IP Library › Granted Patent US 11,001,606
Granted Patent B2
US 11,001,606 · App. 16/118,425 · Granted May 11, 2021

Compositions and methods for fractal assembly of micron-scale nucleic acid structures

Inventors: Grigory Tikhomirov (Pasadena, CA); Philip F. Petersen (Covina, CA); Lulu Qian (La Crescenta, CA)
Assignee: CALIFORNIA INSTITUTE OF TECHNOLOGY
C07H21/04B81B1/006B81C1/00007B82B3/0047
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Quick Facts
Patent No.
US 11,001,606
App. No.
16/118,425
Granted
May 11, 2021
Kind
B2
Abstract

Compositions and methods of the present disclosure provide for staged assembly of nucleic acid microstructures made of an array of x number of polynucleotide tiles, where each of the polynucleotide tiles is a polygon configuration and is made from a single-stranded helical polynucleotide scaffold and a plurality of single-stranded polynucleotide staple strands of y number of unique staple sequences corresponding to the selected tile configuration, the y number of unique staple sequences capable of being constant for any value of x.

Claims (11)

1. A nucleic acid microstructure comprising:

an n×n array of n 2 polynucleotide square tiles, each of the n 2 polynucleotide square tiles comprising:

a single-stranded helical polynucleotide scaffold of a known sequence; and

a plurality of selected single-stranded polynucleotide staple strands being at least partially complementary to the polynucleotide scaffold and annealed to the polynucleotide scaffold to form a square tile shape;

the n×n array of n 2 polynucleotide square tiles further comprising a plurality of 2×2 sub-arrays, each of the plurality of 2×2 sub-arrays comprising a set of four polynucleotide square tiles, each of the four polynucleotide square tiles having p number of inside single-tile extended polynucleotide staple strands or p number of inside single-tile truncated polynucleotide staple strands, the inside single tile extended polynucleotide staple strands being annealed with the inside single-tile truncated polynucleotide staple strands to form the plurality of 2×2 sub-arrays, wherein each of the plurality of 2×2 subarrays comprise four two-tile edges and any inside two-tile edges in any of the plurality of 2×2 sub-arrays have less than p number of inside two-tile extended polynucleotide staple strands or less than p number of inside two-tile truncated polynucleotide staple strands, where the inside two-tile extended polynucleotide staple strands are annealed with the inside two-tile truncated polynucleotide staple strands to form at least one 4×4 subarray.

2. The nucleic acid microstructure of claim 1 , wherein n is 2, 4, or 8.

3. The nucleic acid microstructure of claim 1 , wherein the single-stranded helical polynucleotide scaffold is derived from M13mp18 DNA.

4. A method of assembling the nucleic acid microstructure of claim 1 , the method comprising:

selecting a value for n in the n by n array of n 2 polynucleotide square tiles;

determining a number of subarray annealing stages as log 2 n; and

preparing n 2 mixtures for each of the n 2 polynucleotide square tiles, each mixture comprising the single-stranded helical polynucleotide scaffold and corresponding single-stranded polynucleotide staple strands specific to each of the n 2 polynucleotide square tiles out of the plurality of selected single-stranded polynucleotide staple strands.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2018
From: TIKHOMIROV, GRIGORY; PETERSEN, PHILIP F.; QIAN, LULU
To: CALIFORNIA INSTITUTE OF TECHNOLOGY
Reel/Frame 047647/0289 →
Continuity (2)
Provisional Application 62551925 · Aug 30, 2017
Related Publication 20190062366A1 · Feb 28, 2019
Cited By (5)
US 12,305,167 US 12,503,694 US 12,612,656 US 12,742,167 US 12,742,168