IP Library Granted Patent US 11,111,453
Granted Patent B2
US 11,111,453 · App. 16/341,195 · Granted Sep 7, 2021

Method for lubricating internal combustion engine

Inventor: Shigeki Takeshima (Tokyo, JP)
Assignee: ENEOS Corporation
C10M169/04C10M101/02C10M129/26C10M129/54C10M133/12C10M135/10C10M137/02C10M139/00C10M159/20C10M159/24C10M171/00C10M2203/1025C10M2207/144C10M2215/064C10M2219/044C10M2223/02C10M2227/09C10N2010/04C10N2020/02C10N2030/04C10N2030/06C10N2030/10C10N2040/255
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Quick Facts
Patent No.
US 11,111,453
App. No.
16/341,195
Granted
Sep 7, 2021
Kind
B2
Abstract

A method for lubricating an internal combustion engine, the method including: supplying a lubricating oil composition to a cylinder of an internal combustion engine, wherein the internal combustion engine has a mean effective pressure of no less than 1.3 MPa, wherein an integrated intensity ratio of peaks of CaO in a X-ray diffraction spectrum of an ash is no more than 16.5%, the ash being obtained by incinerating the lubricating oil composition in an air at 950° C.

Claims (83)

1. A cylinder lubricating oil composition for a premix combustion crosshead diesel engine, the lubricating oil composition comprising:

a mineral base oil or a synthetic base oil or a mixture thereof, as a lubricant base oil; and

(A) a metallic detergent, the component (A) comprising:

(A1) a calcium borate-overbased metallic detergent in an amount of 0.35 to 1.70 mass % in terms of calcium on the basis of the total mass of the composition, the component (A1) comprising a calcium borate-overbased calcium salicylate detergent, or a calcium borate-overbased calcium sulfonate detergent, or any combination thereof; and

(A2) a calcium carbonate-overbased metallic detergent in an amount of 0.35 to 1.30 mass % in terms of calcium on the basis of the total mass of the composition, the component (A2) comprising a calcium carbonate-overbased calcium salicylate detergent, or a calcium carbonate-overbased calcium sulfonate detergent, or any combination thereof,

wherein an integrated intensity ratio of peaks of CaO in a X-ray diffraction spectrum of an ash is no more than 16.5%, the ash being obtained by incinerating the lubricating oil composition in an air at 950° C.;

a molar ratio B/Ca of a boron content B (unit: mol) of the lubricating oil composition derived from the component (A) and a calcium content Ca (unit: mol) of the lubricating oil composition derived from the component (A) is no less than 0.52; and

the lubricating oil composition is used to lubricate at least a cylinder in a premix combustion crosshead diesel engine, wherein the premix combustion crosshead diesel engine uses a main fuel having a flash point of no more than 15° C.

2. The lubricating oil composition according to claim 1 , further comprising:

one or more selected from the group consisting of: (B) an ashless dispersant, (C) a phosphorus-containing anti-wear agent, (D) an amine antioxidant, and (E) an oil-soluble organic molybdenum compound.

3. The lubricating oil composition according to claim 1 ,

wherein the component (A1) consists of

the calcium borate-overbased calcium salicylate detergent, or

the calcium borate-overbased calcium sulfonate detergent, or

any combination thereof; and

the molar ratio B/Ca is 0.52 to 1.43.

4. The lubricating oil composition according to claim 1 ,

wherein the lubricating oil composition has a kinematic viscosity at 100° C. of 16.3 to 21.9 mm 2 /s.

5. A method for lubricating a cylinder of a premix combustion crosshead diesel engine, comprising:

a) supplying the lubricating oil composition as defined in claim 1 to a cylinder of a premix combustion crosshead diesel engine, wherein the premix combustion crosshead diesel engine has a mean effective pressure of no less than 1.3 MPa; and

b) making a main fuel ignite in the cylinder, wherein the main fuel has a flash point of no more than 15° C.

6. The method according to claim 5 ,

wherein the main fuel consists of

a C 1-4 hydrocarbon, or

dimethyl ether, or

any combination thereof.

7. The method according to claim 6 ,

wherein the b) making a main fuel ignite in the cylinder comprises:

i) compressing a fuel-air mixture of the main fuel and an air in the cylinder; and

ii) injecting a pilot fuel into the cylinder, to ignite the fuel-air mixture,

wherein the pilot fuel consists of a heavy fuel oil, a light fuel oil, or kerosene, or any combination thereof.

8. A lubricating oil composition for a premix combustion middle-speed trunk piston diesel engine, the lubricating oil composition comprising:

a mineral base oil or a synthetic base oil or a mixture thereof, as a lubricant base oil; and

(A) a metallic detergent, the component (A) comprising:

(A1) a calcium borate-overbased metallic detergent in an amount of 0.25 to 1.20 mass % in terms of calcium on the basis of the total mass of the composition, the component (A1) comprising a calcium borate-overbased calcium salicylate detergent, or a calcium borate-overbased calcium sulfonate detergent, or any combination thereof; and

(A2) a calcium carbonate-overbased metallic detergent in an amount of 0.25 to 0.90 mass % in terms of calcium on the basis of the total mass of the composition, the component (A2) comprising a calcium carbonate-overbased calcium salicylate detergent, or a calcium carbonate-overbased calcium sulfonate detergent, or any combination thereof,

wherein an integrated intensity ratio of peaks of CaO in a X-ray diffraction spectrum of an ash is no more than 16.5%, the ash being obtained by incinerating the lubricating oil composition in an air at 950° C.;

a molar ratio B/Ca of a boron content B (unit: mol) of the lubricating oil composition derived from the component (A) and a calcium content Ca (unit: mol) of the lubricating oil composition derived from the component (A) is no less than 0.52; and

the lubricating oil composition is used to lubricate at least a cylinder in a premix combustion middle-speed trunk piston diesel engine, wherein the premix combustion middle-speed trunk piston diesel engine uses a main fuel having a flash point of no more than 15° C.

9. The lubricating oil composition according to claim 8 , further comprising:

one or more selected from the group consisting of: (B) an ashless dispersant, (C) a phosphorus-containing anti-wear agent, (D) an amine antioxidant, and (E) an oil-soluble organic molybdenum compound.

10. The lubricating oil composition according to claim 8 ,

wherein the component (A1) consists of

the calcium borate-overbased calcium salicylate detergent, or

the calcium borate-overbased calcium sulfonate detergent, or

any combination thereof; and

the molar ratio B/Ca is 0.52 to 1.43.

11. The lubricating oil composition according to claim 8 ,

wherein the lubricating oil composition has a kinematic viscosity at 100° C. of no less than 9.3 mm 2 /s and less than 16.3 mm 2 /s.

12. A method for lubricating a premix combustion middle-speed trunk piston diesel engine, the method comprising:

a) supplying the lubricating oil composition as defined in claim 8 to a cylinder of a premix combustion middle-speed trunk piston diesel engine, wherein the premix combustion middle-speed trunk piston diesel engine has a mean effective pressure of no less than 1.3 MPa; and

b) making a main fuel ignite in the cylinder, wherein the main fuel has a flash point of no more than 15° C.

13. The method according to claim 12 ,

wherein the main fuel consists of

a C 1-4 hydrocarbon, or

dimethyl ether, or

any combination thereof.

14. The method according to claim 13 ,

wherein the b) making a main fuel ignite in the cylinder comprises:

i) compressing a fuel-air mixture of the main fuel and an air in the cylinder; and

ii) injecting a pilot fuel into the cylinder, to ignite the fuel-air mixture,

wherein the pilot fuel consists of a heavy fuel oil, a light fuel oil, or kerosene, or any combination thereof.

15. A lubricating oil composition for a turbocharged gasoline engine, the lubricating oil composition comprising:

a mineral base oil or a synthetic base oil or a mixture thereof, as a lubricant base oil; and

(A) a metallic detergent, the component (A) comprising:

(A1) a calcium borate-overbased metallic detergent in an amount of 0.10 to 0.28 mass % in terms of calcium on the basis of the total mass of the composition, the component (A1) comprising a calcium borate-overbased calcium salicylate detergent, or a calcium borate-overbased calcium sulfonate detergent, or any combination thereof; and

(A2) a calcium carbonate-overbased metallic detergent in an amount of 0.10 to 0.18 mass % in terms of calcium on the basis of the total mass of the composition, the component (A2) comprising a calcium carbonate-overbased calcium salicylate detergent, or a calcium carbonate-overbased calcium sulfonate detergent, or any combination thereof,

wherein an integrated intensity ratio of peaks of CaO in a X-ray diffraction spectrum of an ash is no more than 16.5%, the ash being obtained by incinerating the lubricating oil composition in an air at 950° C.;

a molar ratio B/Ca of a boron content B (unit: mol) of the lubricating oil composition derived from the component (A) and a calcium content Ca (unit: mol) of the lubricating oil composition derived from the component (A) is no less than 0.52; and

the lubricating oil composition is used to lubricate at least a cylinder in a turbocharged gasoline engine.

16. The lubricating oil composition according to claim 15 , further comprising:

one or more selected from the group consisting of: (B) an ashless dispersant, (C) a phosphorus-containing anti-wear agent, (D) an amine antioxidant, and (E) an oil-soluble organic molybdenum compound.

17. The lubricating oil composition according to claim 15 ,

wherein the component (A1) consists of

the calcium borate-overbased calcium salicylate detergent, or

the calcium borate-overbased calcium sulfonate detergent, or

any combination thereof; and

the molar ratio B/Ca is 0.52 to 1.43.

18. The lubricating oil composition according to claim 15 ,

wherein the lubricating oil composition has a kinematic viscosity at 100° C. of no less than 4.0 mm 2 /s and less than 9.3 mm 2 /s.

19. A method for lubricating a premix combustion turbocharged gasoline engine, the method comprising:

a) supplying the lubricating oil composition as defined in claim 15 to a cylinder of a turbocharged gasoline engine, wherein the turbocharged gasoline engine has a mean effective pressure of no less than 1.3 MPa; and

b) making a fuel ignite in the cylinder, wherein the fuel consists of gasoline.

Assignments (2)
CHANGE OF NAME Recorded Jun 21, 2021
From: JXTG NIPPON OIL & ENERGY CORPORATION
To: ENEOS CORPORATION
Reel/Frame 056633/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 11, 2019
From: TAKESHIMA, SHIGEKI
To: JXTG NIPPON OIL & ENERGY CORPORATION
Reel/Frame 048861/0967 →
Priority Claims (1)
JP JP2016-204413 · Oct 18, 2016 · national
Continuity (1)
Related Publication 20190233758A1 · Aug 1, 2019