IP Library › Granted Patent US 11,242,253
Granted Patent B2
US 11,242,253 · App. 16/477,814 · Granted Feb 8, 2022

Method for producing polycrystalline silicon

Inventor: Yuichi Inoue (Yamaguchi, JP)
Assignee: TOKUYAMA CORPORATION
C01B33/03
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,242,253
App. No.
16/477,814
Granted
Feb 8, 2022
Kind
B2
Abstract

Provided is a method which not only prevents (i) accumulation of fine silicon powder in a separation device and a pipe which are provided in steps after passage of a filter and (ii) damage to a pump, but also reduces adhesion of a silane oligomer to the filter. A method, in accordance with an embodiment of the present invention, for producing polycrystalline silicon, includes: a silicon deposition step; a separation step; and a fine powder removal step of removing the fine silicon powder by passing a chlorosilane condensate through a filter.

Claims (11)

1. A method for producing a polycrystalline silicon, comprising the steps of:

a) depositing the polycrystalline silicon by reacting a chlorosilane compound and a hydrogen together;

b) separating an exhaust gas which is discharged through step a) into a chlorosilane condensate and a gas component, wherein the chlorosilane condensate contains a fine silicon powder in an amount of 0.01% by mass to 0.3% by mass, wherein the gas component contains a hydrogen gas and a hydrogen chloride;

c) removing the fine silicon powder by passing the chlorosilane condensate containing the fine silicon powder through a filter by use of a slurry pump to prevent an accumulation of the fine silicon powder in a separation device and a pipe which are provided in steps after passage of the filter and damage to the slurry pump, and further to reduce adhesion of a silane oligomer to the filter; and

d) distilling the chlorosilane condensate after the fine silicon powder removal in step c) to obtain a chlorosilane compound and circulating the chlorosilane compound to step a).

2. The method as set forth in claim 1 , further comprising

circulating part of the chlorosilane condensate discharged from the slurry pump to step b).

3. The method as set forth in claim 2 , wherein:

the chlorosilane condensate is carried to the slurry pump after the chlorosilane condensate is passed through a strainer.

4. The method as set forth in claim 1 , wherein:

the filter has a pore size of 1 μm to 5 μm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 15, 2019
From: INOUE, YUICHI
To: TOKUYAMA CORPORATION
Reel/Frame 049748/0184 →
Priority Claims (1)
JP JP2017-005439 · Jan 16, 2017 · national
Continuity (1)
Related Publication 20190375642A1 · Dec 12, 2019