IP Library Granted Patent US 10,683,371
Granted Patent B2
US 10,683,371 · App. 15/773,591 · Granted Jun 16, 2020

Device for producing poly(meth)acrylate in powder form

Inventors: Marco Krueger (Mannheim, DE); Karl Possemiers ('S Gravenwezel, BE); Gerald Gruenewald (Antwerp, BE); Juergen Freiberg (Lampertheim, DE); Markus Muehl (Mommenheim, DE)
Assignee: BASF SE
C08F2/01B01J2/16B01J4/002B01J19/24B01J19/2405C08F2/12C08F2/34C08F20/14B01J2219/0072B01J2219/00414B01J2219/185
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Quick Facts
Patent No.
US 10,683,371
App. No.
15/773,591
Granted
Jun 16, 2020
Kind
B2
Abstract

The invention relates to an apparatus for producing pulverulent poly(meth)acrylate, comprising a reactor for droplet polymerization having an apparatus for dropletization of a monomer solution for the preparation of the poly(meth)acrylate having holes through which the monomer solution is introduced, an addition point for a gas above the apparatus for dropletization, at least one gas withdrawal point on the circumference of the reactor, a fluidized bed and an apparatus for product discharge from the fluidized bed. The apparatus for product discharge comprises a discharge apparatus, with a backup segment ( 39 ) disposed above the discharge apparatus.

Claims (17)

1. An apparatus for producing pulverulent poly(meth)acrylate, comprising a

reactor for droplet polymerization having an apparatus for dropletization of a monomer solution for the preparation of the poly(meth)acrylate having holes through which the monomer solution is introduced, an addition point for a gas above the apparatus for dropletization, at least one gas withdrawal point on the circumference of the reactor, a fluidized bed and an apparatus for product discharge from the fluidized bed, wherein the apparatus for product discharge comprises a discharge apparatus, with a backup segment disposed above the discharge apparatus, the backup segment serving as a gas barrier in that by accumulation of product a compaction results.

2. The apparatus according to claim 1 , wherein the backup segment has an upper sensor for detecting a maximum fill level and a lower sensor for detecting a minimum fill level.

3. The apparatus according to claim 2 , wherein a closed-loop fill level control system is included, in which the upper sensor detects a first upper fill level and, when the latter is attained, a feed is reduced, and detects a second upper fill level and, when the latter is attained, the feed is closed, and the lower sensor detects a first lower fill level and, when the latter is attained, the product flow out of the apparatus for product discharge is reduced, and detects a second lower fill level and, when the latter is attained, the apparatus for product discharge is closed, such that no product is withdrawn.

4. The apparatus according to claim 1 , wherein a closure element is disposed above the backup segment.

5. The apparatus according to claim 1 , wherein a solids comminutor is disposed above the backup segment.

6. The apparatus according to claim 5 , wherein the solids comminutor is a lump breaker.

7. The apparatus according to claim 6 , wherein the lump breaker is a finger breaker having a breaking grid and a rotating breaking tool.

8. The apparatus according to claim 1 , wherein the discharge apparatus is a star feeder, a flap, a screw conveyor or a segmented ball valve.

9. The apparatus according to claim 1 , wherein a gas supply is disposed in the backup segment in order to introduce gas into the backup segment.

10. The apparatus according to claim 1 , wherein the apparatus for product discharge is heatable.

11. The apparatus according to claim 10 , wherein the apparatus for product discharge is heated by virtue of a solids comminutor, the backup segment and/or the discharge apparatus having electrical heating, a jacket or externally mounted heating coils, it being possible for a heating medium to flow through the jacket or the heating coils.

12. The apparatus according to claim 1 , wherein the gas withdrawal point is connected to an apparatus for fine dust removal and the apparatus for fine dust removal has a solids discharge comprising a discharge apparatus and, above the discharge apparatus, a closure element.

13. The apparatus according to claim 12 , wherein the discharge apparatus from the solids discharge of the apparatus for fine dust separation is a star feeder, a flap, a conveying screw or a segmented ball valve.

14. The apparatus according to claim 12 , wherein the closure element in the solids discharge of the apparatus for fine dust separation is a flap, a slide vane, a segmented ball valve or another valve.

15. The apparatus according to claim 12 , wherein at least one fill level sensor is positioned above the closure element.

16. The apparatus according to claim 1 , wherein the apparatus for product discharge and/or the solids discharge of an apparatus for fine dust removal open(s) into a suction line which pneumatically conveys the pulverulent poly(meth)acrylate onward.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 4, 2018
From: MUEHL, MARKUS; FREIBERG, JUERGEN; GRUENEWALD, GERALD; POSSEMIERS, KARL; KRUEGER, MARCO
To: BASF SE
Reel/Frame 045713/0602 →
Priority Claims (1)
EP 15194980 · Nov 17, 2015 · regional
Continuity (1)
Related Publication 20180319906A1 · Nov 8, 2018