IP Library Granted Patent US 10,508,041
Granted Patent B2
US 10,508,041 · App. 15/430,570 · Granted Dec 17, 2019

Anhydrous, amorphous and porous magnesium carbonates and methods of production thereof

Inventors: Maria Strömme (Uppsala, SE); Albert Mihranyan (Uppsala, SE); Johan Gómez De La Torre (Uppsala, SE); Sara Frykstrand Ångström (Sollentuna, SE)
Assignee: Disruptive Materials AB
C01F5/02A23L33/16A61K8/19A61K31/192A61K47/02A61Q19/00B01J20/043B01J20/267B01J20/28011B01J20/28019B01J20/28059B01J20/28061B01J20/28064B01J20/28066B01J20/28071B01J20/28083B01J41/14B01J45/00C01F5/24A23V2002/00A61K9/143A61K2800/10C01P2002/02C01P2002/72C01P2002/74C01P2002/82C01P2002/85C01P2002/88C01P2004/03C01P2006/12C01P2006/14C01P2006/16C01P2006/17Y02C10/08
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Quick Facts
Patent No.
US 10,508,041
App. No.
15/430,570
Granted
Dec 17, 2019
Kind
B2
Abstract

An X-ray amorphous magnesium carbonate is disclosed that is characterized by a cumulative pore volume of pores with a diameter smaller than 10 nm of at least 0.018 cm 3 /g, and a specific surface areas of at least 60 m 2 /g. The X-ray amorphous magnesium carbonate is produced by reacting an inorganic magnesium compound with alcohol in a CO 2 atmosphere. The X-ray amorphous magnesium carbonate can be a powder or a pellet and acts as a desiccant in, for example, production of food, chemicals or pharmaceuticals.

Claims (20)

1. A magnesium carbonate, wherein the magnesium carbonate is X-ray amorphous and is anhydrous, and wherein the magnesium carbonate has an incremental pore volume in cm 3 /g that has a maximum value of less than 0.08 cm 3 /g for pores with a diameter of 30 nm or less, and wherein the incremental pore volume is measured by nitrogen adsorption, and wherein the magnesium carbonate with pores with a diameter of 30 nm or less is 83% of the magnesium carbonate powder.

2. The magnesium carbonate according to claim 1 , wherein the magnesium carbonate with pores with a diameter of 30 nm or less has a cumulative pore volume of less than 0.4 cm 3 /g.

3. The magnesium carbonate of claim 1 , wherein the magnesium carbonate is characterized by a BET specific surface area obtained from N 2 sorption isotherms of between 60 m 2 /g and 1500 m 2 /g.

4. The magnesium carbonate of claim 3 , wherein the magnesium carbonate is characterized by a BET specific surface area obtained from N 2 sorption isotherms of between 600 m 2 /g and 1500 m 2 /g.

5. The magnesium carbonate of claim 1 , wherein the magnesium carbonate is characterized by adsorbing more than 0.3 mmol water/g material at an RH of 3% at room temperature.

6. The magnesium carbonate of claim 5 , wherein the magnesium carbonate is characterized by adsorbing more than 14 mmol water/g material at an RH of 90% at room temperature.

7. A desiccant comprising the magnesium carbonate according to claim 1 .

8. A pellet or a film comprising the magnesium carbonate according to claim 1 .

9. An additive to a food, a chemical, a cosmetic or a pharmaceutical comprising the magnesium carbonate according to claim 1 .

10. An excipient in a cosmetic or a pharmaceutical comprising the magnesium carbonate according to claim 1 .

11. A magnesium carbonate, wherein the magnesium carbonate is X-ray amorphous and is anhydrous, and wherein the magnesium carbonate has an incremental pore volume in cm 3 /g that has a maximum value of less than 0.08 cm 3 /g for pores with a diameter between 10 and 30 nm, the incremental pore volume measured by nitrogen adsorption, and wherein the magnesium carbonate with pores with a diameter between 10 and 30 nm is 80% of the magnesium carbonate powder.

12. The magnesium carbonate according to claim 11 , wherein the magnesium carbonate with pores with a diameter between 10 and 30 nm has a cumulative pore volume of 0.386 cm 3 /g.

13. The magnesium carbonate of claim 11 , wherein the magnesium carbonate is characterized by a BET specific surface area obtained from N 2 sorption isotherms of between 60 m 2 /g and 1500 m 2 /g.

14. The magnesium carbonate of claim 13 , wherein the magnesium carbonate is characterized by a BET specific surface area obtained from N 2 sorption isotherms of between 600 m 2 /g and 1500 m 2 /g.

15. The magnesium carbonate of claim 11 , wherein the magnesium carbonate is characterized by adsorbing more than 0.3 mmol water/g material at an RH of 3% at room temperature.

16. The magnesium carbonate of claim 15 , wherein the magnesium carbonate is characterized by adsorbing more than 14 mmol water/g material at an RH of 90% at room temperature.

17. A desiccant comprising the magnesium carbonate according to claim 11 .

18. A pellet or a film comprising the magnesium carbonate according to claim 11 .

19. An additive to a food, a chemical, a cosmetic or a pharmaceutical comprising the magnesium carbonate according to claim 11 .

20. An excipient in a cosmetic or a pharmaceutical comprising the magnesium carbonate according to claim 11 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 19, 2021
From: DISRUPTIVE MATERIALS AB
To: DISRUPTIVE MATERIALS OPERATIONS AB
Reel/Frame 056896/0595 →
Continuity (3)
Continuation 14648780
Provisional Application 61734144 · Dec 6, 2012
Related Publication 20170152151A1 · Jun 1, 2017
Cited By (2)
US 12,419,816 US 12,459,829