IP Library › Granted Patent US 11,407,845
Granted Patent B2
US 11,407,845 · App. 16/335,576 · Granted Aug 9, 2022

Residual monomer content controlling method of polymer

Inventors: Yong Joon Choi (Daejeon, KR); Won Chan Park (Daejon, KR)
Assignee: LG Chem, Ltd.
C08F6/005C08L55/02F26B3/06F26B3/08F26B21/06
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Quick Facts
Patent No.
US 11,407,845
App. No.
16/335,576
Granted
Aug 9, 2022
Kind
B2
Abstract

A method for controlling a residual monomer content of a polymer, wherein when a hot-air temperature and a hot-air velocity are maintained, the controlling method can predict the content of the residual monomer by controlling a hot-air mass ratio without influence of other external factors.

Claims (18)

1. A method for controlling a residual monomer content in a polymer in a drying process using a dryer, comprising:

controlling the residual monomer content to a desired level based on a hot-air mass ratio factor represented by Equation 1 below:

A/B  [Formula 1]

wherein, A is a mass (Kg) of hot-air flowing into the dryer, and B is a mass (Kg) of the polymer flowing into the dryer.

2. The residual monomer content controlling method of the polymer according to claim 1 ,

wherein the residual monomer content in the polymer is controlled without consideration of one or more external factors selected from the group consisting of bed sizes, superficial velocities, hot-air flow rates, retention times and polymer types.

3. The residual monomer content controlling method of the polymer according to claim 1 ,

wherein as the hot-air mass ratio represented by Equation 1 increases, the content of the residual monomer decreases linearly or non-linearly.

4. The residual monomer content controlling method of the polymer according to claim 1 , further comprising:

controlling the residual monomer content based on a hot-air temperature factor.

5. The residual monomer content controlling method of the polymer according to claim 4 ,

wherein the residual monomer content in the polymer is controlled to 4500 ppm or less by maintaining a hot-air temperature in a range of 60 to 100° C. and a hot-air mass ratio in a range of of 2 to 10.

6. The residual monomer content controlling method of the polymer according to claim 4 , further comprising:

controlling the residual monomer content based on a hot-air velocity factor.

7. The residual monomer content controlling method of the polymer according to claim 6 ,

wherein the residual monomer content in the polymer is controlled to 4000 ppm or less by maintaining a hot-air temperature at 70° C. and a hot-air velocity within a range of 0.2 to 0.6 m/s.

8. The residual monomer content controlling method of the polymer according to claim 1 ,

wherein the polymer is acrylonitrile butadiene styrene (ABS) copolymer particles.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 25, 2019
From: CHOI, YONG JOON; PARK, WON CHAN
To: LG CHEM, LTD.
Reel/Frame 048684/0561 →
Priority Claims (1)
KR 10-2016-0121802 · Sep 23, 2016 · national
Continuity (1)
Related Publication 20200017612A1 · Jan 16, 2020