IP Library Granted Patent US 10,800,657
Granted Patent B2
US 10,800,657 · App. 15/995,576 · Granted Oct 13, 2020

Substrate-free 2D tellurene

Inventors: Wenzhuo Wu (West Lafayette, IN); Yixiu Wang (West Lafayette, IN)
Assignee: Purdue Research Foundation
C01B19/02C30B7/10C30B7/105C30B29/02C30B29/60C30B30/00C01P2002/60C01P2002/74C01P2004/20
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Quick Facts
Patent No.
US 10,800,657
App. No.
15/995,576
Granted
Oct 13, 2020
Kind
B2
Abstract

The present disclosure generally relates to compositions comprising substrate-free 2D tellurene crystals, and the method of making and using the substrate-free 2D tellurene crystals. The 2D tellurene crystals of the present disclosure are characterized by an X-ray diffraction pattern (CuKα radiation, λ=1.54056 A) comprising a peak at 23.79 (2θ±0.1°) and optionally one or more peaks selected from the group consisting of 41.26, 47.79, 50.41, and 64.43 (2θ±0.1°).

Claims (8)

1. A composition comprising substrate-free 2D tellurene crystals, wherein the 2D tellurene crystals are characterized by an X-ray diffraction pattern (CuKα radiation, λ=1.54056 A), wherein the X-ray diffraction pattern consists of five peaks from a range of 23.79 (29±0.1°) to 64.43 (29±0.1°) within an intensity range of 7.8% to 100%, and wherein the five peaks are ranked in an order of intensity from high to low by 23.79 (29±0.1°), 47.79 (29±0.1°), 41.26 (29±0.1°), 64.43 (29±0.1°), and 50.41 (29±0.1°).

2. The composition of claim 1 , wherein the 2D tellurene crystals have a lateral length from 0.1-500 μm.

3. The composition of claim 2 , wherein the 2D tellurene crystals have a lateral length from 0.1-100 μm.

4. The composition of claim 1 , wherein the 2D tellurene crystals have a thickness from 0.5-250 nm.

5. The composition of claim 4 , wherein the 2D tellurene crystals have a thickness from 0.5-100 nm.

6. The composition of claim 1 , wherein the 2D tellurene crystals comprises 2D tellurene single crystals.

7. The composition of claim 1 , wherein the 2D tellurene crystals comprises mono layer 2D tellurene crystals.

8. The composition of claim 1 , wherein the 2D tellurene crystals comprises two or more layers of 2D tellurene crystals.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 13, 2020
From: WU, WENZHUO; WANG, YIXIU
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 051812/0263 →
Continuity (2)
Provisional Application 62521695 · Jun 19, 2017
Related Publication 20180362342A1 · Dec 20, 2018