IP Library Granted Patent US 11,492,347
Granted Patent B2
US 11,492,347 · App. 16/967,746 · Granted Nov 8, 2022

Fused thiophene derivatives and their uses

Inventors: Eric Meldrum (Riehen, CH); Benoît De Chassey (Lyons, FR); Peter Machin (London, GB); Roberta Lanaro (Cambridge, GB); Calum MacLeod (Harlow, GB); Karine Fabienne Malagu (Cambridge, GB); Nicolas Proisy (Harlow, GB); David Robert Vesey (Harlow Essex, GB); Paul Colin Michael Winship (Cambridge, GB); Mark Chambers (Saffron Walden Essex, GB)
Assignee: ENYO PHARMA
C07D413/14A61P25/28A61P29/00A61P31/14A61P31/16A61P35/00C07D333/66C07D333/68C07D401/12C07D403/12C07D409/12C07D409/14C07D413/12C07D491/107C07D495/04
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Quick Facts
Patent No.
US 11,492,347
App. No.
16/967,746
Granted
Nov 8, 2022
Kind
B2
Abstract

The present invention relates to a new class of fused thiophene derivatives and their uses for treating diseases such as infection, cancer, metabolic diseases, cardiovascular diseases, iron storage disorders and inflammatory disorders.

Claims (67)

1. A compound of formula (I):

wherein:

X represents:

—CR 1b R 1b′ ;

n is 0, 1, or 2;

R 1a , R 1a′ , R 1b , R 1b′ , R 1c , R 1c′ , R 1d , and R 1d′ represent independently:

a hydrogen,

a halogen,

a (C 1 -C 6 )alkyl, optionally substituted by at least one halogen,

a (C 1 -C 6 )alkyloxy,

a cyano, or

an aryl optionally substituted by at least one radical selected from the group consisting of:

a halogen,

a (C 1 -C 6 )alkyl optionally substituted by at least one halogen,

a hydroxy, and

a (C 1 -C 6 )alkyloxy; or

R 1a and R 1a′ , R 1b and R 1b′ , R 1c and R 1c′ , or R 1d and R 1d′ form together a cycloalkyl; or

R 1a or R 1a′ and R 1d or R 1d′ form together a bridged carbocyclyl;

and wherein at least two of R 1a , R 1a′ , R 1b , R 1b′ , R 1c , R 1c′ , R 1d , and R 1d′ are not a hydrogen;

R 2 represents —COOH;

R 3 represents:

a 5-10 membered ring, saturated or unsaturated, selected from the group consisting of:

an aryl optionally fused to a dioxole,

a heteroaryl selected from the group consisting of a pyridinyl, a pyridazinyl, a pyrimidinyl, a pyrazinyl, an imidazolyl, and a pyrazolyl,

a cycloalkyl,

a heterocycloalkyl, and

a 5-10 membered bridged carbocyclyl or heterocyclyl, said 5-10 membered ring is optionally substituted by at least one radical selected from the group consisting of:

a halogen,

a (C 1 -C 6 )alkyl optionally substituted by at least one halogen, or a (C 1 -C 6 )alkyloxy,

a —NH—(C 1 -C 6 )alkyl or a —N—((C 1 -C 6 )alkyl) 2 , optionally substituted by a heterocycloalkyl or a (C 1 -C 6 )alkyloxy,

a —NH-heterocycloalkyl, a —NH-cycloalkyl, a —N((C 1 -C 6 )alkyl)-heterocycloalkyl or a —N((C 1 -C 6 )alkyl)-cycloalkyl, optionally substituted by a (C 1 -C 6 )alkyloxy or a —CO—R 4 with R 4 being a hydrogen or a (C 1 -C 6 )alkyl,

a hydroxy,

a (C 1 -C 6 )alkyloxy optionally substituted by at least one radical selected from the group consisting of a halogen, a hydroxy, a (C 1 -C 6 )alkyloxy, a —NR 5 R 6 with R 5 and R 6 are independently a hydrogen or a (C 1 -C 6 )alkyl, a —NHCOR 7 , a —NHCO 2 R 7 , with R 7 being a (C 1 -C 6 )alkyl, a —CO 2 R 4 with R 4 being a hydrogen or a (C 1 -C 6 )alkyl, and a heterocycle,

a —NHCOR 7 or —NHCO 2 R 7 with R 7 being a (C 1 -C 6 )alkyl, and

a heterocycloalkyl, a heterocycloalkyloxy or a spiroheterocycloalkyl, optionally substituted by a (C 1 -C 6 )alkyloxy, a hydroxy, a halogen or a (C 1 -C 6 )alkyl optionally substituted by a (C 1 -C 6 )alkyloxy; and

the stereoisomers, and the pharmaceutical salts thereof; and

with the proviso that the compound of formula (I) is not 2-[(4-Chlorobenzoylamino]-6,6-dimethyl-5,7-dihydro-4H-benzothiophene-3-carboxylic acid.

2. The compound according to claim 1 , wherein R 1a , R 1a′ , R 1b , R 1b′ , R 1c , R 1c′ , R 1d , and R 1d′ represent independently a hydrogen, a (C 1 -C 6 )alkyl, optionally substituted by at least one halogen, or a halogen; or R 1a or R 1a′ and R 1d or R 1d′ form together a bridged carbocyclyl; or R 1a and R 1a′ , R 1b and R 1b′ , R 1c and R 1c′ , or R 1d and R 1d′ forms together a cyclopropyl.

3. The compound according to claim 1 , wherein R 1a ═R 1a′ , R 1b ═R 1b′ , R 1c ═R 1c′ , and R 1d ═R 1d′ .

4. The compound according to claim 1 , wherein two of R 1a , R 1a′ , R 1b , R 1b′ , R 1c , R 1c′ , R 1d , and R 1d′ represent a methyl and the others are a hydrogen.

5. The compound according to claim 1 , wherein at least three of R 1a , R 1a′ , R 1b , R 1b′ , R 1c , R 1c′ , R 1d , and R 1d′ represent a methyl and the others are a hydrogen.

6. The compound according to claim 1 , wherein R 1b and R 1b′ form together a cycloalkyl, and R 1a , R 1a′ , R 1c , R 1c′ , R 1d , and R 1d′ are a hydrogen.

7. The compound according to claim 1 , wherein R 3 is a phenyl, a pyridinyl, a pyridazinyl, a pyrimidinyl, a pyrazinyl, an imidazolyl, or a pyrazolyl, optionally substituted by at least one radical selected from the group consisting of:

a halogen,

a (C 1 -C 6 )alkyl optionally substituted by at least one halogen, or a (C 1 -C 6 )alkyloxy,

a —NH—(C 1 -C 6 )alkyl or a —N—((C 1 -C 6 )alkyl) 2 , optionally substituted by a heterocycloalkyl or a (C 1 -C 6 )alkyloxy,

a —NH-heterocycloalkyl, a —NH-cycloalkyl, a —N((C 1 -C 6 )alkyl)-heterocycloalkyl or a —N((C 1 -C 6 )alkyl)-cycloalkyl, optionally substituted by a (C 1 -C 6 )alkyloxy or a —CO—R 4 with R 4 being a hydrogen or a (C 1 -C 6 )alkyl,

a hydroxy,

a (C 1 -C 6 )alkyloxy optionally substituted by at least one radical selected from the group consisting of a halogen, a hydroxy, a (C 1 -C 6 )alkyloxy, a —NR 5 R 6 with R 5 and R 6 are independently a hydrogen or a (C 1 -C 6 )alkyl, a —NHCOR 7 , a —NHCO 2 R 7 , with R 7 being a (C 1 -C 6 )alkyl, a —CO 2 R 4 with R 4 being a hydrogen or a (C 1 -C 6 )alkyl, and a heterocycle,

a —NHCOR 7 or —NHCO 2 R 7 with R 7 being a (C 1 -C 6 )alkyl, and

a heterocycloalkyl, a heterocycloalkyloxy or a spiroheterocycloalkyl, optionally substituted by a (C 1 -C 6 )alkyloxy, a hydroxy, a halogen or a (C 1 -C 6 )alkyl optionally substituted by a (C 1 -C 6 )alkyloxy.

8. The compound according to claim 1 , wherein R 3 represents a phenyl optionally substituted by at least one radical selected from the group consisting of:

a halogen;

a (C 1 -C 6 )alkyl optionally substituted by at least one halogen,

a —NH—(C 1 -C 6 )alkyl, or a —N—((C 1 -C 6 )alkyl) 2 , optionally substituted by a (C 1 -C 6 )alkyloxy, or a heterocycloalkyl selected from the group consisting of a tetrahydropyranyl, a tetrahydrofuranyl, an oxetanyl, a piperidinyl, and an azetidinyl, said heterocycloalkyl being optionally substituted by a (C 1 -C 6 )alkyloxy or a —CO—R 4 with R 4 being a hydrogen or a (C 1 -C 6 )alkyl,

a —NH-heterocycloalkyl, a —NH-cycloalkyl, a —N((C 1 -C 6 )alkyl)-heterocycloalkyl, or a —N((C 1 -C 6 )alkyl)-cycloalkyl, a —NH-tetrahydropyranyl, a —N(CH 3 )-tetrahydropyranyl, a —NH-tetrahydrofuranyl, a NH-piperidinyl, a —NH-azetidinyl, a —NH-oxetanyl, a-NH-cyclohexyl, or a —N(CH 3 )-cyclobutyl, said —NH-heterocycloalkyl, —NH-cycloalkyl, —N((C 1 -C 6 )alkyl)-heterocycloalkyl, or —N((C 1 -C 6 )alkyl)-cycloalkyl being optionally substituted by a (C 1 -C 6 )alkyloxy or a —CO—R 4 with R 4 being a hydrogen or a (C 1 -C 6 )alkyl,

a (C 1 -C 6 )alkyloxy optionally substituted by at least one radical selected from the group consisting of a halogen, a (C 1 -C 6 )alkyloxy, and a heterocycle, and

a heterocycloalkyl or a spiroheterocycloalkyl, said heterocycloalkyl and spiroheterocycloalkyl are optionally substituted by a (C 1 -C 6 )alkyloxy, a hydroxy, a halogen or a (C 1 -C 6 )alkyl optionally substituted by a (C 1 -C 6 )alkyloxy, and

a heterocycloalkyloxy.

9. The compound according to claim 1 , wherein R 3 represents a pyridinyl, a pyridazinyl, a pyrimidinyl, a pyrazolyl, an imidazolyl, or a pyrazinyl, optionally substituted by at least one radical selected from the group consisting of:

a (C 1 -C 6 )alkyl optionally substituted by at least one halogen,

a (C 1 -C 6 )alkyloxy optionally substituted by at least one halogen,

a heterocycloalkyl, and

a heterocycloalkyloxy.

10. The compound according to claim 1 , wherein said compound is selected from the group consisting of:

11. A pharmaceutical composition comprising a compound as defined in claim 1 and an acceptable pharmaceutical excipient.

12. A pharmaceutical composition comprising a compound as defined in claim 10 and an acceptable pharmaceutical excipient.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 12, 2021
From: MELDRUM, ERIC; DE CHASSEY, BENOÎT; MACHIN, PETER; LANARO, ROBERTA; MACLEOD, CALUM; MALAGU, KARINE FABIENNE; PROISY, NICOLAS; VESEY, DAVID ROBERT; WINSHIP, PAUL COLIN MICHAEL; CHAMBERS, MARK
To: ENYO PHARMA
Reel/Frame 055571/0343 →
Priority Claims (1)
EP 18305133 · Feb 8, 2018 · regional
Continuity (1)
Related Publication 20200361924A1 · Nov 19, 2020
Cited By (1)
US 12,691,118