IP Library › Granted Patent US 10,514,370
Granted Patent B2
US 10,514,370 · App. 15/041,098 · Granted Dec 24, 2019

Methods and systems for measuring anions

Inventors: Dilshad Masih (Thuwal, SA); Omar F. Mohammed (Thuwal, SA); Shawkat M. Aly (Thuwal, SA); Erkki Alarousu (Thuwal, SA)
Assignee: KING ABDULLAH UNIVERSITY OF SCIENCE AND TECHNOLOGY
G01N33/182G01N21/6428G01N33/582G01N33/84G01N21/6408G01N2021/6432
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Quick Facts
Patent No.
US 10,514,370
App. No.
15/041,098
Granted
Dec 24, 2019
Kind
B2
Abstract

Embodiments of the present disclosure provide for methods for detecting the presence and/or concentration of anions in a solution, systems for detecting the presence and/or concentration of anions in a solution, anion sensor systems, and the like.

Claims (23)

1. A method of detecting anions, comprising:

contacting a solution including an anion with a Pt(II) porphyrin;

irradiating the solution with visible light;

measuring a photoluminescence signal from the Pt(II) porphyrin; and

determining the presence of the anion;

wherein the Pt(II) porphyrin is 5, 10, 15, 20-tetra(1-methyl-4-pyridino)-porphyrin Pt(II) tetrachloride.

2. The method of claim 1 , wherein the anion is selected from the group consisting of: a halogen anion, a sulfide anion, and a cyanide anion.

3. The method of claim 1 , wherein the anion is iodide.

4. The method of claim 3 , wherein the anion is present at a level of at least about 30 pmol in the solution.

5. The method of claim 1 , further comprising: measuring a UV-Vis signal.

6. A sensor system, comprising:

a structure having a Pt(II) porphyrin disposed on the surface;

a compartment including a solution including an anion, wherein the anion is selected from the group consisting of a halogen anion, a sulfide anion, and a cyanide anion, wherein the anion and Pt(II) porphyrin interact to quench the photoluminescence of the Pt(II) porphyrin once the structure is placed in the compartment with the solution;

a system for irradiating the solution with visible light; and

a system for measuring a signal selected from a photoluminescence signal, UV-Vis signal, or a combination thereof, wherein a change in the signal relative to a signal without the anion present is correlated to the concentration of the anion in the solution.

7. The system of claim 6 , wherein the anion is present at a level of at least about 30 pmol in the solution.

8. The system of claim 6 , wherein the Pt(II) porphyrin is 5, 10, 15, 20-tetra(1-methyl-4-pyridino)-porphyrin (Pt(II) tetrachloride.

9. A method comprising, comprising:

placing a structure having a Pt(II) porphyrin disposed on the surface in a compartment including a solution including an anion, wherein the anion is selected from the group consisting of a halogen anion, a sulfide anion, and a cyanide anion, wherein the anion and Pt(II) porphyrin interact to quench the photoluminescence of the Pt(II) porphyrin;

irradiating the solution with visible light; and

measuring a signal selected from a photoluminescence signal, UV-Vis signal, or a combination thereof, wherein a change in the signal relative to a signal without the anion present is correlated to the concentration of the anion in the solution.

10. The method of claim 9 , wherein the anion is present at a level of at least about 30 pmol in the solution.

11. The method of claim 10 , wherein the Pt(II) porphyrin is 5, 10, 15, 20-tetra(1-methyl-4-pyridino)-porphyrin (Pt(II) tetrachloride.

Continuity (2)
Provisional Application 62115354 · Feb 12, 2015
Related Publication 20160238582A1 · Aug 18, 2016
Cited By (1)
US 12,320,774