IP Library Granted Patent US 11,268,952
Granted Patent B2
US 11,268,952 · App. 16/745,231 · Granted Mar 8, 2022

Flavors, flavor modifiers, tastants, taste enhancers, umami or sweet tastants, and/or enhancers and use thereof

Inventors: Catherine Tachdjian (San Diego, CA); Andrew P. Patron (San Marcos, CA); Sara L. Adamski-Werner (San Diego, CA); Farid Bakir (San Diego, CA); Qing Chen (San Diego, CA); Vincent Darmohusodo (Encinitas, CA); Stephen Terrence Hobson (San Marcos, CA); Xiaodong Li (San Diego, CA); Ming Qi (Shanghai, CN); Daniel H. Rogers (San Diego, CA); Marketa Rinnova (San Diego, CA); Guy Servant (San Diego, CA); Xiao-Qing Tang (San Diego, CA); Mark Zoller (La Jolla, CA); David Wallace (San Diego, CA); Amy Xing (San Diego, CA); Klaus Gubernator (Del Mar, CA)
Assignee: Firmenich Incorporated
G01N33/543A23L2/56A23L27/202A23L27/203A23L27/2054A23L27/88A61K8/4973A61K8/55A61K47/22A61K47/24C07C233/65C07C235/54C07C275/30C07C275/34C07D209/08C07D209/42C07D213/40C07D213/81C07D213/85C07D215/48C07D217/06C07D231/14C07D261/18C07D263/56C07D271/12C07D275/03C07D277/64C07D285/135C07D307/52C07D307/68C07D307/79C07D307/82C07D307/84C07D317/68C07D333/24C07D333/38C07D401/04C07D405/12C07D409/12C07D417/12C07F9/65517G01N33/5041G01N33/566G01N33/74A23V2002/00G01N2333/726
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Quick Facts
Patent No.
US 11,268,952
App. No.
16/745,231
Granted
Mar 8, 2022
Kind
B2
Abstract

The present invention relates to the discovery that certain non-naturally occurring, non-peptide amide compounds and amide derivatives, such as oxalamides, ureas, and acrylamides, are useful flavor or taste modifiers, such as a flavoring or flavoring agents and flavor or taste enhancer, more particularly, savory (the “umami” taste of monosodium glutamate) or sweet taste modifiers, savory or sweet flavoring agents and savory or sweet flavor enhancers, for food, beverages, and other comestible or orally administered medicinal products or compositions.

Claims (34)

1. A method for modifying the taste of an ingestible composition, the method comprising combining an ingestible composition with an amide compound or a comestibly acceptable salt thereof, wherein the amide compound is a compound of the formula:

wherein:

R 1 is an aryl group, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy;

R 2 is a hydrogen atom; and

R 3 is a cycloalkyl group having from 5 to 12 ring carbon atoms, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

2. The method of claim 1 , wherein R 1 is a phenyl group, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

3. The method of claim 2 , wherein R 1 is a phenyl group, which comprises two substituents selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

4. The method of claim 3 , wherein R 1 is a phenyl group, which comprises three substituents selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

5. The method of claim 4 , wherein R 1 is a phenyl group, which comprises four substituents selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

6. The method of claim 2 , wherein R 1 is a phenyl group, which comprises three substituents selected independently from the group consisting of methyl, methoxy, trifluoromethyl, and fluoro.

7. The method of claim 6 , wherein R 1 is a phenyl group, which comprises four substituents selected independently from the group consisting of methyl, methoxy, trifluoromethyl, and fluoro.

8. The method of claim 6 , wherein R 1 is a phenyl group, which comprises three substituents selected independently from the group consisting of methyl and fluoro.

9. The method of claim 8 , wherein R 1 is a phenyl group, which comprises four substituents selected independently from the group consisting of methyl and fluoro.

10. The method of claim 9 , wherein R 1 is 2,3,5,6-tetrafluoro-4-methylphenyl or pentafluorophenyl.

11. The method of claim 2 , wherein R 3 is a cyclohexyl group, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

12. The method of claim 6 , wherein R 3 is a cyclohexyl group, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

13. The method of claim 8 , wherein R 3 is a cyclohexyl group, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

14. The method of claim 6 , wherein R 3 is 2,3-dimethylcyclohexyl or 2-methylcyclohexyl.

15. The method of claim 9 , wherein R 3 is 2,3-dimethylcyclohexyl or 2-methylcyclohexyl.

16. The method of claim 10 , wherein R 3 is 2,3-dimethylcyclohexyl or 2-methylcyclohexyl.

17. A compound of the formula:

wherein:

R 1 is a phenyl group, which comprises three substituents selected independently from the group consisting of methyl, trifluoromethyl, and fluoro;

R 2 is a hydrogen atom; and

R 3 is 2,3-dimethylcyclohexyl or 2-methylcyclohexyl.

18. The compound of claim 17 , wherein R 1 is a phenyl group, which comprises three substituents selected independently from the group consisting of methyl and fluoro.

19. The compound of claim 18 , wherein R 1 is 2,3,5,6-tetrafluoro-4-methylphenyl or pentafluorophenyl.

20. A comestible composition, the composition comprising:

a sweetener; and

a compound of the formula:

wherein:

R 1 is an aryl group, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy;

R 2 is a hydrogen atom; and

R 3 is a cycloalkyl group having from 5 to 12 ring carbon atoms, which comprises a substituent selected independently from the group consisting of hydroxy, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SCH 2 CH 3 , methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

Continuity (8)
Continuation 16114108 · Aug 27, 2018
Division 14509761 · Oct 8, 2014
Division 13336272 · Dec 23, 2011
Division 12257017 · Oct 23, 2008
Division 10913303 · Aug 6, 2004
Provisional Application 60552064 · Mar 9, 2004
Provisional Application 60494071 · Aug 6, 2003
Related Publication 20200225217A1 · Jul 16, 2020