IP Library Granted Patent US 11,291,233
Granted Patent B2
US 11,291,233 · App. 16/440,253 · Granted Apr 5, 2022

Compositions and methods for improving rebaudioside M solubility

Inventors: Indra Prakash (Alpharetta, GA); Gil Ma (Atlanta, GA); Avetik Markosyan (Kuala Lumpur, MY); Youlung Chen (Marietta, GA)
Assignee: The Coca-Cola Company
A23L27/36A23L2/60A23L27/30A23V2002/00
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Quick Facts
Patent No.
US 11,291,233
App. No.
16/440,253
Granted
Apr 5, 2022
Kind
B2
Abstract

Rebaudioside M compositions with improved aqueous solubility and methods for preparing the same are provided herein. The rebaudioside M compositions include (i) disordered crystalline compositions comprising rebaudioside M and rebaudioside D, (ii) spray-dried compositions comprising rebaudioside M, rebaudioside D and steviol glycoside mixtures and/or rebaudioside B and/or NSF-02, (iii) spray-dried compositions comprising rebaudioside M, rebaudioside D and at least one surfactant, polymer, saponin, carbohydrate, polyol, preservative or a combination thereof. Sweetened compositions, such a beverages, containing the rebaudioside M compositions with improved water solubility are also provided herein.

Claims (17)

1. A beverage comprising a composition comprising (i) rebaudioside M, (ii) rebaudioside D and (iii) a substance selected from the group consisting of a second steviol glycoside mixture, rebaudioside B, glucosylated steviol glycosides and a combination thereof, wherein

a. rebaudioside M and rebaudioside D are provided as a first steviol glycoside mixture, wherein rebaudioside M is present in the first steviol glycoside mixture in an amount from about 75% to about 90% by weight and rebaudioside D is present in the first steviol glycoside mixture in an amount from about 5% to about 25% by weight;

b. the composition is spray-dried prior to dissolution in the beverage; and

c. the composition has a water solubility of about 0.3% (w/v) or greater.

2. The beverage of claim 1 , wherein the beverage is selected from a mid-calorie, low-calorie and zero-calorie beverage.

3. The beverage of claim 1 , wherein the beverage is a carbonated beverage.

4. The beverage of claim 3 , wherein the carbonated beverage is selected from the group consisting of a cola, lemon-lime flavored sparkling beverage, orange-flavored sparkling beverage, grape-flavored sparkling beverage, strawberry-flavored sparkling beverage, pineapple-flavored sparkling beverage, ginger ale, soft drink, root beer and malt beverage.

5. The beverage of claim 1 , wherein the beverage is a non-carbonated beverage.

6. The beverage of claim 5 , wherein the non-carbonated beverage is selected form the group consisting of a fruit juice, fruit-flavored juice, juice drink, nectar, vegetable juice, vegetable-flavored juice, sports drink, energy drink, enhanced water, enhanced water with vitamins, near water drink, coconut water, tea, coffee, cocoa drink, beverage containing milk component, beverage containing cereal extract and smoothie.

7. The beverage of claim 1 , wherein rebaudioside M s present in the first steviol glycoside mixture in an amount from about 80% to about 85% by weight and rebaudioside D is present in the first steviol glycoside mixture in an amount from about 10% to about 15% by weight.

8. The beverage of claim 1 , wherein the second steviol glycoside mixture comprises at least about 50% rebaudioside A by weight.

9. The beverage of claim 1 , wherein the second steviol glycoside mixture comprises from about 1% to about 30% rebaudioside B by weight.

10. The beverage of claim 1 , wherein the weight ratio of (i) rebaudioside M and rebaudioside D to (ii) rebaudioside B is from about 20:1 to about 5:1.

11. The beverage of claim 1 , wherein the weight ratio of (i) rebaudioside M and rebaudioside D to (ii) the second steviol glycoside mixtures is from about 20:1 to about 5:1.

12. The beverage of claim 1 , wherein the weight ratio of (i) rebaudioside M and rebaudioside D to (ii) the glucosylated steviol glycosides is from about 20:1 to about 5:1.

13. The beverage of claim 1 , wherein the composition has a water solubility of about 0.5% (w/v) or greater.

14. The beverage of claim 1 , wherein the composition has a water solubility of about 1.0% (w/v) or greater.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 5, 2019
From: MARKOSYAN, AVETIK
To: PURECIRCLE SDN BHD
Reel/Frame 051201/0898 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 5, 2019
From: PRAKASH, INDRA; MA, GIL; CHEN, YOULUNG
To: THE COCA-COLA COMPANY
Reel/Frame 051853/0688 →
Continuity (4)
Continuation 15395457 · Dec 30, 2016
Continuation 14046514 · Oct 4, 2013
Provisional Application 61845817 · Jul 12, 2013
Related Publication 20200015505A1 · Jan 16, 2020
Cited By (3)
US 12,264,176 US 12,550,923 US 12,590,116