Apparatus for producing water-absorbing resin particles
An apparatus for producing water-absorbing resin particles for which surface cross-linking treatment is conducted, the surface cross-linking treatment being conducted by spraying a surface cross-linking agent to a water-absorbing resin particle precursor and heating the agent and the precursor, the apparatus includes a treatment container in which the surface cross-linking treatment is conducted, a stirring device including a stirring member disposed in the treatment container, a heating device that heats an inside of the treatment container; and a spray nozzle disposed in the treatment container, the spray nozzle spraying into the treatment container the surface cross-linking agent supplied from a surface cross-linking agent supply source in an exterior of the treatment container through a supply pipe. In a flow path in the spray nozzle spanning from an entrance of the spray nozzle to a spray exit, a point whose opening cross-section is smallest in a flow path through which a fluid passes is the spray exit. A product with further stable physical properties can thereby be acquired.
1. A method for producing water-absorbing resin particles, the method comprising a surface cross-linking treatment being conducted by spraying a surface cross-linking agent to a water-absorbing resin particle precursor and heating the agent and the precursor, the water-absorbing resin particle precursor including unreacted monomers, wherein
the surface cross-linking treatment is conducted by an apparatus for producing water-absorbing resin particles, and
the apparatus includes:
a treatment container in which the surface cross-linking treatment is conducted;
a stirring device including a stirring member disposed in the treatment container;
a heating device that heats an inside of the treatment container;
a decompressing device that reduces a pressure in the treatment container; and
a spray nozzle disposed in the treatment container, the spray nozzle spraying into the treatment container the surface cross-linking agent, in a flow path in the spray nozzle spanning from an entrance of the spray nozzle to a spray exit, a point whose opening cross-section is smallest in a flow path through which a fluid passes is the spray exit.
2. The method for producing water-absorbing resin particles according to claim 1 , the apparatus comprising a strainer disposed in a supply pipe on an upstream side of the entrance of the spray nozzle, the strainer including plural openings each having an opening cross-section smaller than an opening cross-section of the spray exit of the spray nozzle.
3. The method for producing water-absorbing resin particles according to claim 2 , wherein the heating device is a heating jacket arranged on an outer circumference of the treatment container, and the strainer is disposed in the supply pipe on an outer side of the heating jacket.
4. The method for producing water-absorbing resin particles according to claim 2 , wherein
the supply pipe for the surface cross-linking agent includes a first pipe that is a header pipe having plural spray nozzles connected thereto and a second pipe that connects the surface cross-linking agent supply source and the first pipe to each other, and
the first pipe and the plural spray nozzles are arranged inside the treatment container, and the strainer is disposed in a portion on an outer side of the treatment container, of the second pipe.
5. The method for producing water-absorbing resin particles according to claim 2 , the apparatus further comprising a cooling device that cools the strainer.
6. The method for producing water-absorbing resin particles according to claim 2 , wherein a nitrogen supply pipe is connected to the supply pipe.
7. The method for producing water-absorbing resin particles according to claim 1 , wherein the heating device includes a heat transmitting part that is arranged in an inside of the stirring device.
8. The method for producing water-absorbing resin particles according to claim 2 , wherein the strainer is disposed on a downstream side of a pump which is disposed in the supply pipe to supply the surface cross-linking agent to the spray nozzle through the supply pipe.
9. A method for producing water-absorbing resin particles, the method comprising:
spraying a surface cross-linking agent to a water-absorbing resin particle precursor in a treatment container, the water-absorbing resin particle precursor including unreacted monomers;
stirring the water-absorbing resin particle precursor in the treatment container;
heating the surface cross-linking agent and the water-absorbing resin particle precursor in the treatment container; and
reducing a pressure in the treatment container, wherein
the surface cross-linking agent is sprayed into the treatment container through a spray nozzle disposed in the treatment container, in a flow path in the spray nozzle spanning from an entrance of the spray nozzle to a spray exit, a point whose opening cross-section is smallest in a flow path through which a fluid passes is the spray exit.