IP Library › Granted Patent US 11,125,732
Granted Patent B2
US 11,125,732 · App. 16/080,753 · Granted Sep 21, 2021

System, apparatus, and method for monitoring organic compounds in a gas environment

Inventor: Drew Gentner (New York, NM)
Assignee: Yale University
G01N33/0047G01N1/00G01N30/08G01N30/12G01N30/20G01N30/30G01N30/32G01N30/64G01N30/88G01N33/0006G01N33/0073G01N1/405G01N2001/4088G01N2030/025G01N2030/085G01N2030/121G01N2030/3084G01N2030/326G01N2030/642G01N2030/884G01N2033/0019
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Quick Facts
Patent No.
US 11,125,732
App. No.
16/080,753
Granted
Sep 21, 2021
Kind
B2
Abstract

The invention relates to a system and micro monitor apparatus, a space-, time-, and cost-efficient device to concentrate, identify, and quantify organic compounds in gas environments. The invention further relates to a method centered on gas chromatography for identifying and quantifying organic compounds in gas environments, using air as the carrier gas, without the need for a compressed pre-bottled purified carrier gas.

Claims (33)

1. A system for analyzing a gas mixture, comprising:

a filter;

a flow constrictor;

a trap;

a chromatographic column;

a detector; and

a pump,

wherein the trap and the pump are fluidly connected to form a first gas flow path with the pump positioned downstream of the trap,

wherein the filter, the flow constrictor, the trap, the chromatographic column, the detector, and the pump, are fluidly connected to form a second gas flow path, with the pump positioned downstream of the filter, the trap, the chromatographic column, and the detector, and the flow constrictor is positioned upstream of the trap, the chromatographic column, the detector, and the pump; and

wherein the flow constrictor is positioned only in the second gas flow path.

2. The system of claim 1 , wherein the detector and the pump are fluidly connected to form a third gas flow path.

3. The system of claim 1 , wherein the chromatographic column is selected from the group consisting of a gas-solid adsorption chromatographic column, and a gas-liquid gas chromatography column.

4. The system of claim 1 , wherein the trap further comprises an adsorbent material.

5. The system of claim 1 , wherein the filter is an activated charcoal filter.

6. The system of claim 1 , wherein the detector is selected from the group consisting of a photo ionization detector, a mass spectrometer, a spectrophotometer, and a thermal conductivity detector.

7. The system of claim 1 , wherein the detector is a photo ionization detector.

8. The system of claim 1 , wherein the pump provides negative pressure.

9. The system of claim 1 , further comprising a housing.

10. The system of claim 9 , wherein the housing is no larger than 216 cubic inch.

11. The system of claim 1 , wherein the system is capable of detecting chemical compounds with a sensitivity of parts-per-trillion.

12. A system for analyzing a gas mixture, comprising:

a filter;

a flow constrictor;

a trap;

a chromatographic column;

a detector; and

a pump,

wherein the trap and the pump are fluidly connected to form a first gas flow path with the pump positioned downstream of the trap,

wherein the filter, the flow constrictor, the trap, the chromatographic column, the detector, and the pump, are fluidly connected to form a second gas flow path, with the pump positioned downstream of the filter, the flow constrictor, the trap, the chromatographic column, and the detector, and the flow constrictor is positioned downstream of the filter and upstream of the trap, the chromatographic column, the detector, and the pump.

13. A system for analyzing a gas mixture, comprising:

a first gas flow path having a trap and a downstream pump configured to direct a first flow of gas; and

a second gas flow path having the trap, a flow constrictor upstream of the trap, a chromatographic column, a detector, and the downstream pump configured to direct a second flow of gas;

wherein the second flow of gas exiting the flow constrictor in the second gas flow path enters the trap in a direction opposite the first flow of gas.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 22, 2018
From: GENTNER, DREW
To: YALE UNIVERSITY
Reel/Frame 047255/0776 →
Continuity (2)
Provisional Application 62322980 · Apr 15, 2016
Related Publication 20190094195A1 · Mar 28, 2019