IP Library Granted Patent US 11,104,658
Granted Patent B2
US 11,104,658 · App. 15/537,283 · Granted Aug 31, 2021

Method of treating or preventing Ras-mediated diseases

Inventors: Gary A. Piazza (Daphne, AL); Xi Chen (Hoover, AL); Adam B. Keeton (Gardendale, AL); Michael R. Boyd (Orange Beach, AL)
Assignee: ADT Pharmaceuticals, LLC
C07D317/64A61K31/165A61K31/167A61K31/216A61K31/341A61K31/36A61K31/40A61K31/401A61K31/421A61K31/44A61K31/4402A61K31/445A61K31/4406A61K31/496A61K31/5375A61K31/5377A61K45/06C07C233/58C07C235/32C07C235/34C07C237/20C07C311/29C07D207/14C07D207/335C07D207/337C07D211/56C07D213/24C07D213/40C07D213/75C07D235/30C07D307/38C07D307/52C07D307/54C07D405/12G01N33/5748A61K2300/00C07C2601/02C07C2602/08
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Quick Facts
Patent No.
US 11,104,658
App. No.
15/537,283
Granted
Aug 31, 2021
Kind
B2
Abstract

Disclosed are compounds, for example, a compound of formula I, wherein R, R 0 , R 1 -R 8 , n, X, Y, Y′, and E are as described herein, pharmaceutical compositions containing such compounds, and methods of treating or preventing a disease or condition for example, cancer, mediated by the ras gene.

Claims (30)

1. A method of inhibiting growth of a tumor in a human patient, said tumor having been determined to contain a mutant ras gene encoding for expression of a hyperactive Ras, the method comprising administering to said patient a prodrug of formula II,

wherein:

R and R 0 are independently selected from the group consisting of hydrogen, alkyl, and alkoxy;

n is 0, 1, or 2;

Y and Y′ together is double-bonded oxygen;

R 1 , R 3 , and R 4 are hydrogen and R 2 is selected from halogen and alkoxy;

R 7 is hydrogen;

R 8 is alkyl;

R 12 and R 16 are hydrogen; R 13 , R 14 , and R 15 are alkoxy; and

X is NR′R″, where R′ is selected from the group consisting of heterocyclyl and heterocyclylalkyl wherein the heterocyclyl of the heterocyclyl and heterocyclylalkyl is an unsubstituted group selected from furanyl, pyridinyl, piperidinyl, piperazinyl, pyrrolidinyl and morpholinyl; and R″ is hydrogen;

wherein R 14 of said prodrug is converted in vivo in said patient to a Ras-inhibitory effective amount of a compound of formula II wherein R 14 is hydroxyl.

2. The method of claim 1 , wherein the prodrug is selected from:

(Z)-2-(1-(3,4,5-trimethoxybenzylidene)-5-methoxy-2-methyl-1H-inden-3-yl)-N-(pyridin-3-yl)acetamide,

(Z)-2-(5-fluoro-1-(3,4,5-trimethoxybenzylidene)-2-methyl-1H-inden-3-yl)-N-(furan-2-ylmethyl)acetamide,

(Z)-2-(1-(3,4,5-trimethoxybenzylidene)-5-methoxy-2-methyl-1H-inden-3-yl)-N-(pyridin-3-ylmethyl)acetamide,

(Z)-2-(5-fluoro-1-(3,4,5-trimethoxybenzylidene)-2-methyl-1H-inden-3-yl)-N-(pyridin-2-ylmethyl)acetamide,

(Z)-2-(5-fluoro-1-(3,4,5-trimethoxybenzylidene)-2-methyl-1H-inden-3-yl)-N-(pyridin-3-ylmethyl)acetamide, and

(Z)-2-(1-(3,4,5-trimethoxybenzylidene)-5-methoxy-2-methyl-1H-inden-3-yl)-N-(pyridin-2-ylmethyl)acetamide.

3. The method of claim 1 , wherein the prodrug is

(Z)-2-(1-(3,4,5-trimethoxybenzylidene)-5-methoxy-2-methyl-1H-inden-3-yl)-N-(pyridin-3-yl)acetamide.

4. The method of claim 1 , wherein the prodrug is

(Z)-2-(5-fluoro-1-(3,4,5-trimethoxybenzylidene)-2-methyl-1H-inden-3-yl)-N-(furan-2-ylmethyl)acetamide.

5. The method of claim 1 , wherein the prodrug is

(Z)-2-(1-(3,4,5-trimethoxybenzylidene)-5-methoxy-2-methyl-1H-inden-3-yl)-N-(pyridin-3-ylmethyl).

6. The method of claim 1 , wherein the prodrug is

(Z)-2-(5-fluoro-1-(3,4,5-trimethoxybenzylidene)-2-methyl-1H-inden-3-yl)-N-(pyridin-2-ylmethyl)acetamide.

7. The method of claim 1 , wherein the prodrug is

(Z)-2-(5-fluoro-1-(3,4,5-trimethoxybenzylidene)-2-methyl-1H-inden-3-yl)-N-(pyridin-3-ylmethyl)acetamide.

8. The method of claim 1 , wherein the prodrug is

(Z)-2-(1-(3,4,5-trimethoxybenzylidene)-5-methoxy-2-methyl-1H-inden-3-yl)-N-(pyridin-2-ylmethyl)acetamide.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 16, 2018
From: PIAZZA, GARY A.; CHEN, XI; KEETON, ADAM B.; BOYD, MICHAEL R.
To: ADT PHARMACEUTICALS, LLC
Reel/Frame 045256/0555 →
Continuity (3)
Continuation In Part 14571690 · Dec 16, 2014
Related Publication 20180044314A1 · Feb 15, 2018
Related Publication 20180251443A9 · Sep 6, 2018
Cited By (1)
US 12,479,813