IP Library Granted Patent US 11,028,478
Granted Patent B2
US 11,028,478 · App. 16/006,010 · Granted Jun 8, 2021

Atomic layer deposition of films comprising silicon, carbon and nitrogen using halogenated silicon precursors

Inventors: Victor Nguyen (Novato, CA); Ning Li (San Jose, CA); Mihaela Balseanu (Sunnyvale, CA); Li-Qun Xia (Cupertino, CA); Mark Saly (Santa Clara, CA); David Thompson (San Jose, CA)
Assignee: Applied Materials, Inc.
C23C16/45553C23C16/345C23C16/36C23C16/4554C23C16/45536C23C16/45542
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Quick Facts
Patent No.
US 11,028,478
App. No.
16/006,010
Granted
Jun 8, 2021
Kind
B2
Abstract

Provided are methods for the deposition of films comprising SiCN. Certain methods involve exposing a substrate surface to a silicon precursor, wherein the silicon precursor is halogenated with Cl, Br or I, and the silicon precursor comprises a halogenated silane, a halogenated carbosilane, an halogenated aminosilane or a halogenated carbo-sillyl amine. Then, the substrate surface can be exposed to a nitrogen-containing plasma or a nitrogen precursor and densification plasma.

Claims (16)

1. A method of depositing a film comprising Si, C and N, the method comprising

exposing a substrate surface to a silicon precursor, wherein the silicon precursor comprises a halogenated bis(silyl) methane precursor selected from the group consisting of:

and

exposing the substrate to a nitrogen-containing plasma or a nitrogen precursor.

2. A method of depositing a film comprising Si, C and N, the method comprising:

exposing a substrate surface to a silicon precursor, wherein the silicon precursor is a halogenated bis(silyl) methane-based precursor is selected from the group consisting of

and

exposing the substrate to a nitrogen-containing plasma.

3. The method of claim 2 , wherein the nitrogen-containing plasma comprises ammonia, an amine or carbonitride.

4. A method of depositing a film comprising Si, C and N, the method comprising:

exposing a substrate surface to a silicon precursor, wherein the silicon precursor comprises a halogenated bis(silyl) methane precursor selected from the group consisting of:

exposing the substrate surface to a nitrogen precursor to provide a film; and

exposing the film to a densification plasma.

5. The method of claim 4 , wherein the nitrogen precursor comprises an alkyl amine.

6. The method of claim 4 , further comprising exposing the film comprising Si and N to a carbon source.

7. The method of claim 6 , wherein the carbon source comprises exposing the film to a compound with a C═C bond.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 22, 2019
From: NGUYEN, VICTOR; LI, NING; BALSEANU, MIHAELA; XIA, LI-QUN; SALY, MARK; THOMPSON, DAVID
To: APPLIED MATERIALS, INC.
Reel/Frame 049250/0759 →
Continuity (3)
Division 14533496 · Nov 5, 2014
Provisional Application 61907717 · Nov 22, 2013
Related Publication 20180291505A1 · Oct 11, 2018