IP Library › Granted Patent US 11,278,843
Granted Patent B2
US 11,278,843 · App. 16/633,212 · Granted Mar 22, 2022

Method for separating a natural gas stream into a methane-enriched fraction and a fraction enriched in C

Inventors: Paul Terrien (Newton, MA); Pascal Marty (Bry sur Marne, FR); Yong Ding (Waban, MA)
Assignees: L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation Des Procedes Georges Claude; Air Liquide Advanced Technologies U.S. LLC
B01D53/229B01D53/002F25J3/061F25J3/063B01D2256/245B01D2257/702F25J2205/80F25J2210/04F25J2230/30F25J2245/02
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Quick Facts
Patent No.
US 11,278,843
App. No.
16/633,212
Granted
Mar 22, 2022
Kind
B2
Abstract

A process for purifying a feed gas including methane and heavy hydrocarbons, including: step a): cooling the feed gas in a heat exchanger; step b): introducing the resulting into a first phase separator to produce a liquid stream depleted in methane and enriched in heavy hydrocarbons and a gas stream; step c): separating the gas stream in a membrane from which a methane-enriched permeate stream and a partially condensed residue stream exit; step d): introducing the residue stream from step c) into a second phase separator vessel in order to produce a liquid stream and a gas stream; step e): introducing at least one portion of the gas stream resulting from step d) into a JT expansion means; and step f): heating at least one portion of the expanded stream in the heat exchanger used in step a) counter-current to the feed stream in order to cool the latter.

Claims (15)

1. A process for purifying a feed gas stream comprising methane and hydrocarbons containing at least two carbon atoms, comprising the following steps:

Step a): cooling the feed gas stream in a heat exchanger;

Step b): introducing the stream resulting from step a) into a first phase separator vessel in order to produce a liquid stream depleted in methane and enriched in hydrocarbons containing more than two carbon atoms and a gas stream;

Step c): separating the gas stream resulting from step b) in a membrane permeation unit from which at least one methane-enriched gaseous permeate stream and one partially condensed residue stream enriched in hydrocarbons containing at least two carbon atoms exit;

Step d): introducing the residue stream resulting from step c) into a second phase separator vessel in order to produce at least two phases including a liquid stream and a gas stream;

Step e): introducing at least one portion of the gas stream resulting from step d) into a Joule-Thomson expansion means;

Step f): heating at least one portion of the expanded stream resulting from step e) by introduction into the heat exchanger used in step a) counter-current to the feed gas stream in order to cool the latter.

2. The process as claimed in claim 1 , wherein the heated stream resulting from step f) is recycled by mixing with the feed gas stream.

3. The process as claimed in claim 1 , wherein at least one portion of the liquid stream resulting from step d) is introduced into the heat exchanger used in step a) counter-current to the feed gas stream.

4. The process as claimed in claim 3 , wherein at least one portion of the liquid stream resulting from step b) is mixed with said at least one portion of the liquid stream resulting from step d) before being introduced into the heat exchanger used in step a) counter-current to the feed gas stream.

5. The process as claimed in claim 1 , wherein at least one portion of the methane-enriched permeate stream resulting from step c) is heated by introduction into the heat exchanger used in step a) counter-current to the feed stream in order to cool the latter.

6. The process as claimed in claim 5 , wherein said at least one portion of the permeate stream resulting from step d) undergoes a Joule-Thomson expansion prior to the introduction thereof into the heat exchanger.

7. The process as claimed in claim 1 , wherein at least one portion of the liquid stream resulting from step d) is introduced into a third phase separator vessel in order to produce at least two phases, including a liquid stream and a gas stream.

8. The process as claimed in claim 7 , wherein said gas stream at the outlet of the third phase separator vessel is mixed with the permeate stream resulting from step c).

9. The process as claimed in claim 7 , wherein the gas stream at the outlet of the third phase separator vessel is heated by introduction into the heat exchanger used in step a) counter-current to the feed stream in order to cool the latter.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 3, 2026
From: AIR LIQUIDE ADVANCED TECHNOLOGIES U.S. LLC
To: L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE
Reel/Frame 076064/0658 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 14, 2021
From: MARTY, PASCAL
To: L'AIR LIQUIDE, SOCIÉTÉ ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCÉDÉS GEORGES CLAUDE
Reel/Frame 054914/0569 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 14, 2021
From: DING, YONG; TERRIEN, PAUL
To: AIR LIQUIDE ADVANCED TECHNOLOGIES U.S. LLC
Reel/Frame 054915/0232 →
Priority Claims (1)
FR 1757155 · Jul 27, 2017 · national
Continuity (1)
Related Publication 20200188844A1 · Jun 18, 2020