IP Library Granted Patent US 10,759,986
Granted Patent B2
US 10,759,986 · App. 15/679,890 · Granted Sep 1, 2020

Loss circulation material composition having alkaline nanoparticle based dispersion and water soluble hydrolysable ester

Inventors: Vikrant Wagle (Abqaiq, SA); Rajendra Kalgaonkar (Abqaiq, SA); Abdullah Al-Yami (Dhahran, SA); Zainab Alsaihati (Saihat, SA)
Assignee: Saudi Arabian Oil Company
C09K8/5086C01B32/20C01B33/1417C01F11/18C04B28/24C04B28/26C08G63/08C09K8/506C09K8/5045C09K8/516C09K8/032C09K2208/08C09K2208/10
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Quick Facts
Patent No.
US 10,759,986
App. No.
15/679,890
Granted
Sep 1, 2020
Kind
B2
Abstract

A lost circulation material (LCM) is provided having an alkaline nanosilica dispersion and an ester activator. The alkaline nanosilica dispersion and the ester activator may form a gelled solid after interaction over a contact period. Methods of lost circulation control using the LCM are also provided.

Claims (8)

1. A method to control lost circulation in a lost circulation zone in a wellbore, comprising:

introducing a lost circulation material (LCM) into the wellbore such that the LCM contacts the lost circulation zone and reduces a rate of lost circulation into the lost circulation zone as compared to a period before introducing the LCM, wherein the LCM comprises an alkaline nanosilica dispersion, a water soluble ester, and a catalyst selected to increase a hydrolysis rate of the water soluble ester, wherein the alkaline nanosilica dispersion has a pH in the range of 8.5 to 10.5, wherein the weight ratio of the alkaline nanosilica dispersion to the water soluble ester is in the range of 50:1 to 80:1, wherein the water soluble ester comprises ethyl lactate; and maintaining the LCM in contact with the lost circulation zone for a contact period to form a gelled solid, wherein the contact period comprises a range of 0.5 hours to 24 hours.

2. The method of claim 1 , wherein the LCM consists of the alkaline nanosilica dispersion and the water soluble ester.

3. The method of claim 1 , wherein the lost circulation zone has a temperature that is at least 100° F.

4. The method of claim 1 , comprising mixing the alkaline nanosilica dispersion and the water soluble ester to form the LCM at the surface before introducing the LCM into the wellbore.

5. The method of claim 1 , wherein the LCM comprises at least one of calcium carbonate particles, fibers, mica, and graphite.

6. The method of claim 5 , wherein the fibers comprises at least one of ester fibers, polypropylene fibers, starch fibers, polyketone fibers, ceramic fibers, glass fibers and nylon fibers.

7. The method of claim 1 , wherein the catalyst comprises hydrochloric acid, or sulfuric acid.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2017
From: WAGLE, VIKRANT; KALGAONKAR, RAJENDRA; AL-YAMI, ABDULLAH; ALSAIHATI, ZAINAB
To: SAUDI ARABIAN OIL COMPANY
Reel/Frame 043367/0024 →
Continuity (1)
Related Publication 20190055456A1 · Feb 21, 2019