IP Library Granted Patent US 10,663,448
Granted Patent B2
US 10,663,448 · App. 15/505,650 · Granted May 26, 2020

Methods of ranking formation stabilizer performance

Inventors: Venkata Satya Srikalyan Bhamidipati (Kingwood, TX); Ajish Potty (Stafford, TX); Syed Muhammad Farrukh Hamza (Houston, TX)
Assignee: HALLIBURTON ENERGY SERVICES, INC.
G01N33/24E21B21/062E21B49/005G01N21/51G01N21/64G01N33/241
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Quick Facts
Patent No.
US 10,663,448
App. No.
15/505,650
Granted
May 26, 2020
Kind
B2
Abstract

Methods of ranking formation stabilizer performance are described. The methods include obtaining drill cuttings from a subterranean formation, grinding and sieving the drill cuttings to a particle size larger than 200 mesh, adding a formation stabilizer solution to the ground and sieved drill cuttings to form a mixture, agitating the mixture, and measuring turbidity of the agitated mixture.

Claims (40)

1. A method comprising:

producing drill cuttings in a drilling fluid as a subterranean formation is drilled with the drilling fluid, wherein the subterranean formation comprises shale;

separating the drill cuttings from the drilling fluid to obtain drill cuttings from the subterranean formation;

grinding and sieving the drill cuttings to a particle size between 420 microns to 595 microns;

adding a formation stabilizer solution to the ground and sieved drill cuttings to form a mixture;

agitating the mixture; and

measuring turbidity of the agitated mixture.

2. The method of claim 1 , further comprising deducing a chemical stability, a mechanical stability, or both, of the formation from the turbidity measurement.

3. The method of claim 2 , further comprising correlating the turbidity measurement to a rock mechanical stability.

4. The method of claim 3 , wherein the rock mechanical stability comprises a hardness, a compressive strength, a tensile strength, a shear strength, a stiffness, or any combination thereof.

5. The method of claim 2 , wherein a chemical stability, a mechanical stability, or both are deduced at a planar feature.

6. The method of claim 5 , wherein the planar feature comprises a fracture face of the formation.

7. The method of claim 1 , performed on-site or off-site.

8. The method of claim 1 , wherein the shale comprises clays of the smectite group, the kaolin group, the ilite group, the chlorite group, or any combination thereof.

9. The method of claim 1 , wherein agitating the mixture comprises rotating the mixture end-over-end.

10. The method of claim 1 , wherein the formation stabilizer solution comprises one or more of potassium chloride, sodium chloride, ammonium chloride, tetramethyl ammonium chloride, a cationic polymer, a cationic surfactant, a hydrophobic resin, a transition metal, a furfuryl alcohol, ethylene glycol, a quaternary amine, or a bisquaternary amine.

11. A method comprising:

producing drill cuttings in a drilling fluid as a subterranean formation is drilled with the drilling fluid, wherein the subterranean formation comprises shale;

separating the drill cuttings from the drilling fluid to obtain drill cuttings from the subterranean formation;

grinding and sieving the drill cuttings to a particle size between 420 microns to 595 microns;

adding a plurality of formation stabilizer solutions to the ground and sieved drill cuttings to form a plurality of mixtures;

agitating the plurality of mixtures; and

measuring turbidity of the plurality of agitated mixtures.

12. The method of claim 11 , further comprising comparing the turbidity of the plurality of agitated mixtures and selecting the least turbid mixture.

13. The method of claim 11 , further comprising deducing a chemical stability, a mechanical stability, or both, of the formation from the turbidity measurements.

14. The method of claim 11 , further comprising correlating the turbidity measurements to a rock hardness.

15. The method of claim 14 , wherein the rock hardness comprises a Brinell hardness, a strength or a stiffness.

16. The method of claim 11 , wherein a chemical stability, a mechanical stability, or both are deduced at any representative location of drilling cuttings of the formation.

17. The method of claim 11 , wherein the formation stabilizer solutions comprise one or more of potassium chloride, sodium chloride, ammonium chloride, tetramethyl ammonium chloride, a cationic polymer, a cationic surfactant, a hydrophobic resin, a transition metal, a furfuryl alcohol, ethylene glycol, a quaternary amine, or a bisquaternary amine.

18. A method of ranking formation stabilizer performance comprising:

producing drill cuttings in a drilling fluid as a shale formation is drilled with the drilling fluid;

separating the drill cuttings from the drilling fluid to obtain drill cuttings from the shale formation;

grinding and sieving the drill cuttings to a particle size between 420 microns to 595 microns;

adding a plurality of formation stabilizer solutions to the ground and sieved drill cuttings to form a plurality of mixtures;

rotating the plurality of mixtures end-over-end;

measuring turbidity of the plurality of agitated mixtures;

comparing the turbidity of the plurality of agitated mixtures; and

selecting the least turbid mixture.

19. The method of claim 18 , further comprising treating the shale formation with the formation stabilizer solution in the least turbid mixture.

20. The method of claim 18 , wherein the formation stabilizer solutions comprise one or more of potassium chloride, sodium chloride, ammonium chloride, tetramethyl ammonium chloride, a cationic polymer, a cationic surfactant, a hydrophobic resin, a transition metal, a furfuryl alcohol, ethylene glycol, a quaternary amine, or a bisquaternary amine.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 22, 2017
From: BHAMIDIPATI, VENKATA SATYA SRIKALYAN; POTTY, AJISH; HAMZA, SYED MUHAMMAD FARRUKH
To: HALLIBURTON ENERGY SERVICES, INC.
Reel/Frame 041331/0098 →
Continuity (1)
Related Publication 20170241972A1 · Aug 24, 2017