IP Library › Granted Patent US 11,377,729
Granted Patent B2
US 11,377,729 · App. 16/956,080 · Granted Jul 5, 2022

Post-processing method for improving anti-wear and friction-reducing properties of CrN coating

Inventors: Yongxin Wang (Zhejiang, CN); Zechao Li (Zhejiang, CN); Jingwen Zhang (Zhejiang, CN); Zhixiang Zeng (Zhejiang, CN); Jinlong Li (Zhejiang, CN); Xia Lu (Zhejiang, CN); Liping Wang (Zhejiang, CN)
Assignee: NINGBO INSTITUTE OF MATERIALS TECHNOLOGY & ENGINEERING, CHINESE ACADEMY OF SCIENCES
C23C14/5806C23C14/0641C23C14/32
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Quick Facts
Patent No.
US 11,377,729
App. No.
16/956,080
Granted
Jul 5, 2022
Kind
B2
Abstract

Disclosed is a post-processing method for improving anti-wear and friction-reducing properties of a CrN coating. According to the method, the CrN coating is subjected to a thermal cycling treatment in a temperature range of −20° C. to 60° C. under a humidity environment of 60%-80% R.H. The post-processing method can substantially improve the anti-wear and friction-reducing properties of the CrN coating, so that friction pair parts deposited with the coating achieve a stable operation for a long time.

Claims (11)

1. A post-processing method for CrN coating, which comprises: performing a thermal cycle treatment on the CrN coating in a temperature range of −20° C. to 60° C. under a humidity environment of 60% to 80% R.H,

wherein, in the thermal cycle treatment, a single thermal cycle comprises a heating process from −20° C. to 60° C. and a cooling process from 60° C. to −20° C., a single thermal cycle time is 2 h, every 6 single thermal cycles is one period, a constant temperature is maintained between every two periods for 12 h, and the constant temperature has a fluctuation of ±0.5° C.,

in the heating process, a heating rate is 2° C/min and a temperature deviation is less than or equal to ±2° C; and

in the cooling process, a cooling rate is 1° C/min and a temperature deviation is less than or equal to ±2° C.

2. The post-processing method of claim 1 , wherein the humidity has a deviation of less than or equal to ±2% R.H.

3. The post-processing method of claim 1 , wherein the time of the thermal cycle treatment is 7 days.

4. The post-processing method of claim 1 , wherein the thickness of the CrN coating is from 2 μm to 80 μm, and the thickness deviation is less than or equal to 0.5 μm.

5. The post-processing method of claim 1 , wherein the CrN coating is plated on a substrate by a multi-arc ion plating technique, and the substrate is a metal or an alloy.

6. The post-processing method of claim 5 , wherein the substrate is a 316 L stainless steel substrate.

7. The post-processing method of claim 5 , wherein the CrN coating is plated on the substrate by multi-arc ion plating technology for 2 h to 24 h and then subjected to the thermal cycle treatment in the temperature range of −20° C. to 60° C., wherein the temperature deviation is less than or equal to ±2° C.

8. The post-processing method of claim 6 , wherein the CrN coating is plated on the 316 L stainless steel substrate by multi-arc ion plating technology for 2 h to 24 h and then subjected to the thermal cycle treatment in the temperature range of −20° C. to 60° C., wherein the temperature deviation is less than or equal to ±2° C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2020
From: WANG, YONGXIN; LI, ZECHAO; ZHANG, JINGWEN; ZENG, ZHIXIANG; LI, JINLONG; LU, XIA; WANG, LIPING
To: NINGBO INSTITUTE OF MATERIALS TECHNOLOGY & ENGINEERING, CHINESE ACADEMY OF SCIENCES
Reel/Frame 052989/0638 →
Priority Claims (1)
CN 201711397143.0 · Dec 21, 2017 · national
Continuity (1)
Related Publication 20200318232A1 · Oct 8, 2020