IP Library Granted Patent US 11,224,587
Granted Patent B2
US 11,224,587 · App. 16/736,606 · Granted Jan 18, 2022

Liquid carbon dioxide botanical extraction system

Inventors: Nelson W. Sorbo (Temecula, CA); Jon R. Turner (Minneapolis, MN); Jon Wikstrom (Eagan, MN)
Assignee: Cool Clean Technologies, LLC
A61K31/352A61K31/465A61K36/185A61K36/81A61K2236/00
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Quick Facts
Patent No.
US 11,224,587
App. No.
16/736,606
Granted
Jan 18, 2022
Kind
B2
Abstract

A process for extracting a botanical organic compound from cannabis with subcritical liquid carbon dioxide includes providing a pressurizable extraction vessel. The cannabis is placed within the pressurizable extraction vessel, whereupon the extraction vessel is filled with liquid carbon dioxide under subcritical conditions. The cannabis is then allowed to be in contact with the subcritical liquid carbon dioxide for a selected period of time so as to extract at least a portion of the botanical organic compounds from the cannabis into the subcritical liquid carbon dioxide. The subcritical liquid carbon dioxide containing the botanical organic compound is then removed from the extraction vessel, and the liquid carbon dioxide is separated from the botanical organic compound.

Claims (31)

1. A process for extracting cannabinoids from cannabis with sub-critical liquid carbon dioxide, the process comprising:

providing a permeable container;

placing the cannabis within the permeable container;

providing a pressurizable extraction vessel having a drum or basket;

placing the permeable container containing the cannabis within the extraction vessel;

filling the extraction vessel with liquid carbon dioxide under subcritical conditions;

activating the drum or basket while the pressurizable extraction vessel is under pressure to allow the cannabis to be in contact with the subcritical liquid carbon dioxide so as to extract at least a portion of the cannabinoids from the cannabis into the subcritical liquid carbon dioxide;

removing from the extraction vessel the subcritical liquid carbon dioxide containing the cannabinoids extracted from the cannabis ; and

separating the liquid carbon dioxide from cannabinoids.

2. The process of claim 1 , further comprising adding ethanol to the liquid carbon dioxide.

3. The process of claim 1 , wherein the drum or basket includes a rotatable drum containing baffles, wherein activating the drum or basket includes rotating the drum when the permeable container and the cannabis are in contact with the subcritical liquid carbon dioxide in order for the baffles to contact the permeable container.

4. The process of claim 1 , further comprising:

depressurizing the extraction vessel; and

removing from the extraction vessel the first permeable container containing the cannabis.

5. The process of claim 1 , wherein the extraction of the at least portion of the organic compound from the cannabis into the sub-critical liquid carbon dioxide is conducted at a pressure between 2.76 to 4.99 MPa.

6. The process of claim 1 , wherein the extraction of at least a portion of the cannabinoids from the cannabis into the subcritical liquid carbon dioxide is conducted at a temperature between −10° C. to 14° C.

7. The process of claim 1 , further comprising distilling the subcritical liquid carbon dioxide containing the cannabinoid to yield the cannabinoids.

8. The process of claim 1 , wherein the basket or drum includes a rotatable impeller, wherein activating the drum or basket includes rotating the impeller to permit the subcritical liquid carbon dioxide to contact the cannabis contained within the permeable container.

9. A process for extracting a cannabinoid from cannabis , the process comprising:

providing a permeable container;

placing the cannabis within the permeable container;

providing a pressurizable extraction vessel having an agitation device a rotatable impeller;

placing the permeable container containing the cannabis within the extraction vessel;

filling the extraction vessel with liquid carbon dioxide under subcritical conditions;

activating the agitation device rotatable impeller while the pressurizable extraction vessel is under pressure to allow the cannabis to be in contact with the subcritical liquid carbon dioxide so as to extract at least a portion of the cannabinoid from the cannabis into the subcritical liquid carbon dioxide;

removing from the extraction vessel the subcritical liquid carbon dioxide containing the cannabinoid extracted from the cannabis ; and

separating the liquid carbon dioxide from the cannabinoid.

10. The process of claim 9 , further comprising adding ethanol to the liquid carbon dioxide.

11. The process of claim 9 , wherein the extraction of the at least portion of the cannabinoid from the cannabis into the sub-critical liquid carbon dioxide is conducted at a pressure between 2.76 to 4.99 MPa.

12. The process of claim 9 , wherein the extraction of the at least portion of the cannabinoid from the cannabis into the sub-critical liquid carbon dioxide is conducted at a temperature between −10° C. to 14° C.

13. The process of claim 9 , further comprising distilling the subcritical liquid carbon dioxide containing the cannabinoid to yield the cannabinoid.

Continuity (4)
Continuation 16283140 · Feb 22, 2019
Continuation 15633079 · Jun 26, 2017
Provisional Application 62354354 · Jun 24, 2016
Related Publication 20200138774A1 · May 7, 2020