9.0 nm and forming a periodic structure, and

optionally in addition at least one layer (C) of Ti d Si (1−d) N with 0.70≤d≤0.98 and with a layer thickness of from 50 nm to 1 μm.

2. The tool according to claim 1 , wherein the layer (B) exhibits a sequence of at least 4 sublayers of Ti b Si (1−b) N and 4 sublayers of Al c Cr (1−c) N arranged superposed in alternation and/or wherein the layer (B) exhibits a sequence of at most 1500 sublayers of Ti b Si (1−b) N and 1500 sublayers of Al c Cr (1−c) N arranged superposed in alternation.

3. The tool according to claim 1 , wherein the layer (B) exhibits a total layer thickness of from 40 nm to 3 μm.

4. The tool according to claim 1 , wherein the wear protection coating exhibits one of the following sequences of layers, in which m, n, o, p, q and r are whole numbers>0:

[A-B] n with 1≤n≤100

([A-B] n -C) m with 1≤n≤100 and 15≤m≤20

A-[B-C] n with 1≤n≤30

[A-B-C] n with 2≤n≤30

{([A-B] o -C) q -(A-[B-C] p ) r } m with 1≤o≤30, 1≤p≤30, 1≤q≤30, p+q≥2, (13q+25r)m≤500.

5. The tool according to claim 1 , wherein the sublayers of Ti b Si (1−b) N and Al c Cr (1−c) N exhibit a cubically face-centered crystal structure.

6. The tool according to claim 1 , wherein the wear protection coating exhibits a total thickness of from 0.5 μm to 10 μm.

7. The tool according to claim 6 , wherein the total thickness of the wear protection coating is from 1.0 μm to 3.0 μm.

8. The tool according to claim 1 , wherein the wear protection coating includes, at least in regions arranged as an outermost layer, a thin wear recognition layer with a thickness of from 0.1 to 1.5 μm.

9. The tool according to claim 8 , wherein the thin wear recognition layer is a TiN or ZrN layer.

10. The tool according to claim 1 , wherein the wear protection coating exhibits a Vickers hardness HV of from 2500 to 4000.

11. The tool according to claim 10 , wherein the Vickers hardness HV of the wear protection coating is from 3000 to 3500.

12. The tool according to claim 1 , wherein the wear protection coating exhibits a modulus of elasticity (E-modulus) of >380 GPa.

13. The tool according to claim 12 , wherein the modulus of elasticity (E-modulus) of the wear protection coating is >400 GPa.

14. The tool according to claim 1 , wherein the tool is an indexable cutter insert and/or wherein the tool is a solid hard metal tool.

15. The tool according to claim 1 , wherein the wear protection coating exhibits a mean surface roughness Ra, measured over a length of 10 μm, of ≤1.0 μm.

16. The tool according to claim 15 , wherein the mean surface roughness Ra, measured over a length of 10 μm, is ≤0.5 μm.

17. The tool according to claim 1 , wherein the wear protection coating exhibits the following sequence of layers, in which n is a whole number>0:

[A-B] n with 1≤n≤100.

18. The tool according to claim 1 , wherein the wear protection coating exhibits one of the following sequences of layers, in which m and n are whole numbers>0:

([A-B] n -C) m with 1≤n≤100 and 15≤m≤20

[A-B-C] n with 2≤n≤30.

19. The tool according to claim 1 , wherein the wear protection coating includes one or more further layers having a composition of TiN, TiAlN, TiCN, AlCrN, TiAlCrN or TiAlCrSiN.

20. The tool according to claim 19 , wherein the wear protection coating includes, at least in regions arranged as an outermost layer, a thin wear recognition layer with a thickness of from 0.1 to 1.5 μm.

21. The tool according to claim 1 , wherein the wear protection coating includes one or more further layers having a composition including one or more of Ti, Al, Cr and Si and one or more of N, B, C and O.

22. The tool according to claim 21 , wherein the wear protection coating includes, at least in regions arranged as an outermost layer, a thin wear recognition layer with a thickness of from 0.1 to 1.5 μm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 24, 2015
From: SCHIER, VEIT
To: WALTER AG
Reel/Frame 035237/0414 →
Priority Claims (1)
DE 10 2012 109 254 · Sep 28, 2012 · national
Continuity (1)
Related Publication 20150232978A1 · Aug 20, 2015