IP Library Granted Patent US 10,882,876
Granted Patent B2
US 10,882,876 · App. 16/459,776 · Granted Jan 5, 2021

Pegylated imidazoquinolines as TLR7 and TLR8 agonists

Inventors: Helene G. Bazin-Lee (Hamilton, MT); David A. Johnson (Hamilton, MT)
Assignee: GLAXOSMITHKLINE BIOLOGICALS SA
C07F9/6561A61P17/12A61P31/14A61P31/20A61P35/00
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Quick Facts
Patent No.
US 10,882,876
App. No.
16/459,776
Granted
Jan 5, 2021
Kind
B2
Abstract

The present invention provides novel phospholipidated imidazoquinolines as TLR7 and TLR8 agonists, pharmaceutical compositions, therapeutic uses and processes for preparing the same.

Claims (19)

1. A compound, or a pharmaceutically acceptable salt thereof, of formula (I):

wherein

R 1 is selected from H, C 1-6 alkyl, C 1-6 alkylamino, C 1-6 alkoxy, C 3-6 cycloalkylC 1-6 alkyl, C 3-6 cycloalkylC 1-6 alkylamino, C 3-6 cycloalkylC 1-6 alkoxy, C 1-6 alkoxyC 1-6 alkyl, C 1-6 alkoxyC 1-6 alkylamino and C 1-6 alkoxyC 1-6 alkoxy; wherein the C 1-6 alkyl, C 1-6 alkylamino, C 1-6 alkoxy, C 3-6 cycloalkylC 1-6 alkyl, C 3-6 cycloalkylC 1-6 alkylamino, C 3-6 cycloalkylC 1-6 alkoxy, C 1-6 alkoxyC 1-6 alkyl, C 1-6 alkoxyC 1-6 alkylamino or C 1-6 alkoxyC 1-6 alkoxy is branched or unbranched and optionally terminally substituted with a hydroxyl, amino, thio, hydrazino, hydrazido, azido, acetylenyl, carboxyl, or maleimido group;

Z is selected from C 2 -C 6 alkyl and C 2 -C 6 alkenyl, wherein the C 2 -C 6 alkyl or C 2 -C 6 alkenyl is unsubstituted or terminally substituted by —(O—C 2 -C 6 alkyl) 1-6 -;

X is O or S;

n is 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19 or 20;

R 2 is H or a straight or branched, optionally unsaturated, C 4 -C 24 alkyl, or a straight or branched, optionally unsaturated, C 4 -C 24 , acyl;

R 3 is a straight or branched, optionally unsaturated, C 4 -C 24 alkyl or a straight or branched, optionally unsaturated, C 4 -C 24 acyl.

2. The compound or pharmaceutically acceptable salt according to claim 1 wherein R 1 is selected from H, C 1-6 alkyl, C 1-6 alkylamino and C 1-6 alkoxy wherein the C 1-6 alkyl, C 1-6 alkylamino or C 1-6 alkoxy is branched or unbranched and optionally terminally substituted with a hydroxyl, amino, thio, hydrazino, hydrazido, azido, acetylenyl, carboxyl, or maleimido group.

3. The compound or pharmaceutically acceptable salt according to claim 1 wherein R 1 is n-butyl.

4. The compound or pharmaceutically acceptable salt of claim 1 wherein Z is (CH 2 ) 2 .

5. The compound or pharmaceutically acceptable salt of claim 1 wherein X is O.

6. The compound or pharmaceutically acceptable salt of claim 1 wherein n is selected from 3 or 6.

7. The compound or pharmaceutically acceptable salt of claim 1 wherein R 2 is a straight or branched, optionally unsaturated, C 4 -C 24 acyl.

8. The compound or pharmaceutically acceptable salt of claim 1 wherein R 3 is a straight or branched, optionally unsaturated, C 4 -C 24 acyl.

9. The compound or pharmaceutically acceptable salt of claim 1 wherein R 2 is unbranched C 16 acyl (palmitoyl, COC 15 H 31 ).

10. The compound or pharmaceutically acceptable salt of claim 1 wherein R 3 is unbranched C 16 acyl (palmitoyl, COC 15 H 31 ).

11. The compound of claim 1 wherein R 1 =n-butyl; Z is (CH 2 ) 2 ; n is selected from 3, 6 and 9; R 2 is unbranched C 16 acyl (palmitoyl, COC 15 H 31 ) and R 3 is unbranched C 16 acyl (palmitoyl, COC 15 H 31 ).

12. A pharmaceutical composition comprising a compound according to claim 1 and a pharmaceutically acceptable carrier or diluent.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 2, 2019
From: BAZIN-LEE, HELENE G.; JOHNSON, DAVID A.
To: GLAXOSMITHKLINE BIOLOGICALS S.A.
Reel/Frame 049651/0513 →
Continuity (3)
Division 15781905
Provisional Application 62266880 · Dec 14, 2015
Related Publication 20190375772A1 · Dec 12, 2019