IP Library › Granted Patent US 11,371,132
Granted Patent B2
US 11,371,132 · App. 16/764,756 · Granted Jun 28, 2022

Nitrided part

Inventors: Takahide Umehara (Tokyo, JP); Masato Yuya (Tokyo, JP)
Assignee: NIPPON STEEL CORPORATION
C23C8/26C22C38/001C22C38/002C22C38/008C22C38/02C22C38/06C22C38/18C22C38/32C22C38/38C22C38/42C22C38/44C22C38/46C22C38/48C22C38/50
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Quick Facts
Patent No.
US 11,371,132
App. No.
16/764,756
Granted
Jun 28, 2022
Kind
B2
Abstract

The present invention has as its technical problem the provision of a part excellent in contact fatigue strength or wear resistance in addition to the rotating bending fatigue strength. In the present invention, the contents of the constituents of the steel, in particular C, Mn, Cr, V, and Mo, are adjusted in accordance with the targeted properties and nitrided parts are prepared while controlling the nitriding potential.

Claims (35)

1. A nitrided part comprising

a steel core containing, by mass %,

C: 0.05 to 0.35%,

Si: 0.05 to 1.50%,

Mn: 0.20 to 2.50%,

P: 0.025% or less,

S: 0.050% or less,

Cr: 0.50 to 2.50%,

V: 0.05 to 1.30%,

Al: 0.050% or less,

N: 0.0250% or less,

Mo: 0 to 1.50%,

Cu: 0 to 0.50%,

Ni: 0 to 0.50%,

Nb: 0 to 0.100%,

Ti: 0 to 0.050%,

B: 0 to 0.0100%,

Ca: 0 to 0.0100%,

Pb: 0 to 0.50%,

Bi: 0 to 0.50%,

In: 0 to 0.20%,

Sn: 0 to 0.100%, and

a balance of Fe and impurities,

a nitrogen diffusion layer formed on the steel core, and

a compound layer formed on the nitrogen diffusion layer, 90% or more of elements included in the compound layer being nitrogen and iron, the compound layer having a thickness of 5 to 15 μm, wherein

in a cross-section perpendicular to a surface of the compound layer, a pore area ratio in a range from the surface to a depth of 3 μm from the surface is 10% or less,

if defining the X determined based on the contents of C, Mn, Cr, V, and Mo at the steel core as

X=−2.1×C+0.04×Mn+0.5×Cr+1.8×V−1.5×Mo,

(i) 0≤X≤0.25 and an area ratio of γ′ phases of the nitride iron in the compound layer is 50% or more and 80% or less or

(ii) 0.25≤X≤0.50 and an area ratio of γ′ phases of the nitride iron in the compound layer is 80% or more, wherein

the pore area ratio is measured by a scanning electron microscope, the ratio of the total area of the pores in the area of 90 μm 2 of a range of 3 μm depth from the surfacemost layer being found by analysis using an image processing application, the average value of 10 fields measured being defined as the pore area ratio; and

the area ratio of the γ′ phases is found by image processing structural photographs, by using electron back scatter diffraction (EBSD), 10 structural photographs of cross-sections of 90 μm 2 perpendicular to the surface at the nitrided part surface layer photographed at 4000× being examined to differentiate the γ′ phases and ε phases in the compound layer, the area ratios of the γ′ phases in the compound layer being found by binarization by image processing, the average value of the area ratios of the γ′ phases of the 10 fields measured being defined as the area ratio of the γ′ phases.

2. The nitrided part according to claim 1 , wherein 0≤X≤0.25 and an area ratio of the γ′ phase of the nitride iron in the compound layer is 50% or more and 80% or less.

3. The nitrided part according to claim 1 , wherein 0.25≤X≤0.50 and an area ratio of the γ′ phase of the nitride iron in the compound layer is 80% or more.

4. The nitrided part according to claim 3 , wherein the area ratio of the γ′ phase of the nitride iron in the compound layer is 90% or less.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: UMEHARA, TAKAHIDE; YUYA, MASATO
To: NIPPON STEEL CORPORATION
Reel/Frame 052686/0365 →
Priority Claims (2)
JP JP2017-220885 · Nov 16, 2017 · national
JP JP2017-220894 · Nov 16, 2017 · national
Continuity (1)
Related Publication 20200362447A1 · Nov 19, 2020
Cited By (1)
US 12,655,820