IP Library › Granted Patent US 11,390,564
Granted Patent B2
US 11,390,564 · App. 16/713,026 · Granted Jul 19, 2022

Ceramic material and method for preparing the same

Inventors: Enzhu Li (Chengdu, CN); Hongyu Yang (Chengdu, CN); Hongcheng Yang (Chengdu, CN); Yawei Chen (Chengdu, CN); Chaowei Zhong (Chengdu, CN); Shuren Zhang (Chengdu, CN)
Assignee: UNIVERSITY OF ELECTRONIC SCIENCE AND TECHNOLOGY OF CHINA
C04B35/495C04B2235/3232C04B2235/3253C04B2235/3275
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Quick Facts
Patent No.
US 11,390,564
App. No.
16/713,026
Granted
Jul 19, 2022
Kind
B2
Abstract

A ceramic material including Co 0.5 Ti 0.5 TaO 4 . The ceramic material is prepared as follows: 1) weighting and mixing raw powders of Co 2 O 3 , TiO 2 and Ta 2 O 5 proportioned according to the chemical formula of Co 0.5 Ti 0.5 TaO 4 , to yield a mixture; 2) mixing the mixture obtained in 1), zirconia balls, and deionized water according to a mass ratio of 1:4-6:3-6, ball-milling for 6-8 h, drying at 80-120° C., sieving with a 60-200 mesh sieve, calcining in air atmosphere at 800-1100° C. for 3-5 h, to yield powders comprising a main crystalline phase of Co 0.5 Ti 0.5 TaO 4 ; and 3) mixing the powders obtained in 2), zirconia balls, and deionized water according to a mass ratio of 1:3-5:2-4, ball-milling for 4-6 h, and drying at 80-100° C.; adding a 2-5 wt. % of polyvinyl alcohol solution to a resulting product, granulating, sintering resulting granules at 1000-1100° C. in air atmosphere for 4-6 h.

Claims (8)

1. A ceramic material, comprising Co 0.5 Ti 0.5 TaO 4 having a trirutile structure.

2. The ceramic material of claim 1 , wherein the ceramic material is prepared through a method comprising:

1) weighting and mixing raw powders of Co 2 O 3 , TiO 2 and Ta 2 O 5 proportioned according to the chemical formula of CO 0.5 Ti 0.5 TaO 4 , to yield a mixture;

2) mixing the mixture obtained in 1), zirconia balls, and deionized water according to a mass ratio of 1: 4-6: 3-6, ball-milling for 6-8 h, drying at 80-120° C., sieving with a 60-200 mesh sieve, calcining in air atmosphere at 800-1100° C. for 3-5 h, to yield powders comprising a main crystalline phase of Co 0.5 Ti 0.5 TaO 4 ; and

3) mixing the powders obtained in 2), zirconia balls, and deionized water according to a mass ratio of 1: 3-5: 2-4, ball-milling for 4-6 h, and drying at 80-100° C., adding a 2-5 wt. % of polyvinyl alcohol solution to a resulting product, granulating, sintering resulting granules at 1000-1100° C. in air atmosphere for 4-6 h, to yield the ceramic material.

3. The ceramic material of claim 2 , wherein a dielectric constant of the ceramic material is between 36 and 41.

4. The ceramic material of claim 2 , wherein a quality factor (Q×f) of the ceramic material is between 13135 and 17291 GHz.

5. The ceramic material of claim 2 , wherein a temperature coefficient of resonant frequency of the ceramic material is between 113 and 116 ppm/° C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2019
From: LI, ENZHU; YANG, HONGYU; YANG, HONGCHENG; CHEN, YAWEI; ZHONG, CHAOWEI; ZHANG, SHUREN
To: UNIVERSITY OF ELECTRONIC SCIENCE AND TECHNOLOGY OF CHINA
Reel/Frame 051271/0421 →
Priority Claims (1)
CN 201811529803.0 · Dec 14, 2018 · national
Continuity (1)
Related Publication 20200189980A1 · Jun 18, 2020