IP Library › Granted Patent US 11,352,348
Granted Patent B2
US 11,352,348 · App. 17/247,117 · Granted Jun 7, 2022

Splicing modulator antibody-drug conjugates and methods of use

Inventors: Ermira Pazolli (Wayland, MA); Silvia Buonamici (Boston, MA); Thiwanka Samarakoon (Westwood, MA); Sudeep Prajapati (Somerville, MA); Nathan Fishkin (Weymouth, MA); James Palacino (Wellesley, MA); Michael Seiler (Belmont, MA); Ping Zhu (Acton, MA); Andrew Cook (Stow, MA); Peter Smith (Arlington, MA); Xiang Liu (Winchester, MA); Shelby Ellery (Boston, MA); Dominic Reynolds (Stoneham, MA); Lihua Yu (Acton, MA); Zhenhua Wu (Belmont, MA); Shouyong Peng (Belmont, MA); Nicholas Calandra (Boston, MA); Megan Sheehan (Allston, MA); Yonghong Xiao (Belmont, MA)
Assignee: EISAI R&D MANAGEMENT CO., LTD.
C07D405/12A61K9/127A61K9/51A61K31/365A61K31/496A61K39/0011A61K39/3955A61K39/39558A61K45/06A61K47/60A61K47/6845A61K47/6849A61K47/6851A61K47/6857A61K47/6869A61K47/6871A61K47/6889A61P35/00C07D313/00C07D405/06C07K16/24C07K16/28C07K16/2803C07K16/2818C07K16/2827C07K16/2896C07K16/3007C07K16/3092C07K16/32C07K16/40C12Q1/6886G01N33/5011G01N33/574A61K2039/505A61K2039/53A61K2039/545C07K2317/565C07K2317/76C12Q2600/106G01N2500/10
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Quick Facts
Patent No.
US 11,352,348
App. No.
17/247,117
Granted
Jun 7, 2022
Kind
B2
Abstract

Linker-drug compounds and antibody-drug conjugates that bind to human oncology targets are disclosed. The linker-drug compounds and antibody-drug conjugates comprise a splicing modulator drug moiety. The disclosure further relates to methods and compositions for use in the treatment of neoplastic disorders by administering the antibody-drug conjugates provided herein. In an embodiment, the splicing modulator comprises a pladienolide or a pladienolide derivative.

Claims (95)

1. A compound of Formula (III):

or a pharmaceutically acceptable salt thereof,

wherein:

R 1 is chosen from absent, hydrogen, C 1 -C 6 alkyl groups, C 1 -C 6 alkylalkoxy groups, C 1 -C 6 alkylamino groups, C 1 -C 6 alkylcarboxylic acid groups, C 1 -C 6 alkylhydroxy groups, C 3 -C 8 cycloalkyl groups, benzyl groups, C 3 -C 8 heterocyclyl groups, —O—C(═O)—(C 1 -C 6 alkyl) groups, and —CD 3 ;

R 2 is a linker L comprising at least one cleavable peptide moiety;

R 3 is chosen from hydrogen, C 1 -C 6 alkyl groups, C 1 -C 6 alkylalkoxy groups, C 1 -C 6 alkylamino groups, C 1 -C 6 alkylcarboxylic acid groups, C 1 -C 6 alkylhydroxy groups, C 3 -C 8 cycloalkyl groups, benzyl groups, C 3 -C 8 heterocyclyl groups, and —O—C(═O)—(C 1 -C 6 alkyl) groups;

R 4 , R 5 , and R 8 are each independently chosen from hydrogen, hydroxyl groups, —O—(C 1 -C 6 alkyl) groups, —O—C(═O)—(C 1 -C 6 alkyl) groups, and C 1 -C 6 alkyl groups;

R 6 and R 7 are each independently chosen from hydrogen, —O—R 17 , —O—C(═O)—R 17 , —O—C(═O)—NR 15 R 16 , C 1 -C 6 alkyl groups, and —NR 15 R 16 ;

R 15 and R 16 are each independently chosen from hydrogen, R 17 , —C(═O)—R 17 , and —C(═O)—O—R 17 ;

R 17 is chosen from hydrogen, C 1 -C 6 alkyl groups, C 3 -C 8 cycloalkyl groups, benzyl groups, and C 3 -C 8 heterocyclyl groups; and

Z″ is chosen from

wherein R 1 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 , R 15 , R 16 , and R 17 are each independently substituted with 0 to 3 groups independently chosen from halogens, hydroxyl groups, C 1 -C 6 alkyl groups, —O—(C 1 -C 6 alkyl) groups, —NR 15 R 16 , C 3 -C 8 cycloalkyl groups, C 1 -C 6 alkylhydroxy groups, C 1 -C 6 alkylalkoxy groups, benzyl groups, and C 3 -C 8 heterocyclyl groups;

wherein at least one of R 6 and R 7 is hydrogen; and

wherein if Z″ is

and R 3 , R 6 , and R 7 are H and R 4 is methoxy and R 5 is hydroxyl, then R 1 is neither absent nor methyl.

2. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein:

R 1 is chosen from absent, hydrogen, C 1 -C 4 alkyl groups, C 1 -C 4 alkylcarboxylic acid groups, C 1 -C 4 alkylhydroxy groups, and C 3 -C 8 cycloalkyl groups;

R 2 is a linker L comprising at least one cleavable peptide moiety;

R 3 is chosen from hydrogen, C 1 -C 4 alkyl groups, C 1 -C 4 alkylalkoxy groups, C 1 -C 4 alkylcarboxylic acid groups, and C 1 -C 4 alkylhydroxy groups;

R 4 is chosen from hydrogen, hydroxyl groups, —O—(C 1 -C 4 alkyl) groups, —O—C(═O)—(C 1 -C 4 alkyl) groups, and C 1 -C 4 alkyl groups;

R 5 is chosen from hydrogen, hydroxyl groups, —O—(C 1 -C 4 alkyl) groups, and C 1 -C 4 alkyl groups;

R 6 is chosen from hydrogen, —O—R 17 , —O—C(═O)—R 17 , and C 1 -C 4 alkyl groups;

R 7 is chosen from hydrogen, —O—R 17 , —O—C(═O)—R 17 , —O—C(═O)—NR 15 R 16 , C 1 -C 6 alkyl groups, and —NR 15 R 16 ;

R 8 is chosen from hydrogen, hydroxyl groups, —O—(C 1 -C 4 alkyl) groups, and C 1 -C 4 alkyl groups;

R 15 and R 16 are each independently chosen from hydrogen, R 17 , —C(═O)—R 17 , and —C(═O)—O—R 17 ;

R 17 is chosen from hydrogen, C 1 -C 6 alkyl groups, C 3 -C 8 cycloalkyl groups, benzyl groups, and C 3 -C 8 heterocyclyl groups;

Z″ is chosen from

wherein R 1 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 , R 15 , R 16 , and R 17 are each independently substituted with 0 to 3 groups independently chosen from halogens, hydroxyl groups, C 1 -C 6 alkyl groups, —O—(C 1 -C 6 alkyl) groups, —NR 15 R 16 , C 3 -C 8 cycloalkyl groups, C 1 -C 6 alkylhydroxy groups, C 1 -C 6 alkylalkoxy groups, benzyl groups, and C 3 -C 8 heterocyclyl groups;

wherein at least one of R 6 and R 7 is hydrogen; and

wherein if Z″ is

and R 3 , R 6 , and R 7 are H and R 4 is methoxy and R 5 is hydroxyl, then R 1 is neither absent nor methyl.

3. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein:

R 1 is chosen from absent, hydrogen, methyl, and C 1 -C 4 alkylcarboxylic acid groups;

R 2 is a linker L comprising at least one cleavable peptide moiety;

R 3 is chosen from hydrogen and C 1 -C 4 alkylcarboxylic acid groups;

R 4 is chosen from hydrogen, hydroxyl groups, —O—(C 1 -C 4 alkyl) groups, —O—C(═O)—(C 1 -C 4 alkyl) groups, and C 1 -C 4 alkyl groups;

R 5 is chosen from hydrogen and hydroxyl groups;

R 6 is hydrogen;

R 7 is hydrogen;

R 8 is chosen from hydrogen and hydroxyl groups; and

Z″ is chosen from

wherein R 1 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 are each independently substituted with 0 to 3 groups independently chosen from halogens, hydroxyl groups, C 1 -C 6 alkyl groups, —O—(C 1 -C 6 alkyl) groups, C 3 -C 8 cycloalkyl groups, C 1 -C 6 alkylhydroxy groups, C 1 -C 6 alkylalkoxy groups, benzyl groups, and C 3 -C 8 heterocyclyl groups; and

wherein if R 3 , R 6 , and R 7 are H and R 4 is methoxy and R 5 is hydroxyl, then R 1 is neither absent nor methyl.

4. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

5. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

6. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

7. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

8. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

9. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

10. A pharmaceutical composition comprising the compound of claim 1 , or a pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier.

11. A method of treating a subject having or suspected of having a neoplastic disorder, comprising administering to the subject a therapeutically effective amount of the compound of claim 1 .

12. The method of claim 11 , wherein the neoplastic disorder is a leukemia, a lymphoma, or a myeloma.

13. The method of claim 12 , wherein the myeloma is multiple myeloma.

14. A method of reducing or inhibiting growth of a tumor in a subject having or suspected of having a neoplastic disorder, comprising administering to the subject a therapeutically effective amount of the compound of claim 1 .

15. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

16. The compound of claim 1 , wherein the compound is chosen from a compound of formula

and

pharmaceutically acceptable salts thereof.

17. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the linker L comprising at least one cleavable peptide moiety further comprises at least one spacer unit.

18. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the at least one cleavable peptide moiety comprises valine-alanine (Val-Ala).

19. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the at least one cleavable peptide moiety comprises valine-citrulline (Val-Cit), glutamic acid-valine-citrulline (Glu-Val-Cit), or alanine-alanine-asparagine (Ala-Ala-Asn).

20. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the linker L comprising at least one cleavable peptide moiety comprises p-aminobenzyloxycarbonyl.

21. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the linker L comprising at least one cleavable peptide moiety further comprises a polyethylene glycol moiety and/or an alkyl moiety.

22. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the linker L comprising at least one cleavable peptide moiety further comprises maleimidocaproyl (MC).

23. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the linker L comprising at least one cleavable peptide moiety is a compound of formula:

24. The compound of claim 1 or a pharmaceutically acceptable salt thereof, wherein the linker L comprising at least one cleavable peptide moiety is a compound of formula:

25. A compound of formula:

or

a pharmaceutically acceptable salt thereof,

wherein:

R 1 is chosen from absent, hydrogen, C 1 -C 6 alkyl groups, C 1 -C 6 alkylalkoxy groups, C 1 -C 6 alkylamino groups, C 1 -C 6 alkylcarboxylic acid groups, C 1 -C 6 alkylhydroxy groups, C 3 -C 8 cycloalkyl groups, benzyl groups, C 3 -C 8 heterocyclyl groups, —O—C(═O)—(C 1 -C 6 alkyl) groups, and —CD 3 ;

R 2 is a linker L comprising at least one cleavable peptide moiety;

R 3 is chosen from hydrogen, C 1 -C 6 alkyl groups, C 1 -C 6 alkylalkoxy groups, C 1 -C 6 alkylamino groups, C 1 -C 6 alkylcarboxylic acid groups, C 1 -C 6 alkylhydroxy groups, C 3 -C 8 cycloalkyl groups, benzyl groups, C 3 -C 8 heterocyclyl groups, and —O—C(═O)—(C 1 -C 6 alkyl) groups;

R 4 is chosen from hydrogen, hydroxyl groups, —O—C(═O)—(C 1 -C 6 alkyl) groups, and C 1 -C 6 alkyl groups;

R 5 and R 8 are each independently chosen from hydrogen, hydroxyl groups, —O—(C 1 -C 6 alkyl) groups, —O—C(═O)—(C 1 -C 6 alkyl) groups, and C 1 -C 6 alkyl groups;

R 6 and R 7 are each independently chosen from hydrogen, —O—R 17 , —O—C(═O)—R 17 , —O—C(═O)—NR 15 R 16 , C 1 -C 6 alkyl groups, and —NR 15 R 16 ;

R 15 and R 16 are each independently chosen from hydrogen, R 17 , —C(═O)—R 17 , and —C(═O)—O—R 17 ;

R 17 is chosen from hydrogen, C 1 -C 6 alkyl groups, C 3 -C 8 cycloalkyl groups, benzyl groups, and C 3 -C 8 heterocyclyl groups; and

Z″ is chosen from

wherein R 1 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 , R 15 , R 16 , and R 17 are each independently substituted with 0 to 3 groups independently chosen from halogens, hydroxyl groups, C 1 -C 6 alkyl groups, —O—(C 1 -C 6 alkyl) groups, —NR 15 R 16 , C 3 -C 8 cycloalkyl groups, C 1 -C 6 alkylhydroxy groups, C 1 -C 6 alkylalkoxy groups, benzyl groups, and C 3 -C 8 heterocyclyl groups;

wherein at least one of R 6 and R 7 is hydrogen.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2020
From: PAZOLLI, ERMIRA; SAMARAKOON, THIWANKA; PRAJAPATI, SUDEEP; FISHKIN, NATHAN; PALACINO, JAMES; SEILER, MICHAEL; ZHU, PING; COOK, ANDREW; SMITH, PETER; LIU, XIANG; ELLERY, SHELBY; REYNOLDS, DOMINIC; YU, LIHUA; WU, ZHENHUA; PENG, SHOUYONG; CALANDRA, NICHOLAS; SHEEHAN, MEGAN; XIAO, YONGHONG
To: EISAI R&D MANAGEMENT CO., LTD.
Reel/Frame 054496/0494 →
Continuity (5)
Continuation PCTUS2019035015 · May 31, 2019
Provisional Application 62679631 · Jun 1, 2018
Provisional Application 62679672 · Jun 1, 2018
Provisional Application 62779324 · Dec 13, 2018
Related Publication 20210101888A1 · Apr 8, 2021
Cited By (1)
US 12,514,926