IP Library › Granted Patent US 11,505,748
Granted Patent B2
US 11,505,748 · App. 16/331,944 · Granted Nov 22, 2022

Pitch granules which are solid at room temperature

Inventor: Jean-Pierre Mesnil (Puteaux, FR)
Assignee: TOTAL MARKETING SERVICES
C10C3/14B01J2/003B01J2/12B01J2/30C08J7/0427C08J7/06C08L95/00C08J2395/00C08J2401/08C08J2403/02C08J2403/04C08J2405/00C08J2405/04C08J2405/12C08J2471/02C08J2489/06
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Quick Facts
Patent No.
US 11,505,748
App. No.
16/331,944
Granted
Nov 22, 2022
Kind
B2
Abstract

Pitch granules including a core made up of a first composition including at least one pitch, the composition having a penetrability at 25° C. of 0 to 45 1/10 mm, a ring-and-ball softening temperature (TBA) of 55° C. to 175° C., understanding the penetrability as measured according to standard EN 1426 and the TBA as measured according to standard EN 1427, and a layer encapsulating at least one portion of the surface of the core, the layer being made up of a coating composition including at least one anti-caking agent.

Claims (26)

1. Pitch pellets comprising:

a core constituted of a first composition comprising at least one pitch, said composition having a penetrability at 25° C. ranging from 1 to 45 1/10 mm and a ring and ball softening point (RBSP) ranging from 55° C. to 175° C., wherein the penetrability is measured according to the standard EN 1426 and that the RBSP is measured according to the standard EN 1427, and

a layer coating at least part of the surface of the core, said layer being constituted of a coating composition comprising at least one anticaking agent chosen from pyrogenic silicas, and mixtures thereof, wherein the pyrogenic silicas have a specific surface area of between 120 and 280 m 2 /g.

2. The pitch pellets of claim 1 , wherein the anticaking agent is chosen from hydrophobic or hydrophilic pyrogenic silicas and mixtures thereof.

3. The pitch pellets of claim 1 , wherein the coating composition comprises at least 10% by mass of anticaking agent, relative to the total mass of the composition.

4. The pitch pellets of claim 3 , wherein the coating composition comprises from 10% to 90% by mass of anticaking agent, relative to the total mass of the composition.

5. The pitch pellets of claim 4 , wherein the coating composition comprises from 15% to 90% by mass of anticaking agent, relative to the total mass of the composition.

6. The pitch pellets of claim 1 , wherein the coating composition further comprises at least one viscosifying compound.

7. The pitch pellets of claim 6 , wherein the viscosifying compound is selected from the group consisting of:

gelling compounds;

polyethylene glycols (PEGs);

and mixtures thereof.

8. The pitch pellets of claim 6 , wherein the viscosifying compound is chosen from gelling compounds of plant or animal origin.

9. The pitch pellets as claimed 8 , wherein the gelling compound is selected from the group consisting of gelatin, agar-agar, alginates, cellulose derivatives, starches, modified starches and gellan gums.

10. The pitch pellets of claim 6 , wherein the viscosifying compound is chosen from polyethylene glycols (PEGs) having a molecular weight of between 800 g·mol −1 and 8000 g·mol −1 .

11. The pitch pellets of claim 10 , wherein the viscosifying compound is selected from the group consisting of: a PEG with a molecular weight of 800 g·mol −1 (PEG-800), a PEG with a molecular weight of 1000 g·mol −1 (PEG-1000), a PEG with a molecular weight of 1500 g·mol −1 (PEG-1500), a PEG with a molecular weight of 4000 g·mol −1 (PEG-4000) and a PEG with a molecular weight of 6000 g·mol −1 (PEG-6000).

12. The pitch pellets of claim 1 , wherein the coating composition represents between 0.2% and 10% by mass, relative to the total mass of the core of the pitch pellets.

13. The pitch pellets of claim 1 , wherein the coating composition represents between 0.5% and 8% by mass, relative to the total mass of the core of the pitch pellets.

14. The pitch pellets of claim 1 , wherein the coating composition represents between 0.5% and 5% by mass, relative to the total mass of the core of the pitch pellets.

15. The pitch pellets of claim 1 , wherein the size of the pellets is such that the longest mean dimension is less than or equal to 50 mm.

16. The pitch pellets of claim 15 , wherein the size of the pellets is such that the longest mean dimension is from 2 to 30 mm.

17. The pitch pellets of claim 1 , wherein the pellets solid at ambient temperature.

18. A process for manufacturing the pitch pellets of claim 1 , comprising:

i) forming the core of the pellets using a first composition comprising at least one pitch, and

ii) coating the core of the pellets over all or part of their surface with a coating composition comprising at least one anticaking compound.

19. A process comprising at least one of transporting, storing, and handling pitch at ambient temperature, wherein the pitch is in the form of the pitch pellets of claim 1 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 25, 2019
From: MESNIL, JEAN-PIERRE
To: TOTAL MARKETING SERVICES
Reel/Frame 050492/0872 →
Priority Claims (1)
FR 1658338 · Sep 8, 2016 · national
Continuity (1)
Related Publication 20190241813A1 · Aug 8, 2019
Cited By (1)
US 12,687,907