IP Library › Granted Patent US 11,286,426
Granted Patent B2
US 11,286,426 · App. 16/479,263 · Granted Mar 29, 2022

Biogenic low viscosity insulating oil

Inventor: Per Wiklund (Stockholm, SE)
Assignees: NESTE OYJ; AVANTHERM AB
C10G7/00C09K5/10C09K15/08C11B3/12H01B3/22C10G2300/1011C10G2300/80C10G2400/12
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Quick Facts
Patent No.
US 11,286,426
App. No.
16/479,263
Granted
Mar 29, 2022
Kind
B2
Abstract

A method of producing a non-petroleum based electrical insulating oil, wherein the method can include providing a primary mixture of non-petroleum origin, containing isomerized straight chain hydrocarbons; performing a distillation and/or stripping of the primary mixture; collecting a paraffinic base oil as a product of the distillation and/or stripping, containing a mixture of isoalkanes and alkanes; and mixing the base oil with an antioxidant additive.

Claims (44)

1. A method of producing a non-petroleum based electrical insulating oil, the method comprising:

providing a primary mixture of non-petroleum origin, containing isomerized straight chain hydrocarbons in a range of C 10 -C 20 ;

performing a distillation and/or stripping of the primary mixture;

collecting a paraffinic base oil as a product of the distillation and/or stripping, containing a mixture of isoalkanes and alkanes in a range of C 14 -C 20 ;

mixing the paraffinic base oil with an antioxidant additive;

repeatedly taking a sample of a product of the distillation and/or stripping; and

controlling collection of the paraffinic base oil in such a way that:

collection of the product of distillation or stripping is started when a flash point of the sample is larger than 135° C. and lower than or equal to 160° C. measured by closed cup, Pensky-Marten; and

the collection of the product of distillation or stripping is ended when a kinematic viscosity of the sample at 40° C. falls within a range of 3.4 to 4.5 mm 2 /s.

2. The method according to claim 1 , wherein the said kinematic viscosity at 40° C. is selected to fall within a range of 3.6 to 3.9 mm 2 /s, or to be about 3.8 mm 2 /s.

3. The method according to claim 1 , wherein the flash point is selected to be larger than 135° C. and lower than or equal to 155° C., or lower than or equal to 150° C., or lower than or equal to 145° C.

4. The method according to claim 1 , wherein the primary mixture comprises:

isomerized straight chain hydrocarbons selected to be in a range of at least one of C 11 -C 20 , C 11 -C 19 , C 12 -C 19 , or C 12 -C 18 .

5. The method according to claim 1 , wherein the paraffinic base oil comprises:

a mixture of isoalkanes and alkanes selected to be in a range of C 15 -C 19 or C 16 -C 18 .

6. The method according to claim 1 , wherein the antioxidant additive is selected to be in an amount of up to 0.4% by weight, up to 0.3% by weight, or up about to 0.24% by weight.

7. The method according to claim 1 , wherein the antioxidant additive is butylated hydroxytoluene (BHT).

8. The method according to claim 1 , comprising:

mixing the paraffinic base oil with a gassing tendency lowering additive.

9. The method according to claim 1 , wherein the primary mixture comprises:

isomerised straight chain hydrocarbons of fatty acid origin.

10. A non-petroleum based electrical insulating oil manufactured according to the method according to claim 1 .

11. The method according to claim 1 , comprising:

applying the a non-petroleum based electrical insulating oil for cooling of at least one electronic circuit, processor, electronic component, electric transformer, electric shunt reactor, or electric switch gear.

12. A method of producing a non-petroleum based electrical insulating oil, the method comprising:

providing a primary mixture of non-petroleum origin, containing isomerized straight chain hydrocarbons in a range of C 10 -C 20 ;

performing a distillation of the primary mixture;

collecting a paraffinic base oil as a product of the distillation, containing a mixture of isoalkanes and alkanes in a range of C 14 -C 20 ;

mixing the paraffinic base oil with an antioxidant additive;

controlling collection of the paraffinic base oil in such a way that:

an initial boiling point of a distillation cut is chosen so that a flash point is larger than 135° C. and lower than or equal to 160° C. measured by closed cup, Pensky-Marten; and

a final boiling point of the distillation cut is chosen so that a kinematic viscosity of the paraffinic base oil at 40° C. falls within a range of 3.4 to 4.5 mm 2 /s.

13. The method according to claim 12 , wherein the said kinematic viscosity at 40° C. is selected to fall within a range of 3.6 to 3.9 mm 2 /s, or to be about 3.8 mm 2 /s.

14. The method according to claim 12 , wherein the flash point is selected to be larger than 135° C. and lower than or equal to 155° C., or lower than or equal to 150° C., or lower than or equal to 145° C.

15. The method according to claim 12 , wherein the primary mixture comprises:

isomerized straight chain hydrocarbons selected to be in a range of at least one of C 11 -C 20 , C 11 -C 19 , C 12 -C 19 , or C 12 -C 18 .

16. The method according to claim 12 , wherein the paraffinic base oil comprises:

a mixture of isoalkanes and alkanes selected to be in a range of C 15 -C 19 or C 16 -C 18 .

17. The method according to claim 12 , wherein the antioxidant additive is selected to be in an amount of up to 0.4% by weight, up to 0.3% by weight, or up about to 0.24% by weight.

18. The method according to claim 12 , wherein the antioxidant additive is butylated hydroxytoluene (BHT).

19. The method according to claim 12 , comprising:

mixing the paraffinic base oil with a gassing tendency lowering additive.

20. The method according to claim 12 , wherein the primary mixture comprises:

isomerised straight chain hydrocarbons of fatty acid origin.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 13, 2019
From: WIKLUND, PER
To: NESTE OYJ; AVANTHERM AB
Reel/Frame 050368/0198 →
Priority Claims (2)
SE 1750058-8 · Jan 24, 2017 · national
EP 17165805 · Apr 10, 2017 · regional
Continuity (1)
Related Publication 20190382666A1 · Dec 19, 2019