IP Library › Granted Patent US 10,836,464
Granted Patent B2
US 10,836,464 · App. 15/100,768 · Granted Nov 17, 2020

Aluminum—copper—lithium alloy product for a lower wing skin element with improved properties

Inventor: Nicolas Bayona-Carrillo (Voiron, FR)
Assignee: CONSTELLIUM ISSOIRE
B64C3/26B21B3/00B21J1/003C22C21/14C22C21/16C22F1/057B21B2003/001
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Quick Facts
Patent No.
US 10,836,464
App. No.
15/100,768
Granted
Nov 17, 2020
Kind
B2
Abstract

The invention relates to a method for manufacturing a laminated or forged material, the thickness of which is 14 to 100 mm. The materials according to the invention are particularly suitable for manufacturing airplane underwing elements.

Claims (73)

1. A rolled and/or forged product having a thickness of between 14 and 100 mm, wherein at mid-thickness the volume fraction of grains having a brass texture is between 25 and 40% and the texture index is between 12 and 18,

wherein the rolled and/or forged product is produced by a process comprising

(a) casting a slab of alloy comprising, as a percentage by weight,

Cu: 1.8-2.6

Li: 1.3-1.8

Mg: 0.1-0.5

Mn: 0.2-0.4 and Zr<0.04

Ag: 0-0.5

Zn<0.20

Ti: 0.01-0.15

Fe: <0.1

Si: ≤0.1

other elements <0.05 each and <0.15 total, the remainder aluminum with a density less than 2.670 g/cm 3 ,

(b) homogenizing said slab at 480 to 540° C. for 5 to 60 hours,

(c) hot working said slab by rolling and/or forging, the hot working conditions being such that the final hot working temperature is at least 400° C. to obtain a rolled and/or forged product having a thickness of between 14 and 100 mm,

(d) solution-heat treating said product at 490 to 530° C. for 15 minutes to 8 hours,

(e) quenching said product with water,

(f) controlled stretching said product with a permanent deformation of 1 to 6%,

(g) artificially aging said product by heat treatment at 120 to 170° C. for 5 minutes to 100 hours.

2. The rolled and/or forged product according to claim 1 , wherein the copper content of said alloy ranges between 1.9 and 2.3% by weight.

3. The rolled and/or forged product according to claim 1 , wherein the lithium content of said alloy ranges between 1.4 and 1.6% by weight.

4. The rolled and/or forged product according to claim 1 , wherein the magnesium content of said alloy ranges between 0.1 and 0.4% by weight.

5. The rolled and/or forged product according to claim 1 , wherein the silver content of said alloy ranges between 0.05 and 0.25% by weight.

6. The rolled and/or forged product according to claim 1 , wherein the zinc content of said alloy is less than 0.05% by weight, the silicon content of said alloy is less than 0.08% by weight and the iron content of said alloy is less than 0.08% by weight.

7. The rolled and/or forged product according to claim 1 wherein aging is such that the equivalent time t(eq) at 155° C. is between 20 and 40 hours, equivalent time t(eq) at 155° C. being defined by the formula:

t

⁡

(

eq

)

=

∫

exp

⁡

(

-

11400

/

T

)

⁢

dt

exp

⁡

(

-

11400

/

T

ref

)

where T (in Kelvin) is the instantaneous treatment temperature, which changes with time t (in hours), and T ref is a reference temperature set at 428 K, and t(eq) is expressed in hours.

8. The rolled and/or forged product according to claim 1 whose thickness is between 20 mm and 50 mm and whose tensile yield strength at mid-thickness TYS (L) is at least 390 MPa, the fracture toughness KappL-T (W=406 mm) is at least 105 MPa√m after aging for 3,000 hours at 85° C. and the number of cycles in condition 6.5 MPa√m<ΔK<16.6 MPa√m is at least 250,000 for a fatigue test performed according to ASTM E647 on CCT type specimens of width W=160 mm taken in direction L-T at ¼ thickness.

9. The rolled and/or forged product according to claim 8 , wherein the tensile yield strength at mid-thickness TYS (L) is at least 395 MPa.

10. The rolled and/or forged product according to claim 8 , wherein the number of cycles in condition 6.5 MPa√m<ΔK<16.6 MPa√m is at least 280,000.

11. The product according to claim 1 as a structural element in aircraft construction, optionally as an aircraft lower wing skin element.

12. The rolled and/or forged product according to claim 1 , wherein the titanium content of said alloy ranges between 0.02 and 0.10% by weight.

13. The rolled and/or forged product according to claim 1 , wherein the density of the slab of alloy is less than 2.640 g/cm 3 .

14. The rolled and/or forged product according to claim 1 , wherein in (b), said homogenizing is at a temperature between 490 to 510° C. for 5 to 60 hours.

15. The rolled and/or forged product according to claim 7 , wherein the equivalent time t(eq) at 155° C. is between 25 and 35 hours.

16. The rolled and/or forged product according to claim 1 , wherein in (a), the slab of alloy consists essentially of, as a percentage by weight,

Cu: 1.8-2.6

Li: 1.3-1.8

Mg: 0.1-0.5

Mn: 0.2-0.4 and Zr<0.04

Ag: 0-0.5

Zn<0.20

Ti: 0.01-0.15

Fe: <0.1

Si: ≤0.1

other elements <0.05 each and <0.15 total, the remainder aluminum with a density less than 2.670 g/cm 3 .

17. The rolled and/or forged product according to claim 1 , wherein the rolled and/or forged product is produced by a process comprising:

(c) hot working said slab by rolling and/or forging, the hot working conditions being such that the final hot working temperature is at least 410° C. to obtain a rolled and/or forged product having a thickness of between 14 and 100 mm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2016
From: BAYONA-CARRILLO, NICOLAS
To: CONSTELLIUM ISSOIRE
Reel/Frame 038771/0318 →
Priority Claims (1)
FR 13 02833 · Dec 5, 2013 · national
Continuity (1)
Related Publication 20160368589A1 · Dec 22, 2016
Cited By (2)
US 12,421,586 US 12,668,863