IP Library Granted Patent US 11,033,659
Granted Patent B2
US 11,033,659 · App. 15/510,338 · Granted Jun 15, 2021

Nanofiber structures and methods of synthesis and use thereof

Inventors: Jingwei Xie (Omaha, NE); Jiang Jiang (Omaha, NE)
Assignee: BOARD OF REGENTS OF THE UNIVERSITY OF NEBRASKA
A61L27/56A61K9/0092A61K9/70A61L27/18A61L27/38D01D5/003D01D10/00A61L2400/12D10B2331/041D10B2401/10
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Quick Facts
Patent No.
US 11,033,659
App. No.
15/510,338
Granted
Jun 15, 2021
Kind
B2
Abstract

Three dimensional nanofiber structures are provided and methods of production thereof.

Claims (16)

1. A method for producing an expanded nanofibrous structure, the method comprising exposing a nanofiber structure comprising electrospun fibers to gas bubbles, thereby expanding the nanofiber structure,

wherein said nanofiber structure comprises a plurality of nanofibers.

2. The method of claim 1 , wherein said gas bubbles are generated as a product of a chemical reaction.

3. The method of claim 2 , wherein said chemical reaction is the hydrolysis of sodium borohydride.

4. The method of claim 2 , wherein said exposure comprises immersing said nanofiber structure in a liquid comprising the reagents for said chemical reaction.

5. The method of claim 1 , wherein said nanofiber structure comprises a plurality of uniaxially-aligned nanofibers, random nanofibers, and/or entangled nanofibers.

6. The method of claim 1 , further comprising preparing said nanofiber structure comprising a plurality of nanofibers prior to said exposure to bubbles.

7. The method of claim 1 , wherein said nanofiber structure comprises biodegradable fibers.

8. The method of claim 1 , wherein said nanofibers comprise hydrophobic polymers.

9. The method of claim 8 , wherein said hydrophobic polymer is poly(caprolactone).

10. The method of claim 1 , wherein said method further comprises washing the produced nanofibrous structure and removing gas bubbles trapped within said nanofibrous structure.

11. The method of claim 1 , wherein said method further comprises lyophilizing the produced nanofibrous structure.

12. The method of claim 1 , wherein said exposing of the nanofiber structure comprising electrospun fibers to gas bubbles increases the thickness of said nanofiber structure.

13. The method of claim 1 , wherein said nanofiber structure consists of a plurality of nanofibers, and wherein said nanofibers consist of a polymer.

14. The method of claim 13 , wherein said polymer is a hydrophobic polymer.

15. The method of claim 1 , wherein said nanofiber structure is a nanofiber mat prior to said exposure to gas bubbles.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 11, 2017
From: XIE, JINGWEI; JIANG, JIANG
To: BOARD OF REGENTS OF THE UNIVERSITY OF NEBRASKA
Reel/Frame 042216/0813 →
Continuity (2)
Provisional Application 62056899 · Sep 29, 2014
Related Publication 20170296703A1 · Oct 19, 2017
Cited By (2)
US 12,263,250 US 12,383,652