IP Library › Granted Patent US 11,313,029
Granted Patent B2
US 11,313,029 · App. 16/842,896 · Granted Apr 26, 2022

Potassium sodium niobate sputtering target

Inventors: Ryosuke Sakashita (Ibaraki, JP); Yoshitaka Shibuya (Ibaraki, JP)
Assignee: JX NIPPON MINING & METALS CORPORATION
C23C14/088C23C14/3407H01J37/3426H01L41/1873H01L41/316
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Quick Facts
Patent No.
US 11,313,029
App. No.
16/842,896
Granted
Apr 26, 2022
Kind
B2
Abstract

A sputtering target formed from a potassium sodium niobate sintered body to which a dopant has been added; as a dopant, the sputtering target includes one or more types among Li, Mg, Ca, Sr, Ba, Bi, Sb, V, In, Ta, Mo, W, Cr, Ti, Zr, Hf, Sc, Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Cu, Zn, Ag, Mn, Fe, Co, Ni, Al, Si, Ge, Sn, and Ga; and a variation coefficient of a dopant concentration in a plane of the sputtering target is 0.12 or less. In terms of suppressing the generation of particles, provided is a sputtering target which is formed from a sintered body that includes potassium sodium niobate and to which a dopant has been added.

Claims (18)

1. A sputtering target formed from a potassium sodium niobate sintered body to which a dopant has been added, wherein the dopant contained is one or more types among Li, Mg, Ca, Sr, Ba, Bi, Sb, V, In, Ta, Mo, W, Cr, Ti, Zr, Hf, Sc, Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Cu, Zn, Ag, Mn, Fe, Co, Ni, Al, Si, Ge, Sn, and Ga; and wherein a variation coefficient of a dopant concentration in a plane of the sputtering target is 0.12 or less.

2. The sputtering target according to claim 1 , wherein a variation coefficient of a K/Na composition ratio in a plane of the sputtering target is 0.12 or less.

3. The sputtering target according to claim 2 , wherein a relative density is 60% or higher.

4. The sputtering target according to claim 2 , wherein a relative density is 70% or higher.

5. The sputtering target according to claim 2 , wherein a relative density is 80% or higher.

6. The sputtering target according to claim 5 , wherein a flexural strength is 10 MPa or more.

7. The sputtering target according to claim 6 , wherein an average crystal grain size is 1 to 20 μm.

8. The sputtering target according to claim 7 , wherein a content of carbon as a gas component is 1000 wtppm or less.

9. The sputtering target according to claim 8 , wherein a content ratio of niobium (Nb), potassium (K), and sodium (Na) is, in terms of atomic ratio, Nb:K:Na=1.0:X:1−X, where 0.3≤X<1.0.

10. The sputtering target according to claim 9 , wherein a total content of the dopant is 0.04 at % to 4 at %.

11. The sputtering target according to claim 1 , wherein a relative density is 60% or higher.

12. The sputtering target according to claim 1 , wherein a relative density is 70% or higher.

13. The sputtering target according to claim 1 , wherein a relative density is 80% or higher.

14. The sputtering target according to claim 1 , wherein a flexural strength is 10 MPa or more.

15. The sputtering target according to claim 1 , wherein an average crystal grain size is 1 to 20 μm.

16. The sputtering target according to claim 1 , wherein a content of carbon as a gas component is 1000 wtppm or less.

17. The sputtering target according to claim 1 , wherein a content ratio of niobium (Nb), potassium (K), and sodium (Na) is, in terms of atomic ratio, Nb:K:Na=1.0:X:1−X, where 0.3≤X<1.0.

18. The sputtering target according to claim 1 , wherein a total content of the dopant is 0.04 at % to 4 at %.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 8, 2020
From: SAKASHITA, RYOSUKE; SHIBUYA, YOSHITAKA
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 052339/0952 →
Priority Claims (2)
JP JP2019-085350 · Apr 26, 2019 · national
JP JP2019-166017 · Sep 12, 2019 · national
Continuity (1)
Related Publication 20200340096A1 · Oct 29, 2020