IP Library › Granted Patent US 10,976,283
Granted Patent B2
US 10,976,283 · App. 16/672,690 · Granted Apr 13, 2021

Method and apparatus for spatial compression and increased mobility resolution of ions

Inventors: Yehia M. Ibrahim (Richland, WA); Sandilya Garimella (Richland, WA); Richard D. Smith (Richland, WA)
Assignee: Battelle Memorial Institute
G01N27/622H01J49/022
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Quick Facts
Patent No.
US 10,976,283
App. No.
16/672,690
Granted
Apr 13, 2021
Kind
B2
Abstract

Methods and apparatuses for ion peak compression and increasing resolution of ions are disclosed. Packets of ions are introduced into a device. A first electric field is applied for dispersing the ion packets temporally or spatially according to their mobilities. A second intermittent traveling wave is applied for regrouping or merging the dispersed ion packets into a lesser number of trapping regions with narrower peaks. The ions packets are compressed into the narrower peak regions by varying a duty cycle of the intermittent traveling wave.

Claims (31)

1. An apparatus for ion peak compression comprising:

a first region configured to receive an ion packet comprising a plurality of ions and to separate the plurality of ions into one or more first region ion sub-packets having respective peak widths;

a second region separate from the first region, the second region configured to:

receive a first ion sub-packet of the one or more first region ion sub-packets, and

generate an electric field waveform traveling along a first direction of propagation that is configured to drive the received first ion sub-packet along the first direction of propagation and generate a first compressed ion sub-packet from the first ion sub-packet;

wherein the first compressed ion sub-packet has a narrower peak width than the first ion sub-packet.

2. The apparatus of claim 1 , wherein the electric field waveform has a period that changes from a first period in a first sub-region of the second region to a second period in a second sub-region of the second region.

3. The apparatus of claim 2 , wherein change in the period from the first period to the second period is configured to compress ion sub-packets within the second sub-region.

4. The apparatus of claim 2 , wherein the second region is further configured to receive a second ion sub-packet of the one or more first region ion sub-packets wherein the second ion sub-packet comprises a second portion of the plurality of ions of the ion packet, and merge the second ion sub-packet into the first compressed ion sub-packet.

5. The apparatus of claim 4 , wherein the first ion sub-packet has a first temporal duration, the second ion sub-packet has a second temporal duration and the compressed ion sub-packet has a third temporal duration.

6. The apparatus of claim 5 , wherein the third temporal duration is smaller than the first temporal duration.

7. The apparatus of claim 4 , wherein the first ion sub-packet has a first spatial pulse length, the second ion sub-packet has a second spatial pulse length and the first compressed ion sub-packet has a third spatial pulse length.

8. The apparatus of claim 7 , wherein the third spatial pulse length is smaller than the first spatial pulse length.

9. The apparatus of claim 2 , wherein the electric field waveform changes from the first period to the second period at an interface between the first sub-region and second sub-region.

10. The apparatus of claim 1 , wherein a second direction of propagation of the ion packet in the first region is orthogonal to the first direction of propagation of the received first ion sub-packet in the second region.

11. The apparatus of claim 1 , wherein a second direction of propagation of the ion packet in the first region is parallel to the first direction of propagation of the received first ion sub-packet in the second region.

12. The apparatus of claim 1 , wherein a second direction of propagation of the ion packet in the first region and the first direction of propagation of the received first ion sub-packet in the second region are aligned at an angle ranging from about 0 degrees to about 359 degrees.

13. A method for ion peak compression comprising:

receiving, by a first region of an ion manipulation apparatus, an ion packet comprising a plurality of ions;

generating, in the first region, an electric field waveform configured to separate the plurality of ions into one or more first region ion sub-packets having respective peak widths;

receiving, by a second region of the ion manipulation apparatus, a first ion sub-packet of the one or more first region ion sub-packets, wherein the second region is separate from the first region; and

generating, in the second region, an electric field waveform traveling along a first direction of propagation, the electric field waveform configured to drive the received first ion sub-packet along the first direction of propagation and generate a first compressed ion sub-packet from the first ion sub-packet; wherein the first compressed ion sub-packet has a narrower peak width than the first ion sub-packet.

14. The method of claim 13 , wherein the electric field waveform changes from a first period in a first sub-region of the second region to a second period in a second sub-region of the second period.

15. The method of claim 14 , wherein change in the period from the first period to the second period is configured to generate the first compressed ion sub-packet in the second sub-region from the first ion sub-packet in the first sub-region.

16. The method of claim 14 , further comprising:

receiving, by the second region, a second ion sub-packet of the one or more first region ion sub-packets wherein the second ion sub-packet includes a second portion of the plurality of ions of the ion packet, and

merging the second ion sub-packet into the first compressed ion sub-packet.

17. The method of claim 16 , wherein the first ion sub-packet has a first temporal duration, the second ion sub-packet has a second temporal duration and the first compressed ion sub-packet has a third temporal duration.

18. The method of claim 16 , wherein the first ion sub-packet has a first spatial pulse length, the second ion sub-packet has a second spatial pulse length and the first compressed ion sub-packet has a third spatial pulse length.

19. The method of claim 13 , wherein a second direction of propagation of the ion packet in the first region is orthogonal to the first direction of propagation of the received first ion sub-packet in the second region.

20. The method of claim 13 , wherein a second direction of propagation of the ion packet in the first region is parallel to the first direction of propagation of the received first ion sub-packet in the second region.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 4, 2019
From: IBRAHIM, YEHIA M.; GARIMELLA, SANDILYA; SMITH, RICHARD D.
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 050902/0991 →
Continuity (3)
Continuation 16027092 · Jul 3, 2018
Continuation 15157217 · May 17, 2016
Related Publication 20200200708A1 · Jun 25, 2020
Cited By (5)
US 12,228,546 US 12,300,479 US 12,422,402 US 12,620,567 US 12,712,170