IP Library Granted Patent US 11,008,265
Granted Patent B2
US 11,008,265 · App. 16/538,012 · Granted May 18, 2021

Reactors and systems for oxidative coupling of methane

Inventors: Humera A. Rafique (Dublin, CA); Srinivas Vuddagiri (Davis, CA); Guido Radaelli (South San Francisco, CA); Jarod McCormick (San Carlos, CA); Suchia Duggal (San Rafael, CA); Joel Cizeron (Redwood City, CA)
Assignee: Lummus Technology LLC
C07C2/78B01J4/004B01J8/001B01J8/025B01J8/0214B01J8/0278B01J8/0285B01J8/0457B01J8/0492B01J8/0496B01J19/0026B01J23/462B01J23/745B01J23/75B01J23/755B01J35/0013B01J35/026B01J37/009B01J37/0018B01J37/03B01J37/04B01J37/088C07C2/84C07C5/09C10G50/00C10G69/126B01J23/06B01J23/882B01J2208/0092B01J2208/00176B01J2208/00849B01J2208/00902B01J2208/00929B01J2208/00938B01J2208/02B01J2219/0004B01J2219/00006B01J2219/00038C10G2400/02
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Quick Facts
Patent No.
US 11,008,265
App. No.
16/538,012
Granted
May 18, 2021
Kind
B2
Abstract

In an aspect, the present disclosure provides a method for the oxidative coupling of methane to generate hydrocarbon compounds containing at least two carbon atoms (C 2+ compounds). The method can include mixing a first gas stream comprising methane with a second gas stream comprising oxygen to form a third gas stream comprising methane and oxygen and performing an oxidative coupling of methane (OCM) reaction using the third gas stream to produce a product stream comprising one or more C 2+ compounds.

Claims (30)

1. A method for producing hydrocarbon compounds including two or more carbon atoms (C 2+ compounds), the method comprising:

(a) performing an oxidative coupling of methane (OCM) reaction in an OCM reactor to produce an OCM effluent comprising carbon dioxide (CO 2 ), hydrogen (H 2 ), one or more C 2+ compounds, and methane (CH 4 );

(b) separating the OCM effluent into (i) a first stream comprising at least some of the one or more C 2+ compounds and (ii) a second stream comprising carbon monoxide (CO), CO 2 , H 2 , and CH 4 ;

(c) methanating the second stream to produce a first OCM reactor feed comprising CH 4 formed from the H 2 and CO and/or CO 2 in the second stream;

(d) methanating a third stream comprising CH 4 and H 2 to produce a second OCM reactor feed comprising CH 4 , which third stream is from an ethylene cracker; and

(e) directing the first and second OCM reactor feeds to the OCM reactor.

2. The method of claim 1 , wherein the second stream and the third stream are methanated in a single methanation reactor.

3. The method of claim 1 , further comprising providing at least a portion of the first stream to the ethylene cracker.

4. The method of claim 3 , wherein the at least the portion of the first stream is provided to a gas compressor or a fractionation unit of the ethylene cracker.

5. The method of claim 1 , wherein the third stream is the overhead stream of a demethanizer unit of the ethylene cracker.

6. The method of claim 1 , wherein the separating in (b) is performed at least in part in a pressure swing adsorption (PSA) unit.

7. The method of claim 1 , wherein the separating in (b) is performed at least in part with a CO 2 removal system or a process gas dryer.

8. The method of claim 1 , wherein the OCM effluent is compressed prior to (b).

9. The method of claim 1 , further comprising feeding oxygen (O 2 ) as an oxidizing agent to the OCM reactor, which O 2 takes part in the OCM reaction.

10. The method of claim 1 , wherein the OCM effluent comprises carbon monoxide (CO) that is converted into CH 4 in (c).

11. The method of claim 1 , wherein the OCM reaction further reacts CH 4 from natural gas to achieve additional ethylene production.

12. An oxidative coupling of methane (OCM) system for production of hydrocarbon compounds including two or more carbon atoms (C 2+ compounds), comprising:

(a) an OCM subsystem that (i) takes as input a feed stream comprising methane (CH 4 ) and an oxidizing agent, and (ii) generates a product stream comprising C 2+ compounds from the CH 4 and the oxidizing agent;

(b) a separation subsystem fluidically coupled to the OCM subsystem that separates the product stream into (i) a first stream comprising C 2+ compounds and (ii) a second stream comprising hydrogen (H 2 ) and carbon dioxide (CO 2 ) and/or carbon monoxide (CO);

(c) a methanation subsystem fluidically coupled to the second stream and to the OCM subsystem, wherein the methanation subsystem converts H 2 and CO 2 and/or CO into CH 4 ; and

(d) an ethylene cracker subsystem fluidically coupled to the methanation subsystem that provides CH 4 , H 2 , CO 2 , and/or CO to the methanation subsystem.

13. The system of claim 12 , wherein the methanation subsystem provides CH 4 to the OCM subsystem.

14. The system of claim 12 , wherein the ethylene cracker subsystem comprises a demathanizer that provides CH 4 , H 2 , CO 2 , and/or CO to the methanation subsystem.

15. The system of claim 12 , wherein the first stream is fluidically coupled to the ethylene cracker subsystem, and the ethylene cracker subsystem is configured to fractionate the first stream.

16. The system of claim 12 , wherein the separation subsystem comprises a pressure swing adsorption (PSA) unit.

17. The system of claim 12 , wherein the OCM subsystem reacts CH 4 from natural gas with the oxidizing agent in an OCM reaction.

18. The system of claim 12 , wherein the oxidizing agent comprises O 2 .

19. The system of claim 18 , wherein the O 2 is generated from air.

20. The system of claim 12 , wherein the OCM subsystem comprises at least one OCM reactor.

21. The system of claim 20 , wherein the OCM subsystem comprises at least one post-bed cracking unit within the at least one OCM reactor or downstream of the at least one OCM reactor, which post-bed cracking unit is configured to convert at least a portion of alkanes in the product stream to alkenes.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 2, 2020
From: SILURIA TECHNOLOGIES, INC.
To: SILURIA (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
Reel/Frame 053673/0607 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNOR'S NAME PREVIOUSLY RECORDED ON REEL 050161 FRAME 0416. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 2, 2020
From: SILURIA (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
To: LUMMUS TECHNOLOGY LLC
Reel/Frame 053675/0520 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2019
From: SILURIA TECHNOLOGIES, INC.
To: LUMMUS TECHNOLOGY LLC
Reel/Frame 050161/0416 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2019
From: RAFIQUE, HUMERA A.; VUDDAGIRI, SRINIVAS; RADAELLI, GUIDO; MCCORMICK, JAROD; DUGGAL, SUCHIA; CIZERON, JOEL
To: SILURIA TECHNOLOGIES, INC.
Reel/Frame 050157/0385 →
Continuity (11)
Continuation 16021441 · Jun 28, 2018
Continuation In Part 15076402 · Mar 21, 2016
Continuation 14789946 · Jul 1, 2015
Continuation 14592668 · Jan 8, 2015
Provisional Application 62086650 · Dec 2, 2014
Provisional Application 62073478 · Oct 31, 2014
Provisional Application 62050720 · Sep 15, 2014
Provisional Application 61996789 · May 14, 2014
Provisional Application 61955112 · Mar 18, 2014
Provisional Application 61925627 · Jan 9, 2014
Related Publication 20200207684A1 · Jul 2, 2020
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