IP Library Granted Patent US 11,111,563
Granted Patent B2
US 11,111,563 · App. 16/084,106 · Granted Sep 7, 2021

High strength and erosion resistant powder blends

Inventors: Ravi K. Enneti (Towanda, PA); Kevin Prough (Athens, PA); Keith Newman (Athens, PA)
Assignee: GLOBAL TUNGSTEN & POWDERS CORP.
C22C29/08C22C1/051C22C9/00B22F7/06B22F2005/001
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Quick Facts
Patent No.
US 11,111,563
App. No.
16/084,106
Granted
Sep 7, 2021
Kind
B2
Abstract

Composites comprising various fractions of ultra coarse (UC) tungsten carbide (WC) and cast carbide (CC), along with composites comprising fractions of UC-WC and CC having various particle size and showing an improved strength and erosion resistance, and methods for making the inventive composites.

Claims (23)

1. A method for preparing a composite comprising:

a) contacting about 40-70 wt % of a first fraction of ultra coarse tungsten carbide

with about 30-60 wt % a first fraction of cast carbide (CC) to form a blend, wherein the blend has a tap density of about 9-11.5 g/cm 3 ;

b) tapping the blend for at least 5 cycles; and

c) infiltrating the tapped blend with a copper containing alloy, thereby forming the composite,

wherein the formed composite exhibits volume loss of at least 20% lower as compared to a conventional GM-6 metal powder when measured accordingly to ASTM G65 and ASTM G76.

2. The method of claim 1 , wherein the first fraction of ultra-coarse tungsten carbide has a particle size from about 44 micrometers (325 mesh) to about 177 micrometers (80 mesh).

3. The method of claim 1 , wherein the first fraction of cast carbide has a particle size from 44 micrometers (325 mesh) to about 250 micrometers (60 mesh).

4. The method of claim 1 , wherein the first fraction of ultra-coarse tungsten carbide is present in an amount of about 60%.

5. The method of claim 4 , wherein the first fraction of cast carbide is present in an amount 40%.

6. The method of claim 4 , wherein the first fraction of ultra-coarse tungsten carbide has a particle size of at least about 44 micrometers (325 mesh).

7. The method of claim 4 , wherein the first fraction of cast carbide has a particle size of smaller than about 250 micrometers (60 mesh) but greater than about 125 micrometers (120 mesh).

8. The method of claim 1 , further comprising a step of mixing the blend with greater than 0 wt % to about 5 wt % of nickel prior to the step of infiltrating.

9. The method of claim 1 , further comprising a step of mixing the blend with greater than 0 wt % to about 5 wt % of iron prior to the step of infiltrating.

10. The method of claim 1 , further comprising a step of mixing the blend with one or more of: (a) from about 5 to about 25 wt % of a second fraction of ultra-coarse tungsten carbide having a particle size of greater than 63 micrometer (230 mesh) but smaller than 88 micrometer (170 mesh); (b) from about 5 to about 25 wt % of a third fraction of ultra-coarse tungsten carbide having a particle size of greater than 44 micrometer (325 mesh) but smaller than 63 micrometer (230 mesh); (c) from about 5 to about 25 wt % of a second fraction of cast carbide having a particle size of greater than 63 micrometer (230 mesh) but smaller than 88 micrometer (170 mesh); or d) from about 5 to about 25 wt % of a third fraction of cast carbide having a particle size of greater than 63 micrometer (230 mesh) but smaller than 125 micrometer (120 mesh) prior to the step of infiltrating.

11. The method of claim 1 , wherein the formed composite exhibits a Transverse Rupture Strength (TRS) of greater than 120 KSI.

12. The method of claim 1 , wherein the formed composite exhibits a volume loss under abrasion testing according to ASTM G65 of less than about 6 mm 3 .

13. The method of claim 1 , wherein the cast carbide has a plurality of particles having a microstructured surface.

14. The method of claim 1 , wherein the method comprises tapping the blend for at least 50 cycles.

15. The method of claim 14 , wherein the formed composite exhibits an average volume loss under abrasion testing according to ASTM G65 from 4.26 mm 3 to 4.86 mm 3 .

16. The method of claim 14 , wherein the formed composite exhibits an average Transverse Rupture Strength (TRS) of from 133.6 KSI to 144.6 KSI.

17. The method of claim 14 , further comprising a step of mixing the blend with greater than 0 wt % to about 5 wt % of nickel prior to the step of infiltrating.

18. The method of claim 14 , further comprising a step of mixing the blend with greater than 0 wt % to about 5 wt % of iron prior to the step of infiltrating.

Assignments (2)
CHANGE OF NAME Recorded Jan 31, 2023
From: GLOBAL TUNGSTEN & POWDERS CORP.
To: GLOBAL TUNGSTEN & POWDERS LLC
Reel/Frame 062591/0409 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 9, 2018
From: ENNETI, RAVI K.; PROUGH, KEVIN; NEWMAN, KEITH
To: GLOBAL TUNGSTEN & POWDERS CORP.
Reel/Frame 047461/0060 →
Continuity (2)
Provisional Application 62574469 · Oct 19, 2017
Related Publication 20200063244A1 · Feb 27, 2020