Lost circulation material compositions and methods of isolating a lost circulation zone of a wellbore
A lost circulation material (LCM) composition for sealing a lost circulation zone in a wellbore is disclosed that includes from 50 weight percent to 97 weight percent epoxy resin and from 2 weight percent to 30 weight percent curing agent. The epoxy resin may include at least one of 2,3-epoxypropyl o-tolyl ether, alkyl glycidyl ethers having from 12 to 14 carbon atoms, bisphenol-A-epichlorohydrin epoxy resin, or a compound having formula (OC 2 H 3 )—CH 2 —O—R 1 —O—CH 2 —(C 2 H 3 O), where R 1 is a linear or branched hydrocarbyl having from 4 to 24 carbon atoms. A method for isolating a lost circulation zone using the LCM compositions is also disclosed and includes introducing a spacer fluid to the lost circulation zone, introducing the LCM composition to the lost circulation zone, and curing the LCM composition in the lost circulation zone to isolate the lost circulation zone.
1. A composition for sealing a lost circulation zone in a wellbore, the composition comprising:
from 50 weight percent to 97 weight percent epoxy resin based on the total weight of the composition, the epoxy resin comprising 2,3-epoxypropyl o-tolyl ether; and
from 2 weight percent to 30 weight percent curing agent based on the total weight of the composition.
2. The composition of claim 1 where the curing agent comprises at least one of tetraethylenepentamine (TEPA), diethylenetriamine (DETA), triethylenetetramine (TETA), or isophoronediamine (IPDA).
3. The composition of claim 2 where the epoxy resin comprises an epoxy equivalent weight of from 150 grams per epoxy equivalent to 350 grams per epoxy equivalent.
4. The composition of claim 2 where the epoxy resin exhibits a dynamic viscosity from 7 mPa·s to 10 mPa·s.
5. The composition of claim 2 where the epoxy resin further comprises from 0.1 weight percent to 80 weight percent bisphenol-A-epichlorohydrin based on the total weight of the epoxy resin in the composition.
6. The composition of claim 5 where the curing agent is TEPA.
7. The composition of claim 2 further comprising a reactive diluent.
8. The composition of claim 7 where the reactive diluent has the formula R—O—CH 2 —(C 2 H 3 O), where R is a hydrocarbyl having from 12 to 14 carbon atoms.
9. The composition of claim 2 where the composition has a cure time of less than or equal to 3 hours.
10. The composition of claim 2 where a density of the composition is from 55 pounds per cubic foot to 170 pounds per cubic foot.
11. The composition of claim 2 where a viscosity of the composition is from 1 millipascal seconds (mPa·s) to 50,000 mPa·s.