IP Library › Granted Patent US 10,640,632
Granted Patent B2
US 10,640,632 · App. 16/062,418 · Granted May 5, 2020

Bimodal cellulose composition

Inventors: Antti Laukkanen (Helsinki, FI); Jason Mckee (Helsinki, FI)
Assignee: BETULIUM OY
C08L1/02C08L97/005D21H11/18B82Y30/00C08L5/14C08L89/00C08L97/02
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Quick Facts
Patent No.
US 10,640,632
App. No.
16/062,418
Granted
May 5, 2020
Kind
B2
Abstract

A method of producing from cellulose pith a composition having bimodal distribution of its components. The composition can be used to modify rheological properties of compositions of matter and for making articles of manufacture and nanocomposites.

Claims (21)

1. A process for preparing a composition comprising:

A nanofibrillar parenchymal cellulose; and

B cellulose fibers;

wherein both A and B are obtained from cellulose pith, the process comprising:

a. providing or isolating cellulose pith from cellulose pith material;

b. treating the cellulose pith with an alkali; and

c. fibrillating the alkali treated cellulose pith.

2. The process of claim 1 comprising a fractionating step between steps a. and b., or between the steps b. and c., to recover a parenchymal cell rich fraction or to alter the relative fraction of parenchymal cells and cellulose fibers.

3. The process of claim 2 wherein the fractionating step is by dry fractioning or wet fractioning.

4. The process of claim 1 comprising a fractionating step after step c to recover the nanofibrillar parenchymal cell rich fraction or to alter the relative fraction of A and B fractions.

5. The process of claim 1 wherein the alkali treatment in step b. comprises washing the alkali treated cellulose pith and removing the filtrate.

6. The process of claim 1 wherein a chemical derivatization is carried before, after or during the step b, the chemical derivatization including cationization, oxidation, bleaching, acetylation, esterification, etherification reactions, or a combination thereof.

7. The process of claim 2 comprising a fractionating step after step c to recover the nanofibrillar parenchymal cell rich fraction or to alter the relative fraction of A and B fractions.

8. The process of claim 3 comprising a fractionating step after step c to recover the nanofibrillar parenchymal cell rich fraction or to alter the relative fraction of A and B fractions.

9. The process of claim 2 wherein the alkali treatment in step b. comprises washing the alkali treated cellulose pith and removing the filtrate.

10. The process of claim 3 wherein the alkali treatment in step b. comprises washing the alkali treated cellulose pith and removing the filtrate.

11. The process of claim 4 wherein the alkali treatment in step b. comprises washing the alkali treated cellulose pith and removing the filtrate.

12. The process of claim 2 wherein a chemical derivatization is carried before, after or during the step b, the chemical derivatization including cationization, oxidation, bleaching, acetylation, esterification, etherification reactions, or a combination thereof.

13. The process of claim 3 wherein a chemical derivatization is carried before, after or during the step b, the chemical derivatization including cationization, oxidation, bleaching, acetylation, esterification, etherification reactions, or a combination thereof.

14. The process of claim 4 wherein a chemical derivatization is carried before, after or during the step b, the chemical derivatization including cationization, oxidation, bleaching, acetylation, esterification, etherification reactions, or a combination thereof.

15. The process of claim 5 wherein a chemical derivatization is carried before, after or during the step b, the chemical derivatization including cationization, oxidation, bleaching, acetylation, esterification, etherification reactions, or a combination thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 7, 2018
From: LAUKKANEN, ANTTI; MCKEE, JASON
To: BETULIUM OY
Reel/Frame 047705/0272 →
Priority Claims (1)
FI 20155950 · Dec 15, 2015 · national
Continuity (1)
Related Publication 20180371211A1 · Dec 27, 2018