Process and apparatus for vacuum distillation of high-purity magnesium
A process for producing high-purity magnesium by means of distillation at reduced pressure, characterized in that, the high-purity magnesium condenses in the liquid state, whereby the starting material in the form of a magnesium-containing melt is present together with the upper region of a condensation vessel in the upper region of a retort, whereby the retort consist of a material that releases no volatile impurities into the magnesium steam, whereby the upper region of the retort is brought to a temperature above the boiling point of magnesium, within the limits of two level lines, and is then held constant, such that steam rises from the boiling magnesium-containing metal melt and fills the interior of the upper region of the retort, whereby the steam infiltrating the upper region of the condensation vessel condenses below the lower level line and collects as high-purity melt in the lower region of the condensation vessel, and whereby in order to prevent contaminated melt that drops from the region above the upper level line from reaching the opening of the condensation vessel, this is protected by a cover, which conveys the impure magnesium back again into the melt.
1. An apparatus for producing high-purity magnesium by means of distillation at reduced pressure, the apparatus comprising:
a retort and a condensation vessel protected by a cover,
whereby an upper region of the condensation vessel is in an upper region of the retort,
whereby the upper region of the retort is surrounded by a heating element, suitable for heating the upper region of the retort between two different level lines to a temperature above the boiling point of magnesium, and
whereby the condensation vessel is arranged in a way, that the lower part of the condensation vessel is located below the level lines and at a temperature below the boiling point of magnesium, further whereby the condensation vessel is integrally constructed with a closed bottom.
2. The apparatus according to claim 1 , characterized in that, the retort is made of stainless steel.
3. The apparatus according to claim 1 , characterized in that, the cover comprises graphite.
4. The apparatus according to claim 1 , characterized in that, a supply chamber is connected to the retort, whereby the supply chamber is connected with means for evacuating the retort.
5. The apparatus according to claim 4 , whereby the supply chamber is arranged above the retort.
6. The apparatus according to claim 1 , whereby the lower part of the condensation vessel is surrounded by an insulation layer dimensioned to hold the temperature between the melting temperature and the boiling temperature.
7. The apparatus according to claim 1 , whereby the bottom of the condensation vessel is not insulated.