IP Library › Granted Patent US 11,504,303
Granted Patent B2
US 11,504,303 · App. 17/557,483 · Granted Nov 22, 2022

Pulp regeneration compositions and methods of forming and using the same

Inventors: Pamela C. Yelick (Boston, MA); Ali Khademhosseini (Cambridge, MA)
Assignees: TRUSTEES OF TUFTS COLLEGE; THE BRIGHAM AND WOMEN'S HOSPITAL, INC.
A61K6/62A61C5/40A61K6/56
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,504,303
App. No.
17/557,483
Granted
Nov 22, 2022
Kind
B2
Abstract

A dental tissue regenerative composition. The composition includes a combination of (1) human dental pulp stem cells and (2) at least one of human umbilical vein endothelial cells or vascular endothelial growth factor. The combination is encapsulated in a light-activated gelatin methacrylate hydrogel.

Claims (36)

1. A dental tissue regenerative composition comprising:

a material at least partly obtained from an extracted tooth; and

a light-activated gelatin methacrylate hydrogel encapsulating the material.

2. The composition of claim 1 , further comprising a photo-initiator.

3. The composition of claim 2 , wherein the photo-initiator is present at a concentration of about 0.05% to about 0.5% (w/v).

4. The composition of claim 1 , wherein the photo-initiator is selected from the group consisting of: 1-[4-(2-hydroxyethoxy)-phenyl]-2-hydroxy-2-methyl-1-propane-1-one, azobisisobutyronitrile, benzoyl peroxide, di-tert-butyl peroxide, 2,2-dimethoxy-2-phenylacetophenone, Eosin Y, and any combination thereof.

5. The composition of claim 1 , wherein the gelatin methacrylate hydrogel is present at a concentration of about 3% to about 5% (w/v).

6. The composition of claim 1 , wherein the material obtained from the extracted tooth includes dental pulp stem cells.

7. The composition of claim 6 , wherein the material further includes at least one of umbilical vein endothelial cells or vascular endothelial growth factor.

8. The composition of claim 6 , wherein the dental pulp stem cells have been isolated from dental pulp.

9. The composition of claim 8 , wherein the dental pulp is from a mature tooth.

10. The composition of claim 1 , wherein the composition is configured to be used for pulpal revascularization, to replace infected pulpal tissues in pulpotomy, as a temporary intra canal medicament, or for regenerating pulp-like tissues in tooth root segments.

11. A method of regenerating pulp-like tissues in a tooth root segment of a tooth, the method comprising:

providing a composition comprising

a gelatin methacrylate hydrogel,

a photo-initiator, and

a material at least partly obtained from an extracted tooth, the gelatin methacrylate hydrogel and the material having been cross-linked by exposure to a UV or visible light; and

injecting the composition into the tooth root segment.

12. The method of claim 11 , wherein the photo-initiator is present in the composition at a concentration of about 0.05% to about 0.5% (w/v).

13. The method of claim 11 , wherein the photo-initiator is selected from the group consisting of: 1-[4-(2-hydroxyethoxy)-phenyl]-2-hydroxy-2-methyl-1-propane-1-one, azobisisobutyronitrile, benzoyl peroxide, di-tert-butyl peroxide, 2,2-dimethoxy-2-phenylacetophenone, Eosin Y, and any combination thereof.

14. The method of claim 11 , wherein the gelatin methacrylate hydrogel is present in the composition at a concentration of about 3% to about 5% (w/v).

15. The method of claim 11 , wherein the material obtained from the extracted tooth includes dental pulp stem cells.

16. The method of claim 15 , wherein the material further comprises at least one of umbilical vein endothelial cells or vascular endothelial growth factor.

17. The method of claim 15 , wherein the dental pulp stem cells have been isolated from dental pulp.

18. The method of claim 17 , wherein the dental pulp is from a mature tooth.

19. A method of forming a dental tissue regenerative composition, the method comprising:

combining a material at least partly obtained from an extracted tooth, a gelatin methacrylate hydrogel, and a photo-initiator; and

cross-linking the gelatin methacrylate hydrogel with the material by exposure to a UV or visible light.

20. The method of claim 19 , wherein the photo-initiator is present at a concentration of about 0.05% to about 0.5% (w/v).

21. The method of claim 19 , wherein the photo-initiator is selected from the group consisting of: 1-[4-(2-hydroxyethoxy)-phenyl]-2-hydroxy-2-methyl-1-propane-1-one, azobisisobutyronitrile, benzoyl peroxide, di-tert-butyl peroxide, 2,2-dimethoxy-2-phenylacetophenone, Eosin Y, and any combination thereof.

22. The method of claim 19 , wherein the gelatin methacrylate hydrogel is present at a concentration of about 3% to about 5% (w/v).

23. The method of claim 19 , wherein the material obtained from the extracted tooth includes dental pulp stem cells.

24. The method of claim 23 , wherein the material further comprises at least one of umbilical vein endothelial cells or vascular endothelial growth factor.

25. The method of claim 23 , wherein the dental pulp stem cells have been isolated from dental pulp.

26. The method of claim 25 , wherein the dental pulp is from a mature tooth.

27. The method of claim 19 , wherein the composition is configured to be used for pulpal revascularization, to replace infected pulpal tissues in pulpotomy, as a temporary intra canal medicament or for regenerating pulp-like tissues in tooth root segments.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2022
From: YELICK, PAMELA C.
To: TRUSTEES OF TUFTS COLLEGE
Reel/Frame 059215/0617 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2022
From: KHADEMHOSSEINI, ALI
To: THE BRIGHAM AND WOMEN'S HOSPITAL, INC.
Reel/Frame 059215/0664 →
Continuity (3)
Continuation 15777304
Provisional Application 62428870 · Dec 1, 2016
Related Publication 20220110836A1 · Apr 14, 2022