IP Library › Granted Patent US 11,103,845
Granted Patent B2
US 11,103,845 · App. 16/463,232 · Granted Aug 31, 2021

Polysaccharide aerogel

Inventors: Hai Minh Duong (Singapore, SG); Nhan Phan-Thien (Singapore, SG); Bowen Gu (Singapore, SG); Mark Pyne Pennefather (Singapore, SG); Thanh Xuan Nguyen (Singapore, SG)
Assignee: National University of Singapore
B01J13/0091A61L15/225B01D17/0202C08B15/005C08J9/28C08K3/30C08L1/02C08L5/08A61L24/00B01D17/02C08J2201/026C08J2201/0484C08J2205/026C08J2301/02C08J2405/08C08K2003/3045
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Quick Facts
Patent No.
US 11,103,845
App. No.
16/463,232
Granted
Aug 31, 2021
Kind
B2
Abstract

Disclosed herein is a polysaccharide aerogel comprising cotton cellulose fibres and a method of preparing the polysaccharide aerogel. The method comprises: mixing cotton cellulose fibres and a cross-linker to form a mixture; sonicating the mixture; freezing the sonicated mixture; and freeze drying the frozen mixture to form an aerogel. A further embodiment provides a polysaccharide aerogel comprising cotton cellulose fibres and paper cellulose fibres in a weight ratio of 1:1 to 1:6 and a method of preparation thereof wherein in the mixing step, the paper cellulose fibres are added to the cotton cellulose fibres to form a mixture.

Claims (16)

1. A polysaccharide aerogel, comprising cotton cellulose fibres and paper cellulose fibres, wherein the cotton cellulose fibres and the paper cellulose fibres are comprised in the aerogel in a weight ratio of 1:1 to 1:6.

2. The aerogel of claim 1 , wherein the aerogel is compressible.

3. The aerogel of claim 1 , wherein the aerogel is formed from a hydrogel comprising 0.5-1.5 weight % cotton cellulose fibres.

4. The aerogel of claim 1 , wherein the aerogel further comprises at least one additive.

5. The aerogel of claim 4 , wherein the at least one additive comprises chitosan.

6. The aerogel of claim 1 , wherein the aerogel comprises at least one cross-linker.

7. The aerogel of claim 6 , wherein the at least one cross-linker comprises a wet-strength resin.

8. A device, comprising the aerogel of claim 1 .

9. A method of forming the aerogel of claim 1 , the method comprising:

mixing cotton cellulose fibres and paper cellulose fibres in a weight ratio of 1:1 to 1:6 and a cross-linker to form a mixture;

sonicating the mixture;

freezing the sonicated mixture; and

freeze drying the frozen mixture to form the aerogel.

10. The method of claim 9 , wherein the mixing further comprises mixing at least one additive.

11. The method of claim 10 , wherein the at least one additive is chitosan.

12. The method of claim 9 , wherein the method further comprises compressing the aerogel following the freeze drying.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 2, 2021
From: DUONG, HAI MINH; PHAN-THIEN, NHAN; GU, BOWEN; PENNEFATHER, MARK PYNE; NGUYEN, THANH XUAN
To: NATIONAL UNIVERSITY OF SINGAPORE
Reel/Frame 055458/0748 →
Continuity (2)
Provisional Application 62432244 · Dec 9, 2016
Related Publication 20190282988A1 · Sep 19, 2019