IP Library › Granted Patent US 11,332,388
Granted Patent B2
US 11,332,388 · App. 16/999,687 · Granted May 17, 2022

Removal of selenium from water with kaolinite

Inventors: Mingming Fang (Naperville, IL); Heng Wang (Hoffman Estates, IL)
Assignee: Fuel Tech, Inc.
C02F1/281B01J20/12C02F2101/106
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Quick Facts
Patent No.
US 11,332,388
App. No.
16/999,687
Granted
May 17, 2022
Kind
B2
Abstract

The description relates to a composition and a method for reducing the concentration of selenium in water. Contaminated water is contacted with a kaolinite clay characterized by a removal efficiency for selenatearsenate of at least 40 wt % at ambient temperature. The adsorption process is fast. Following sufficient contact, the water is separated from the kaolinite clay. In a preferred form, the kaolinite clay has high surface acidity.

Claims (14)

1. A composition for removing selenium from contaminated water comprises:

a) a kaolinite clay selected from the group consisting of kaolinite, nacrite, halloysite, dickite, and odinite, wherein the kaolinite clay has a surface acidity such that the pH of its slurry in water is less than 6 at 1 weight %;

b) a water phase with pH in the range of 4 to 9,

wherein the kaolinite dosage to the volume of the contaminated water is in the range from about 1 to about 20 g/liter.

2. The composition of claim 1 , wherein the clay is kaolinite.

3. The composition of claim 1 , wherein the kaolinite clay has a surface acidity such that the pH of its slurry in water is less than 5 at 1 weight %.

4. A composition according to claim 1 in unit dosage form for treating a volume of contaminated water, the kaolinite dosage to the volume of the contaminated water is in the range from about 5 to about 15 g/liter of contaminated water.

5. A method for removing selenium from contaminated water which comprises contacting the contaminated water with:

a) a kaolinite clay selected from the group consisting of kaolinite, nacrite, halloysite, dickite, and odinite, wherein the kaolinite clay has a surface acidity such that the pH of its slurry in water is less than 6 at 1 weight %;

b) a water phase with pH in the range of 4 to 9,

wherein the kaolinite dosage to the volume of the contaminated water is in the range from about 1 to about 20 g/liter.

6. The method of claim 5 , wherein the clay is kaolinite.

7. The method of claim 5 , wherein the kaolinite clay has a surface acidity such that the pH of its slurry in water is less than 5 at 1 weight %.

8. A method according to claim 5 in unit dosage form for treating a volume of contaminated water, the kaolinite dosage to the volume of the contaminated water is in the range from about 5 to about 15 g/liter of contaminated water.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 25, 2020
From: FANG, MINGMING; WANG, HENG
To: FUEL TECH, INC.
Reel/Frame 053585/0504 →
Continuity (2)
Provisional Application 62890111 · Aug 22, 2019
Related Publication 20210053845A1 · Feb 25, 2021