Apparatus and method for detecting moisture in a vacuum chamber
A method of sterilizing medical instruments using a vacuum chamber connected to reservoir by a valve in a closed state is disclosed that includes placing instruments in a non-sterile state into a sterilization pack, opening a chamber, placing the pack into the chamber, closing the chamber, withdrawing a first volume of air from the chamber, changing a volume of liquid water into vapor, opening the valve, introducing sterilant into the chamber, introducing a second volume of air into the chamber, opening the chamber, removing the pack from the chamber, and removing the instruments in a sterile-state from the pack. The process may further include the steps of repeatedly determining pressure within the chamber, calculating second-derivative values of pressure with respect to time, and determining whether any local maxima exist in a plot of second derivative values that correspond to pressures above and/or below the triple-point pressure of water.
1. A method of operating a sterilization system having a chamber for sterilizing instruments, comprising:
repeatedly determining pressure within the chamber while withdrawing a first volume of air from the chamber;
calculating second-derivative values of pressure with respect to time;
calculating a summation of positive differences between consecutive second derivative values;
comparing the summation to a threshold value;
determining that the summation is greater than the threshold value; and
in response to determining that the summation is greater than the threshold value, increasing the pressure in the chamber.
2. The method of claim 1 , in which the step of calculating the summation of positive differences is performed for consecutive second derivative values corresponding to a pressure range.
3. The method of claim 2 , in which the pressure range comprises between about 4.6 torr and about 0.3 torr.
4. The method of claim 1 , in which the step of increasing the pressure in the chamber includes introducing a second volume of air into the chamber.
5. The method of claim 4 , further comprising vaporizing a volume of water disposed on an instrument in the chamber with the second volume of air.
6. The method of claim 5 , in which the threshold value is a first threshold value, the summation is a first summation, and the pressure range is a first pressure range.
7. The method of claim 6 further comprising, after repeating the step of increasing the pressure in the chamber:
repeatedly determining pressure within the chamber while withdrawing a third volume of air from the chamber;
calculating second-derivative values of pressure with respect to time corresponding to withdrawing the third volume of air from the chamber;
calculating a second summation of positive differences between consecutive second derivative values;
comparing the second summation to a second threshold value;
determining that the second summation is less than the second threshold value; and
in response to determining that the second summation is less than the second threshold value, introducing a sterilant into the chamber.
8. The method of claim 7 , in which the step of calculating the second summation of positive differences is performed for consecutive second derivative values corresponding to a second pressure range.
9. The method of claim 8 , in which the second pressure range comprises between about 4.6 torr and about 0.3 torr.
10. A method of operating a sterilization system having a chamber for sterilizing instruments, comprising:
repeatedly determining pressure within the chamber while withdrawing a volume of air from the chamber;
calculating second-derivative values of pressure with respect to time;
calculating a summation of positive differences between consecutive second derivative values;
comparing the summation to a threshold value;
determining that the summation is less than the threshold value; and
in response to determining that the summation is less than the threshold value, introducing a sterilant into the chamber.
11. The method of claim 10 , in which the step of calculating the summation of positive differences is performed for consecutive second derivative values corresponding to a pressure range.
12. The method of claim 11 , in which the pressure range comprises between about 4.6 torr and about 0.3 torr.