IP Library › Granted Patent US 11,414,989
Granted Patent B2
US 11,414,989 · App. 16/614,586 · Granted Aug 16, 2022

Optical analysis of wellbore fluid demulsifiers

Inventors: Li Guo (Humble, TX); Jay Paul Deville (Spring, TX); William Walter Shumway (Spring, TX); Kay Ann Galindo (Montegomery, TX)
Assignee: Halliburton Energy Services, Inc.
E21B49/08E21B43/38G01N21/5907G01N21/82G01N21/85G01N33/2823G01N2021/5923
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Quick Facts
Patent No.
US 11,414,989
App. No.
16/614,586
Granted
Aug 16, 2022
Kind
B2
Abstract

Embodiments of the present disclosure provide optical methods and systems to evaluate the performance of a demulsifying agent in wellbore fluid. The present embodiments provide an optical system which scans wellbore fluid in order to detect the phase separation caused by a demulsifying agent. Using spectral data, the optical system quantifies the opacity and/or transparency of the different phases in the wellbore fluid in order to evaluate the demulsifying agent.

Claims (37)

1. An optical method to evaluate performance of a demulsifying agent in wellbore fluid, the method comprising:

optically interacting electromagnetic radiation with an emulsified wellbore fluid to produce sample-interacted light, the wellbore fluid comprising an aqueous phase, oil phase, and demulsifying agent;

optically interacting the sample-interacted light with an optical detector to thereby detect separation of the aqueous and oil phases of the wellbore fluid; and

based upon the detected phase separation, evaluating the performance of the demulsifying agent.

2. The optical method as defined in claim 1 , wherein evaluating the performance of the demulsifying agent comprises determining one or more of:

an amount of separated water;

a clarity of the separated water;

an interface angle which reflects a phase separation quality;

a water recovery percentage; and

a speed of the phase separation.

3. The optical method as defined in claim 1 , wherein:

the optical method is performed before a wellbore completion operation; and

the method further comprises selecting a demulsifying agent for use in the wellbore completion operation based upon the performance evaluation.

4. The optical method as defined in claim 1 , wherein the optical method is performed in real-time using an optical device positioned at a wellbore, the optical device being positioned in-line of the wellbore such that the optical device receives flow back fluid from the wellbore.

5. The optical method as defined in claim 4 , further comprising altering a chemical makeup of the demulsifying agent in real-time based upon the performance of the demulsifying agent.

6. The optical method as defined in claim 1 , wherein the method is performed during a Flow-to-Refinery operation.

7. The optical method as defined in claim 1 , further comprising:

based upon the performance evaluation, selecting a demulsifying agent for use in a wellbore operation; and

demulsifying fluid produced by the wellbore operation using the demulsifying agent.

8. An optical system to evaluate performance of a demulsifying agent in wellbore fluid, the system comprising:

a user interface; and

processing circuitry communicably coupled to the user interface and configured to execute instructions to cause the system to perform operations comprising:

optically interacting electromagnetic radiation with an emulsified wellbore fluid to produce sample-interacted light, the wellbore fluid comprising an aqueous phase, oil phase, and demulsifying agent;

optically interacting the sample-interacted light with an optical detector to thereby detect separation of the aqueous and oil phases of the wellbore fluid; and

based upon the detected phase separation, evaluating the performance of the demulsifying agent.

9. The optical system as defined in claim 8 , wherein evaluating the performance of the demulsifying agent comprises determining one or more of:

an amount of separated water;

a clarity of the separated water;

an interface angle which reflects a phase separation quality;

a water recovery percentage; and

a speed of the phase separation.

10. The optical system as defined in claim 8 , wherein:

the operations are performed before a wellbore completion operation; and

the operations further comprise selecting a demulsifying agent for use in the wellbore completion operation based upon the performance evaluation.

11. The optical system as defined in claim 8 , wherein the operations are performed in real-time using an optical device positioned at a wellbore, the optical device being positioned in-line of the wellbore such that the optical device receives flow back fluid from the wellbore.

12. The optical system as defined in claim 11 , wherein the operations further comprise altering a chemical makeup of the demulsifying agent in real-time based upon the performance of the demulsifying agent.

13. The optical system as defined in claim 8 , wherein the optical system is integrated into a Flow-to-Refinery system.

Continuity (2)
Provisional Application 62558154 · Sep 13, 2017
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