Method and apparatus for extracting plant oils using ethanol water
View Patent ↗The invention provides a method and apparatus for continuous extraction of plant oils from plant tissue using an advantageous azeotrope of ethanol and water and employing the differing solubility of plant oils in ethanol and water to drive formation of a non-toxic oil tincture.
1. A method of extracting oil from plant tissue comprising:
a. The step consisting of mixing ethanol and water in a ratio less than or equal to 95% ethanol in a boiling pot;
b. The step consisting of distilling 95% ethanol from said boiling pot;
c. The step consisting of commingling said 95% ethanol with an oil-bearing plant tissue in an extraction chamber;
d. The step consisting of collecting an oil-bearing ethanol in said boiling pot;
e. The step consisting of removing said oil-bearing ethanol from said boiling pot to a separator;
f. The step consisting of separating an oil from an aqueous phase by a separator that draws off an upper oil phase;
g. The step consisting of returning said separated aqueous phase to said boiling pot;
h. The step consisting of repeating steps a-g without stopping the extraction process.
2. The method of claim 1 further comprising the step of replenishing oil-bearing plant tissue in said extraction chamber by switching a distillate flow to a further extraction chamber.
3. The method of claim 2 further comprising the step of replenishing said boiling pot with ethanol and water.
4. The method of claim 3 further comprising the step of removing a debris from said boiling pot.
5. The method of claim 4 further comprising the step of removing said oil from said separator.
6. The method of claim 5 further comprising the step of chilling said 95% ethanol to a temperature not lower than −144° C. prior to reaching said extraction chamber.
7. The method of claim 6 further comprising the step of reducing the pressure within the system.