IP Library Granted Patent US 10,995,010
Granted Patent B1
US 10,995,010 · App. 16/913,336 · Granted May 4, 2021

Synthesis of copper oxide nanoparticles

Inventors: Ali Aldalbahi (Riyadh, SA); Raneem Aldawish (Riyadh, SA); Manal Ahmed Gasmelseed Awad (Riyadh, SA); Noura Saleem Aldosari (Riyadh, SA); Reem Hamad Alshathri (Riyadh, SA); Leen Abdullah Aldwihi (Riyadh, SA); Raghad Alammari (Riyadh, SA); Khloud Ibrahim Bin Shoqiran (Riyadh, SA)
Assignee: KING SAUD UNIVERSITY
C01G3/02A01N59/20B01J23/72B01J35/004B01J35/023B82Y30/00B82Y40/00C01P2004/64
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Quick Facts
Patent No.
US 10,995,010
App. No.
16/913,336
Granted
May 4, 2021
Kind
B1
Abstract

A method of synthesizing copper oxide nanoparticles includes preparing a liquid extract of Rumex vesicarius , dissolving copper salt in the liquid extract to provide a solution with copper nanoparticles, adding a base to the solution with copper nanoparticles to form a precipitate including copper oxide nanoparticles. Copper oxide nanoparticles prepared according to the method are effective photocatalysts for degrading organic dyes and antibacterial agents and exhibit anticancer activities.

Claims (15)

1. A method of synthesizing metal oxide nanoparticles, comprising the steps of:

a) adding boiled water to Rumex vesicarius material to produce a liquid extract;

b) filtering the liquid extract to produce a filtered liquid extract;

c) dissolving a metal salt in the filtered liquid extract to produce a solution with metal nanoparticles;

d) adding a base to the solution with metal nanoparticles to form a precipitate;

e) removing liquid from the precipitate to provide a pellet;

f) drying the pellet, to produce a powder including metal oxide nanoparticles.

2. The method of claim 1 , further comprising heating the metal salt in the filtered liquid extract to about 80° C.

3. The method of claim 1 , wherein the base is sodium hydroxide.

4. The method of claim 1 , wherein the metal is copper and the metal salt is copper acetate.

5. The method of claim 1 , wherein the Rumex vesicarius material is dried Rumex vesicarius leaves.

6. The method of claim 1 , wherein the base is added dropwise with constant stirring.

7. The method of claim 1 , wherein the pellet is dried at about 60° C. for a period of time ranging from about two to six hours.

8. The method of claim 1 , further comprising a step of calcining the dried pellet.

9. The method of claim 8 , wherein the step of calcining is performed at a temperature ranging from about 300° C. to about 500° C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 26, 2020
From: ALDALBAHI, ALI; ALDAWISH, RANEEM; AWAD, MANAL AHMED GASMELSEED; ALDOSARI, NOURA SALEEM; ALSHATHRI, REEM HAMAD; ALDWIHI, LEEN ABDULLAH; ALAMMARI, RAGHAD; SHOQIRAN, KHLOUD IBRAHIM BIN
To: KING SAUD UNIVERSITY
Reel/Frame 053053/0026 →
Cited By (2)
US 12,220,492 US 12,246,099