IP Library Granted Patent US 10,648,064
Granted Patent B2
US 10,648,064 · App. 16/405,265 · Granted May 12, 2020

Method for creating porous structures by particle expansion

Inventors: Mark Andrew Atwater (Sunbury, PA); Kris Allen Darling (Havre de Grace, MD); Mark Allen Tschopp, Jr. (Bel Air, MD)
Assignees: Millersville University of Pennsylvania; The United States Of America As Represented By The Secretary Of The Army
C22C1/08B22F3/1143B22F2009/043B22F2998/10B22F2999/00
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Quick Facts
Patent No.
US 10,648,064
App. No.
16/405,265
Granted
May 12, 2020
Kind
B2
Abstract

A process for producing a metal foam includes mechanically working a metallic powder such that oxide particles are finely dispersed within a metallic matrix and annealing the mechanically worked metallic powder in a vacuum the annealed metallic powder such that intraparticle porosity is formed by decomposition of the oxide particles at elevated temperature to reduce the oxide particles to metallic form and liberate the oxygen atoms in gaseous form, thereby creating porosity.

Claims (11)

1. A process for producing a metal foam comprising:

mechanically working a metallic powder such that oxide particles and/or dissolved oxygen are finely dispersed within a metallic matrix;

annealing the mechanically worked metallic powder in a vacuum; and

forming the metal foam of the annealed metallic powder having intraparticle porosity formed by decomposition of the oxide particles at an elevated temperature to reduce the oxide particles to metallic form and liberate the oxygen atoms in gaseous form, thereby creating porosity.

2. The process of claim 1 , wherein the metallic powder is a silver containing metallic powder.

3. The process of claim 1 , wherein the mechanical working ball milling the metallic powder.

4. The process of claim 1 , wherein the metallic powder is a copper containing metallic powder.

5. The process of claim 3 , wherein the ball milling is cryogenic ball milling.

6. The process of claim 3 , wherein the ball milling is room temperature ball milling.

7. The process of claim 1 , wherein the annealing occurs at a temperature less than or equal to 800° C.

8. The process of claim 1 , wherein the annealing occurs at a temperature less than or equal to 400° C.

Assignments (3)
CONFIRMATORY LICENSE Recorded Nov 11, 2022
From: THE PENNSYLVANIA STATE UNIVERSITY
To: UNITED STATES ARMY/ARO
Reel/Frame 061931/0408 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 13, 2020
From: ATWATER, MARK ANDREW
To: MILLERSVILLE UNIVERSITY OF PENNSYLVANIA
Reel/Frame 051497/0310 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 13, 2020
From: DARLING, KRIS ALLEN; TSCHOPP, MARK ALLEN, JR.
To: THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE ARMY
Reel/Frame 051497/0629 →
Continuity (4)
Continuation In Part 16241345 · Jan 7, 2019
Continuation 14811049 · Jul 28, 2015
Provisional Application 62029850 · Jul 28, 2014
Related Publication 20190264302A1 · Aug 29, 2019