IP Library Granted Patent US 11,008,643
Granted Patent B2
US 11,008,643 · App. 15/205,217 · Granted May 18, 2021

Tunable anisotropy of co-based nanocomposites for magnetic field sensing and inductor applications

Inventors: Alex M. Leary (Pittsburgh, PA); Paul R. Ohodnicki (Pittsburgh, PA); Michael E. McHenry (Pittsburgh, PA); Vladimir Keylin (Pittsburgh, PA); Kevin Byerly (Pittsburgh, PA)
Assignee: Carnegie Mellon University
C22F1/10B82Y30/00B82Y40/00C22C19/07G01R33/1223H01F1/15333H01F41/0226G01R33/0052
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Quick Facts
Patent No.
US 11,008,643
App. No.
15/205,217
Granted
May 18, 2021
Kind
B2
Abstract

A method includes producing an amorphous precursor to a nanocomposite, performing devitrification of the amorphous precursor, forming, based on the devitrification, the nanocomposite comprising an induced magnetic anisotropy, and for a first portion of the nanocomposite, determining a desired value of a magnetic permeability of the first portion, tuning, based on the desired value, the induced magnetic anisotropy for the first portion, and adjusting, based on the tuning of the induced magnetic anisotropy of the first portion, a first magnetic permeability value of the first portion of the nanocomposite, wherein the first magnetic permeability value is different from a second magnetic permeability value for a second portion of the nanocomposite.

Claims (49)

1. A method comprising:

producing an amorphous precursor to a nanocomposite;

performing devitrification of the amorphous precursor;

forming, based on the devitrification, the nanocomposite comprising an induced magnetic anisotropy; and

for a first portion of the nanocomposite,

determining a desired value of a magnetic permeability of the first portion;

tuning, based on the desired value, the induced magnetic anisotropy for the first portion; and

adjusting, based on the tuning of the induced magnetic anisotropy of the first portion, a first magnetic permeability value of the first portion of the nanocomposite, wherein the first magnetic permeability value is different from a second magnetic permeability value for a second portion of the nanocomposite;

wherein the crystalline grains each comprise a close-packed crystal structure comprising a plurality of aligned faults in the close-packed crystal structure, with each of the faults aligned in a plane of the crystal structure, wherein the plurality of aligned faults in the close-packed crystal structure is configured to cause the induced magnetic anisotropy.

2. The method of claim 1 , further comprising:

annealing the first portion of the nanocomposite, the annealing comprising heating the first portion of the nanocomposite to a predetermined temperature;

modifying the first portion of the nanocomposite to a predetermined geometric configuration, the modifying comprising applying a magnitude of stress to the first portion; and

adjusting the predetermined temperature, the predetermined geometric configuration, or the magnitude of stress applied to the first portion based on the desired value of the magnetic permeability.

3. The method of claim 2 , further comprising:

based on the annealing, controlling a nano-crystallization process for the nanocomposite in one or more geometries.

4. The method of claim 1 , further comprising:

tuning the induced magnetic anisotropy of the first portion by varying one or more of a temperature of one or more heated thermal blocks configured to contact the first portion of the nanocomposite during the tuning and an exposure time of the first portion to the one or more heated thermal blocks.

5. The method of claim 4 , wherein the exposure time of the first portion to the one or more heated thermal blocks is varied by adjusting a length of the one or more heated thermal blocks or a speed of the first portion moving between at least two of the one or more heated thermal blocks.

6. The method of claim 1 , wherein the nanocomposite comprises a tape wound core, the method further comprising:

based on the tuning, producing one or more of (i) a square loop core, and (ii) a balanced flux distribution in the nanocomposite during a single winding of the tape-wound core.

7. The method of claim 1 , further comprising:

tuning the magnetic anisotropy of the first portion by varying one or more of a direction of a stress applied to the first portion and a direction of a magnetic field applied to the first portion.

8. The method of claim 1 , further comprising:

adjusting the first magnetic permeability value to be less than the second magnetic permeability value when the first portion comprises one or more of a bend in the nanocomposite, a pole face of the nanocomposite, and a radius of the nanocomposite.

9. The method of claim 1 , wherein the adjusting of the first magnetic permeability value reduces a flux concentration in the nanocomposite relative to a flux concentration in the nanocomposite independent of adjusting, reduces a stray field magnitude in the nanocomposite with the adjusted magnetic anisotropy relative to a stray field magnitude in the nanocomposite independent of adjusting, or reduces an imbalance of a flux distribution in the nanocomposite between the first portion and the second portion relative to a flux distribution imbalance in the nanocomposite independent of adjusting.

10. The method of claim 1 , further comprising:

forming the nanocomposite to a ribbon geometry with a thickness of 10-35 microns.

11. The method of claim 1 , further comprising

forming the first portion and second portions each to a planar geometry.

12. The method of claim 1 , wherein the nanocomposite comprises 30 atomic % or less of one of Iron (Fe) or Nickel (Ni) and 50 atomic % or less of metals selected from the group comprising boron (B), carbon (C), phosphorous (P), silicon (Si), chromium (Cr), tantalum (Ta), niobium (Nb), vanadium (V), aluminum (Al), molybdenum (Mo), manganese (Mn), tungsten (W), cobalt (Co) and zirconium (Zr).

13. The method of claim 1 , wherein the first magnetic permeability value is adjusted to be less than 50.

14. The method of claim 1 , wherein the nanocomposite comprises a composite structure with crystalline grains less than approximately 50 nanometers in average diameter embedded within an amorphous matrix.

15. The method of claim 1 , further comprising forming a tape-wound core from the nanocomposite having a diameter size of greater than 6 inches.

16. A method comprising:

producing an amorphous precursor to a nanocomposite;

performing devitrification of the amorphous precursor;

forming, based on the devitrification, the nanocomposite comprising an induced magnetic anisotropy;

for a first portion of the nanocomposite,

determining a desired value of a magnetic permeability of the first portion;

applying a stress to the first portion of the nanocomposite;

tuning, based on the desired value, the induced magnetic anisotropy for the first portion based on a value of the stress applied; and

adjusting, based on the tuning of the induced magnetic anisotropy of the first portion, a first magnetic permeability value of the first portion of the nanocomposite, wherein the first magnetic permeability value is different from a second magnetic permeability value for a second portion of the nanocomposite;

wherein the first magnetic permeability value is adjusted to be less than 90 based on the value of the stress applied being less than 400 Megapascals (MPa).

17. The method of claim 16 , wherein the first magnetic permeability value is adjusted to be a value in the range of 80-89.

18. The method of claim 16 , wherein the first magnetic permeability value is adjusted to be a value in the range of 70-79.

19. The method of claim 16 , wherein the first magnetic permeability value is adjusted to be a value in the range of 60-69.

20. The method of claim 16 , wherein the first magnetic permeability value is adjusted to be a value in the range of 50-59.

21. The method of claim 16 , wherein the value of the stress applied is less than 100 MPa.

22. The method of claim 16 , wherein a response of the nanocomposite is greater than 20 (J/m 3 )/MPa.

Assignments (3)
CONFIRMATORY LICENSE Recorded Sep 10, 2020
From: CARNEGIE-MELON UNIVERSITY
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 053737/0777 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2018
From: OHODNICKI, PAUL R.
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 046100/0335 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2016
From: KEYLIN, VLADIMIR; MCHENRY, MICHAEL E.; LEARY, ALEX M.
To: CARNEGIE MELLON UNIVERSITY
Reel/Frame 039165/0919 →
Continuity (4)
Continuation In Part 14278836 · May 15, 2014
Provisional Application 62231536 · Jul 9, 2015
Provisional Application 61855439 · May 15, 2013
Related Publication 20160319412A1 · Nov 3, 2016
Cited By (1)
US 12,349,262