IP Library Granted Patent US 11,098,046
Granted Patent B2
US 11,098,046 · App. 16/760,790 · Granted Aug 24, 2021

Macrocyclic compounds as TRK kinase inhibitors and uses thereof

Inventors: Wen-Lian Wu (Green Brook, NJ); Zhiqiang Yang (Westfield, NJ); Francis Lee (Yardley, PA); John Qiang Tan (North Brunswick, NJ)
Assignee: ANGEX PHARMACEUTICAL, INC.
C07D471/22C07D487/22C07D498/22
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Quick Facts
Patent No.
US 11,098,046
App. No.
16/760,790
Granted
Aug 24, 2021
Kind
B2
Abstract

The present disclosure describes novel TRK kinase inhibitors and methods for preparing them. The pharmaceutical compositions comprising such TRK kinase inhibitors and methods of using them for treating cancer, infectious diseases, and other disorders are also described.

Claims (41)

1. A compound represented by a formula:

or a pharmaceutically acceptable salt thereof;

wherein

is

wherein the ring N atom is attached to Ring B:

(Ring A) is an optionally substituted pyridin-di-yl, which is substituted with 0, 1, 2, or 3 substituents and each substituent is independently R A , F, Cl, Br, I, CN, —OR A , CF 3 , —NO 2 , —NR A R B , —COR A , —CO 2 R A , —OCOR A , —OCONR A R B , —NR A COR B , or —CONR A R B ;

(Ring B) is an optionally substituted pyrazolo[1,5-a]pyrimidin-3,5-di-yl, which is substituted with 0, 1, 2, or 3 substituents and each substituent is independently R A , F, Cl, Br, I, CN, —OR A , CF 3 , —NO 2 , —NR A R B , —COR A , —CO 2 A , —OCOR A , —OCONR A R B , —NR A COR B , or —CONR A R B ;

L is —C(O)NR A , wherein the carbon atom is attached to Ring B;

E is C 1-3 alkylene having, as chemically appropriate, 0, 1, 2, 3, 4, 5, or 6 substituents, wherein the substituents of E are independently F, Cl, Br, I, OH, ═O, C 1-6 alkyl or C 1-6 cycloalkyl, wherein two of the substituents of E may connect together with the attached carbon atom of E to form a 3-membered saturated ring;

W is a covalent bond, O, NR A , CR A1 R B1 , CR A1 ═CR B1 , or C═CR A1 R B1 ;

R A1 and R B1 are independently H, F, Cl, Br, I, or C 1-6 hydrocarbyl;

R A and R B are independently H or C 1-6 hydrocarbyl;

R 1a and R 2a are independently H, OH, C 1-3 alkyl, F, Cl, or Br; and

R represents 0, 1, 2, 3, 4, or 5 substituents at any ring carbon atom of the pyrrolidine ring and each R is independently H, OH, C 1-3 alkyl, F, Cl, or Br.

2. The compound of claim 1 , wherein Ring A is optionally substituted pyridin-2,3-di-yl.

3. The compound of claim 1 , wherein Ring A is optionally substituted 5-fluoro-pyridin-2,3-di-yl.

4. The compound of claim 1 , wherein

is optionally substituted (pyridin-3-yl)2-oxy-yl.

5. The compound of claim 1 , wherein the compound is further represented by a formula:

or a pharmaceutically acceptable salt thereof, wherein R 1 , R 2 , R 3 , R 5 , R 6 , and R 7 are independently R A , F, Cl, Br, I, CN, —OR A , CF 3 , —NO 2 , —NR A R B , —COR A , —CO 2 R A , —OCOR A , —OCONR A R B , —NR A COR B , or —CONR A R B .

6. The compound of claim 5 , wherein R, R 1a , or R 2a is independently H or CH 3 .

7. The compound of claim 1 , wherein W is CH 2 .

8. The compound of claim 1 , wherein W is O.

9. The compound of claim 1 , wherein W is C═CH 2 .

10. The compound of claim 1 , wherein E is:

11. The compound of claim 1 , wherein E is:

12. The compound of claim 1 , wherein E is:

13. The compound of claim 1 , wherein E is:

14. The compound of claim 1 , wherein E-W is:

wherein the asterisk indicates the point of attachment of C atom to L.

15. The compound of claim 1 , wherein E-W is:

wherein the asterisk indicates the point of attachment of C atom to L.

16. The compound of claim 1 , wherein E-W is:

wherein the asterisk indicates the point of attachment of C atom to L.

17. The compound of claim 1 , wherein E-W is:

wherein the asterisk indicates the point of attachment of C atom to L.

18. The compound of claim 1 , wherein E-W is:

wherein the asterisk indicates the point of attachment of C atom to L.

19. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein the compound is an optionally substituted (1 3 E,1 4 E,2 1 R,2 2 R,2 5 S)-4-methylene-2 3 ,6-diaza-1(5,3)-pyrazolo[1,5-a]pyrimidina-3(3,2)-pyridina-2(3,2)-bicyclo[3.1.0]hexanacycloheptaphan-7-one, optionally substituted, (1 3 E,1 4 E,2 1 R,2 4 S,2 5 S)-4-methylene-2 3 ,6-diaza-1(5,3)-pyrazolo[1,5-a]pyrimidina-3(3,2)-pyridina-2(3,4)-bicyclo[3.1.0]hexanacycloheptaphan-7-one, optionally substituted, (1 3 E,1 4 E,2 1 R,2 2 R,2 5 S)-4-oxa-2 3 ,7-diaza-1(5,3)-pyrazolo[1,5-a]pyrimidina-3(3,2)-pyridina-2(3,2)-bicyclo[3.1.0]hexanacycloheptaphan-8-one, optionally substituted (1 3 E,1 4 E,2 1 R,2 4 S,2 5 S)-4-oxa-2 3 ,7-diaza-1(5,3)-pyrazolo[1,5-a]pyrimidina-3(3,2)-pyridina-2(3,4)-bicyclo[3.1.0]hexanacyclooctaphan-8-one, optionally substituted, (1 3 E,1 4 E,2 1 R,2 2 R,2 5 S)-2 3 ,7-diaza-1(5,3)-pyrazolo[1,5-a]pyrimidina-3(3,2)-pyridina-2(3,2)-bicyclo[3.1.0]hexanacycloheptaphan-8-one, or optionally substituted, (1 3 E,1 4 E,2 1 S,2 4 S,2 5 R)-2 6 ,2 6 -dimethyl-2 3 ,7-diaza-1(5,3)-pyrazolo[1,5-a]pyrimidina-3(3,2)-pyridina-2(3,4)-bicyclo[3.1.0]hexanacyclooctaphan-8-one.

20. The compound of claim 1 , or a pharmaceutically acceptable salt thereof, wherein the compound is:

21. A pharmaceutical composition comprising a compound of claim 1 or a pharmaceutically acceptable salt thereof, and at least one pharmaceutically acceptable carrier.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 6, 2020
From: WU, WEN-LIAN; YANG, ZHIQIANG; LEE, FRANCIS; TAN, JOHN QIANG
To: ANGEX PHARMACEUTICAL, INC.
Reel/Frame 052589/0145 →
Continuity (3)
Provisional Application 62677391 · May 29, 2018
Provisional Application 62584466 · Nov 10, 2017
Related Publication 20200385386A1 · Dec 10, 2020