IP Library Granted Patent US 11,401,616
Granted Patent B2
US 11,401,616 · App. 16/584,806 · Granted Aug 2, 2022

Method for making water sterilization electrodes and device having the same

Inventors: Yuanqing Li (Santa Clara, CA); Bofei Liu (Palo Alto, CA); Sidi Huang (San Jose, CA)
Assignee: EENOTECH, INC.
C25B11/02C02F1/46109C25B11/057B82Y40/00C02F2001/46133C02F2001/46161C02F2303/04
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Quick Facts
Patent No.
US 11,401,616
App. No.
16/584,806
Granted
Aug 2, 2022
Kind
B2
Abstract

The method for forming a water sterilization electrode includes heating a conductive medium to an elevated temperature in a heating apparatus. The method further includes growing oxide nanostructures on the conductive medium at the elevated temperature by supplying one or more oxidizing gases to the heating apparatus. The method further includes ramping down from the elevated temperature at 2-30° C./min to a room temperature to form the water sterilization electrode having the oxide nanostructures on the conductive medium.

Claims (39)

1. A method for forming a water sterilization electrode, the method comprising:

heating a conductive medium to an elevated temperature of about 200-1000° C. in a heating apparatus;

growing oxide nanostructures on the conductive medium at the elevated temperature by supplying one or more oxidizing gases to the heating apparatus; and

ramping down from the elevated temperature at 2-30° C./min to a room temperature to form the water sterilization electrode having the oxide nanostructures on the conductive medium.

2. The method of claim 1 , wherein the heating apparatus includes one of an oven, a furnace, or a heating room.

3. The method of claim 1 , wherein the elevated temperature is about 500-1000° C.

4. The method of claim 1 , wherein the one or more oxidizing gases include at least one of air, moisture, oxygen, or an oxidative gas.

5. The method of claim 1 , wherein the conductive medium includes one of a macro porous or non-porous conductive mesh, foam, film, or sheet.

6. The method of claim 5 , wherein the conductive medium includes one or more of silver, copper, nickel, silicon, or MoS 2 .

7. The method of claim 1 , further comprising: growing the oxide nanostructures on the conductive medium at the elevated temperature for more than 0.5 hours.

8. The method of claim 7 , further comprising: growing the oxide nanostructures on the conductive medium at the elevated temperature for more than one hour.

9. The method of claim 1 , wherein the oxide nanostructures include nanowires having a length of 1-10 micro meters.

10. A water sterilization method, comprising:

providing a conduit including an inlet to receive water and an outlet to discharge water;

providing a water sterilization electrode disposed in the conduit between the inlet and the outlet; and

providing a power source configured to provide power to the water sterilization electrode,

wherein the power source provides to the water sterilization electrode an alternative current power having a voltage greater than 5 volts at a frequency at less than 100 Hz; and

wherein the water sterilization electrode is formed by:

heating a conductive medium to about 200-1000° C. in a heating apparatus;

growing oxide nanostructures on the conductive medium at the elevated temperature by supplying one or more oxidizing gases to the heating apparatus; and

ramping down from the elevated temperature at 2-30° C./min to a room temperature to form the water sterilization electrode having the oxide nanostructures on the conductive medium.

11. The method of claim 10 , wherein the water sterilization electrode includes a conductive medium and oxide nanostructures formed on the conductive medium.

12. The method of claim 11 , wherein the conductive medium includes one of a macro porous or non-porous conductive mesh, foam, film, or sheet.

13. The method of claim 12 , wherein the conductive medium includes one or more of silver, copper, nickel, silicon, or MoS 2 .

14. The method of claim 11 , wherein the oxide nanostructures include nanowires having a length of 1-10 micro meters.

15. The method of claim 11 , wherein the conductive medium includes a copper foam body.

16. The method of claim 15 , wherein the nanostructures include nanowires of CuO.

17. A water sterilization method, comprising:

providing a conduit including an inlet to receive water and an outlet to discharge water;

providing a water sterilization electrode disposed in the conduit between the inlet and the outlet, wherein the water sterilization electrode includes a conductive medium and oxide nanostructures formed on the conductive medium; and

providing a power source configured to provide power to the water sterilization electrode,

wherein the power source provides to the water sterilization electrode an alternative current power; and

wherein the water sterilization electrode is formed by:

heating the conductive medium to about 200-1000° C. in a heating apparatus;

growing the oxide nanostructures on the conductive medium at the elevated temperature by supplying one or more oxidizing gases to the heating apparatus; and

ramping down from the elevated temperature at 2-30° C./min to a room temperature to form the water sterilization electrode having the oxide nanostructures on the conductive medium.

18. The method of claim 17 , wherein the conductive medium includes one of a macro porous or non-porous conductive mesh, foam, film, or sheet.

19. The method of claim 17 , wherein the oxide nanostructures formed on the conductive medium include an oxide of the conductive medium.

20. The method of claim 17 , wherein the conductive medium includes one or more of silver, copper, nickel, silicon, or MoS 2 .

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE NAME PREVIOUSLY RECORDED AT REEL: 060836 FRAME: 0426. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT . Recorded Oct 12, 2022
From: EENOTECH GROUP, INC.
To: ENNOPURE, INC.
Reel/Frame 061660/0949 →
MERGER AND CHANGE OF NAME Recorded Aug 17, 2022
From: EENOTECH, INC.; EENOTECH GROUP, INC.
To: EENOTECH GROUP, INC.
Reel/Frame 060836/0322 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 17, 2022
From: EENOTECH GROUP, INC.
To: EENOPURE, INC.
Reel/Frame 060836/0426 →
CHANGE OF NAME Recorded Jul 22, 2020
From: EENOVATE TECHNOLOGY, INC.
To: EENOTECH, INC.
Reel/Frame 053286/0681 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 21, 2020
From: LI, YUANQING; LIU, BOFEI; HUANG, SIDI
To: EENOVATE TECHNOLOGY, INC.
Reel/Frame 053266/0330 →
Continuity (1)
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