IP Library Granted Patent US 11,155,007
Granted Patent B2
US 11,155,007 · App. 14/560,833 · Granted Oct 26, 2021

Nanostructures from laser-ablated nanohole templates

Inventors: William Hudson Hofmeister (Nashville, TN); Alexander Yuryevich Terekhov (Murfreesboro, TN); Jose Lino Vasconcelos da Costa (Tullahoma, TN); Kathleen Stacia Lansford (Manchester, TN); Deepak Rajput (Tullahoma, TN); Lloyd M. Davis (Tullahoma, TN)
Assignee: ULTRA SMALL FIBERS, LLC
B29C41/003B29C33/3842B29C41/02B29C41/38B29C41/42B82Y10/00B82Y40/00C08B3/06C08B5/02C08F110/02C08F120/18C08F120/40C08G63/08C08G63/664C08G77/04G03F7/0002B29K2001/12B29K2001/18B29K2023/06B29K2031/04B29K2033/12B29K2067/04B29K2071/00B29K2083/00B29K2901/10B29K2901/12B29K2907/045B29K2909/00B29K2909/08B29K2909/14B29K2995/0026B29K2995/0094B29L2031/7562Y02P20/582Y10T428/24355Y10T428/24802
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Quick Facts
Patent No.
US 11,155,007
App. No.
14/560,833
Granted
Oct 26, 2021
Kind
B2
Abstract

Solution casting a nanostructure. Preparing a template by ablating nanoholes in a substrate using single-femtosecond laser machining. Replicating the nanoholes by applying a solution of a polymer and a solvent into the template. After the solvent has substantially dissipated, removing the replica from the substrate.

Claims (16)

1. A method for fabricating a nanofiber array, comprising:

(a) providing a template comprising a transparent substrate having a surface, the surface comprising a plurality of nanoholes, each nanohole of said plurality being ablated in said surface using a single femtosecond laser pulse;

(b) filling said plurality of nanoholes with a polymer solution; and

(c) extracting an array of polymer nanofibers from the template;

wherein said nanofibers have an aspect ratio of at least ten-to-one and a diameter of less than 1000 nanometers.

2. The method of claim 1 , wherein said array of polymer nanofibers comprises a plurality of freestanding polymer nanofibers attached to a polymer substrate.

3. The method of claim 2 , wherein said polymer nanofibers are positioned on said polymer substrate in a non-random, user-defined pattern.

4. The method of claim 1 , further comprising treating the surface of the template with a material to modify the surface and bonding characteristics associated with said template and said array.

5. The method of claim 1 , further comprising applying a fluorocarbon-based antistick coating to the template prior to filling said plurality of nanoholes with a polymer solution.

6. The method of claim 5 , wherein the fluorocarbon-based antistick coating is prepared from perfluorodecyltrichlorosilane.

7. The method of claim 1 , further comprising modifying the template to enlarge or change a geometry of said plurality of nanoholes.

8. The method of claim 7 , wherein said modifying comprises using chemical reactions, vapor, etching, or liquid growth processes.

9. The method of claim 1 , wherein said nanofibers have an aspect ratio of greater than twenty-five-to-one.

10. The method of claim 1 , wherein said nanofibers have an average length greater than ten micrometers and a diameter less than one micrometer.

11. The method of claim 1 , wherein said nanofibers have an average length of at least thirty micrometers and a diameter less than one micrometer.

12. The method of claim 1 , wherein said polymer is a polymer capable of forming a continuous film.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2021
From: HOFMEISTER, WILLIAM HUDSON; TEREKHOV, ALEXANDER YURYEVICH; DA COSTA, JOSE LINO VASCONCELOS; LANSFORD, KATHLEEN STACIA; RAJPUT, DEEPAK; DAVIS, LLOYD M.
To: UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
Reel/Frame 057307/0908 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2021
From: UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
To: ULTRA SMALL FIBERS, LLC
Reel/Frame 057308/0001 →
Continuity (3)
Continuation 13769575 · Feb 18, 2013
Provisional Application 61599926 · Feb 16, 2012
Related Publication 20150093550A1 · Apr 2, 2015