IP Library › Granted Patent US 10,851,307
Granted Patent B2
US 10,851,307 · App. 15/681,522 · Granted Dec 1, 2020

System and method for pyrolysis using a liquid metal catalyst

Inventors: Divyaraj Desai (Sunnyvale, CA); Jessica Louis Baker Rivest (Palo Alto, CA)
Assignee: PALO ALTO RESEARCH CENTER INCORPORATED
C10B49/14B01J10/005B01J23/825B01J35/0006B01J35/12C01B3/26C01B32/05C22C9/00C22C19/007C22C38/00D01F9/127C01B32/158C01B32/182C01B32/20C01B32/25C01B2203/0277C01B2203/1058C01B2203/1076C09C1/48
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Quick Facts
Patent No.
US 10,851,307
App. No.
15/681,522
Granted
Dec 1, 2020
Kind
B2
Abstract

A process for decomposing a hydrocarbon-containing composition includes feeding the hydrocarbon-containing composition to a reactor containing a catalytically active molten metal or a catalytically active molten metal alloy, wherein the metal or alloy catalyzes a decomposition reaction of the hydrocarbon-containing composition into a hydrogen-rich gas phase and a solid carbon phase. The solid carbon phase is insoluble in the metal or alloy. The process may be a continuous process.

Claims (21)

1. A process for decomposing a hydrocarbon-containing composition, the process comprising:

feeding the hydrocarbon-containing composition to a reactor containing a catalytically active molten metal or a catalytically active molten metal alloy; and

controlling an interfacial tension within the reactor by maintaining a dynamic equilibrium of oxide to optimize bubble surface area;

wherein the metal or alloy catalyzes a decomposition reaction of the hydrocarbon-containing composition into a hydrogen-rich gas phase and a solid carbon phase;

wherein the solid carbon phase is minimally soluble in the metal or alloy;

wherein the reactor is operated at a temperature of less than 1000° C.;

wherein the hydrocarbon-containing composition is fed to the reactor through a porous diffuser extending through a wall of the reactor; and

wherein the interfacial tension is controlled by doping the hydrocarbon-containing composition with oxygen or ozone to maintain a selected degree of oxidation of the molten metal.

2. The process of claim 1 , wherein the catalytically active molten metal or the catalytically active molten metal alloy comprises gallium.

3. The process of claim 1 , wherein the catalytically active molten metal or the catalytically active molten metal alloy comprises bismuth.

4. The process of claim 1 , wherein the catalytically active molten metal or the catalytically active molten metal alloy comprises at least one carrier element selected from the group consisting of gallium and bismuth.

5. The process of claim 1 , wherein the solid carbon phase forms a floating slag in the reactor; and wherein the process further comprises removing the floating slag.

6. The process of claim 1 , wherein the reactor is connected to a gravity settler or a cyclone separator.

7. The process of claim 1 , wherein the solid carbon phase comprises carbon fibers, graphene, diamond, glassy carbon, high-purity graphite, carbon nanotubes, carbon black, coke, or activated charcoal.

8. The process of claim 1 , wherein the alloy comprises at least one catalyst element selected from the group consisting of nickel, iron, copper, zinc and palladium.

9. The process of claim 1 , wherein:

the reactor contains the catalytically active molten metal alloy and the alloy is a nickel-gallium alloy, a copper-gallium alloy, an iron-gallium alloy, or any combination thereof.

10. The process of claim 1 , wherein the porous diffuser produces bubbles with a diameter in the range of from about 100 nm to about 10 mm.

11. The process of claim 1 , wherein the hydrocarbon-containing composition is selected from:

the group consisting of natural gas, liquefied petroleum gas, naphtha, light crude oil, heavy crude oil, oil sands, shale oil, wood, biomass and organic waste streams; or

the group consisting of straight or branched chain alkanes, alkenes, alkynes, arenes, and any combination thereof with a chain length of C 1 to C 20 .

Assignments (10)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2025
From: XEROX CORPORATION
To: GENESEE VALLEY INNOVATIONS, LLC
Reel/Frame 073562/0677 →
SECOND LIEN NOTES PATENT SECURITY AGREEMENT Recorded Jul 2, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 071785/0550 →
FIRST LIEN NOTES PATENT SECURITY AGREEMENT Recorded Apr 11, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 070824/0001 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT RF 064760/0389 Recorded Feb 13, 2024
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: XEROX CORPORATION
Reel/Frame 068261/0001 →
SECURITY INTEREST Recorded Feb 13, 2024
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 066741/0001 →
SECURITY INTEREST Recorded Nov 20, 2023
From: XEROX CORPORATION
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 065628/0019 →
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVAL OF US PATENTS 9356603, 10026651, 10626048 AND INCLUSION OF US PATENT 7167871 PREVIOUSLY RECORDED ON REEL 064038 FRAME 0001. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 28, 2023
From: PALO ALTO RESEARCH CENTER INCORPORATED
To: XEROX CORPORATION
Reel/Frame 064161/0001 →
SECURITY INTEREST Recorded Jun 22, 2023
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 064760/0389 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 20, 2023
From: PALO ALTO RESEARCH CENTER INCORPORATED
To: XEROX CORPORATION
Reel/Frame 064038/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 21, 2017
From: DESAI, DIVYARAJ; RIVEST, JESSICA LOUIS BAKER
To: PALO ALTO RESEARCH CENTER INCORPORATED
Reel/Frame 043341/0738 →
Continuity (1)
Related Publication 20190055173A1 · Feb 21, 2019
Cited By (2)
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